JPS57175141A - Preparation of iron organic carboxylate - Google Patents

Preparation of iron organic carboxylate

Info

Publication number
JPS57175141A
JPS57175141A JP56059781A JP5978181A JPS57175141A JP S57175141 A JPS57175141 A JP S57175141A JP 56059781 A JP56059781 A JP 56059781A JP 5978181 A JP5978181 A JP 5978181A JP S57175141 A JPS57175141 A JP S57175141A
Authority
JP
Japan
Prior art keywords
iron powder
dialkyl dithiocarbamate
iron
molecular oxygen
flow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP56059781A
Other languages
Japanese (ja)
Other versions
JPS6248657B2 (en
Inventor
Takahisa Sato
Noboru Miyake
Masao Baba
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Priority to JP56059781A priority Critical patent/JPS57175141A/en
Publication of JPS57175141A publication Critical patent/JPS57175141A/en
Publication of JPS6248657B2 publication Critical patent/JPS6248657B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Abstract

PURPOSE: To obtain the titled compound usable as a catalyst, etc. in a short time at a low temperature, by dissolving iron powder in an organic carboxylic acid in the presence of a dialkyl dithiocarbamate as a dissolution accelerator under the flow of molecular oxygen.
CONSTITUTION: Iron powder, usually a particle size in the range of 50W500mesh, is dissolved in an organic carboxylic acid preferably by using air directly at an air flow rate of 1.5W2.0l/g iron powder/hr under the flow of molecular oxygen to prepare an iron organic carboxylate. In the process, a dialkyl dithiocarbamate in an amount of 0.1W30wt%, preferably 1W5wt%, based on the iron powder added thereto is present, and the reaction is carried out at 50W100°C for 50W 100min. Acrylic acid or methacrylic acid in which the iron powder is slightly siluble is particularly effective, and the dialkyl dithiocarbamate has a polymerization inhibiting ability for polymerizable unsaturated carboxylic acids.
COPYRIGHT: (C)1982,JPO&Japio
JP56059781A 1981-04-22 1981-04-22 Preparation of iron organic carboxylate Granted JPS57175141A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP56059781A JPS57175141A (en) 1981-04-22 1981-04-22 Preparation of iron organic carboxylate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56059781A JPS57175141A (en) 1981-04-22 1981-04-22 Preparation of iron organic carboxylate

Publications (2)

Publication Number Publication Date
JPS57175141A true JPS57175141A (en) 1982-10-28
JPS6248657B2 JPS6248657B2 (en) 1987-10-15

Family

ID=13123173

Family Applications (1)

Application Number Title Priority Date Filing Date
JP56059781A Granted JPS57175141A (en) 1981-04-22 1981-04-22 Preparation of iron organic carboxylate

Country Status (1)

Country Link
JP (1) JPS57175141A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03223077A (en) * 1988-06-06 1991-10-02 Hiroshi Yamamoto Floating elevator device
JP2006524284A (en) * 2003-04-23 2006-10-26 ノル−エクス インドストリー アーエス Additive for thermoplastic resin, use and production method thereof, production method of thermoplastic resin containing such additive, and thermoplastic resin thus produced
WO2012090905A1 (en) 2010-12-27 2012-07-05 三菱レイヨン株式会社 Processes for production of iron methacrylate and hydroxyalkyl methacrylate
JP2013016750A (en) * 2011-07-06 2013-01-24 Sumitomo Electric Ind Ltd Method for producing iron nitride powder
WO2014030523A1 (en) 2012-08-24 2014-02-27 三菱レイヨン株式会社 Method for producing iron carbonate

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03223077A (en) * 1988-06-06 1991-10-02 Hiroshi Yamamoto Floating elevator device
JP2006524284A (en) * 2003-04-23 2006-10-26 ノル−エクス インドストリー アーエス Additive for thermoplastic resin, use and production method thereof, production method of thermoplastic resin containing such additive, and thermoplastic resin thus produced
WO2012090905A1 (en) 2010-12-27 2012-07-05 三菱レイヨン株式会社 Processes for production of iron methacrylate and hydroxyalkyl methacrylate
CN103249706A (en) * 2010-12-27 2013-08-14 三菱丽阳株式会社 Processes for production of iron methacrylate and hydroxyalkyl methacrylate
US8697899B2 (en) 2010-12-27 2014-04-15 Mitsubishi Rayon Co., Ltd. Methods for producing iron methacrylate and hydroxyalkyl methacrylate
EP2660236A4 (en) * 2010-12-27 2015-11-11 Mitsubishi Rayon Co Processes for production of iron methacrylate and hydroxyalkyl methacrylate
JP2013016750A (en) * 2011-07-06 2013-01-24 Sumitomo Electric Ind Ltd Method for producing iron nitride powder
WO2014030523A1 (en) 2012-08-24 2014-02-27 三菱レイヨン株式会社 Method for producing iron carbonate
JPWO2014030523A1 (en) * 2012-08-24 2016-07-28 三菱レイヨン株式会社 Method for producing iron carboxylate
US9540308B2 (en) 2012-08-24 2017-01-10 Mitsubishi Rayon Co., Ltd. Method for producing iron carboxylate
JP2018002732A (en) * 2012-08-24 2018-01-11 三菱ケミカル株式会社 Method for producing iron carboxylate
JP2018002731A (en) * 2012-08-24 2018-01-11 三菱ケミカル株式会社 Method for producing iron carboxylate

Also Published As

Publication number Publication date
JPS6248657B2 (en) 1987-10-15

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