JPS5673611A - Manufacture of alkali monofluorophosphate - Google Patents
Manufacture of alkali monofluorophosphateInfo
- Publication number
- JPS5673611A JPS5673611A JP15075879A JP15075879A JPS5673611A JP S5673611 A JPS5673611 A JP S5673611A JP 15075879 A JP15075879 A JP 15075879A JP 15075879 A JP15075879 A JP 15075879A JP S5673611 A JPS5673611 A JP S5673611A
- Authority
- JP
- Japan
- Prior art keywords
- alkali
- metaphosphate
- hydrogen fluoride
- monofluorophosphate
- soln
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
PURPOSE: To easily obtain alkali monofluorophosphate by treating alkali metaphosphate with hydrogen fluoride and neutralizing the product with an alkali metal salt soln.
CONSTITUTION: Alkali metaphosphate is fluorinated with hydrogen fluoride at ordinary temp.Wabout 150°C by mixing hydrogen fluoride gas into the metaphosphate by an equimolar amount or more. The metaphosphate is used in the form of powder, granules or the like. The resulting alkali hydrogenmonofluorophosphate is neutralized with an alkali metal salt soln. such as a soln. of caustic soda or sodium carbonate. The temp. is preferably kept at about 0W20°C. After the reaction the neutralization product is separated by suction filtration and dried at ≤about 100°C. Thus, alkali monofluorophosphate is easily manufactured.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15075879A JPS593927B2 (en) | 1979-11-22 | 1979-11-22 | Method for producing alkali monofluorophosphate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15075879A JPS593927B2 (en) | 1979-11-22 | 1979-11-22 | Method for producing alkali monofluorophosphate |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5673611A true JPS5673611A (en) | 1981-06-18 |
JPS593927B2 JPS593927B2 (en) | 1984-01-26 |
Family
ID=15503763
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15075879A Expired JPS593927B2 (en) | 1979-11-22 | 1979-11-22 | Method for producing alkali monofluorophosphate |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS593927B2 (en) |
-
1979
- 1979-11-22 JP JP15075879A patent/JPS593927B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS593927B2 (en) | 1984-01-26 |
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