JPS5770283A - Electrochemical fluorination of org. compound - Google Patents
Electrochemical fluorination of org. compoundInfo
- Publication number
- JPS5770283A JPS5770283A JP55147970A JP14797080A JPS5770283A JP S5770283 A JPS5770283 A JP S5770283A JP 55147970 A JP55147970 A JP 55147970A JP 14797080 A JP14797080 A JP 14797080A JP S5770283 A JPS5770283 A JP S5770283A
- Authority
- JP
- Japan
- Prior art keywords
- org
- compound
- sulfone
- electrochemical
- electrochemical fluorination
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
PURPOSE: To enhance efficiency of electrochemical fluorination by electrochemically fluorinating an org. compound in the presence of saturated cyclic sulfone to reduce frequency of cleaning of an electrode and exchange of an electrolyte solution.
CONSTITUTION: In subjecting an org. compound to electrochemical fluorinating reaction, a saturated cyclic sulfone shown by a formulaI(wherein R is H or 1W4C alkyl, n is 3W11) is added in an electrolyte solution along with an org. compound and maintained in a desired concn. range. Said sulfone is simultaneously fluorinated along with the org. compound but, by the presence of said sulfone, formation of a resin like polymer is controlled and prevented and, as the result, an electrolytic time can be prolonged to a large extent.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55147970A JPS5770283A (en) | 1980-10-22 | 1980-10-22 | Electrochemical fluorination of org. compound |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55147970A JPS5770283A (en) | 1980-10-22 | 1980-10-22 | Electrochemical fluorination of org. compound |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5770283A true JPS5770283A (en) | 1982-04-30 |
JPS636633B2 JPS636633B2 (en) | 1988-02-10 |
Family
ID=15442211
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55147970A Granted JPS5770283A (en) | 1980-10-22 | 1980-10-22 | Electrochemical fluorination of org. compound |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5770283A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006348382A (en) * | 2005-05-17 | 2006-12-28 | Asahi Kasei Corp | Electrolytic fluorination method |
WO2011093371A1 (en) * | 2010-01-27 | 2011-08-04 | 三菱マテリアル株式会社 | Process for producing perfluorobutanesulfonic acid salt |
-
1980
- 1980-10-22 JP JP55147970A patent/JPS5770283A/en active Granted
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006348382A (en) * | 2005-05-17 | 2006-12-28 | Asahi Kasei Corp | Electrolytic fluorination method |
WO2011093371A1 (en) * | 2010-01-27 | 2011-08-04 | 三菱マテリアル株式会社 | Process for producing perfluorobutanesulfonic acid salt |
CN102741457A (en) * | 2010-01-27 | 2012-10-17 | 三菱综合材料株式会社 | Process for producing perfluorobutanesulfonic acid salt |
JP5497799B2 (en) * | 2010-01-27 | 2014-05-21 | 三菱マテリアル株式会社 | Process for producing perfluorobutane sulfonate |
Also Published As
Publication number | Publication date |
---|---|
JPS636633B2 (en) | 1988-02-10 |
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