JPS5643239A - Preparation of 1,4,4a,9a-tetrahydroanthraquinone compound - Google Patents
Preparation of 1,4,4a,9a-tetrahydroanthraquinone compoundInfo
- Publication number
- JPS5643239A JPS5643239A JP11738879A JP11738879A JPS5643239A JP S5643239 A JPS5643239 A JP S5643239A JP 11738879 A JP11738879 A JP 11738879A JP 11738879 A JP11738879 A JP 11738879A JP S5643239 A JPS5643239 A JP S5643239A
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- thaq
- compound
- produced
- conjugated diolefin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare the titled compound in high quality and yield, with simple process, by the Diels-Alder reaction of 1,4-naphthoquinone with a conjugated diolefin compound using the produced titled compound as a reaction medium.
CONSTITUTION: A liquid or gaseous conjugated diolefin compound is intorduced into a mixture of 1,4-naphthoquinone (NQ) and 1,4,4a,9a-tetrahydroanthraquinone compound (THAQ) maintained at a temperature above the melting point of THAQ, pref. at 110W150°C. After the completion of the reaction, a part of the produced THAQ is extracted from the system, and recycled as the medium of said reaction. The remaining part of the THAQ is utilized as the objective product. Similar effect can be also attained by introducing the conjuagated diolefin compound at the initial stage of the reaction into molten NQ under the reaction conditions, and completing the reaction in the presence of the produced THAQ.
EFFECT: The recovery of the conjugated diolefin compound used in excess is facilitated.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11738879A JPS6045864B2 (en) | 1979-09-14 | 1979-09-14 | Method for producing 1,4,4a,9a-tetrahydroanthraquinone compound |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11738879A JPS6045864B2 (en) | 1979-09-14 | 1979-09-14 | Method for producing 1,4,4a,9a-tetrahydroanthraquinone compound |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5643239A true JPS5643239A (en) | 1981-04-21 |
JPS6045864B2 JPS6045864B2 (en) | 1985-10-12 |
Family
ID=14710406
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11738879A Expired JPS6045864B2 (en) | 1979-09-14 | 1979-09-14 | Method for producing 1,4,4a,9a-tetrahydroanthraquinone compound |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6045864B2 (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62185869U (en) * | 1986-05-19 | 1987-11-26 | ||
JPS6421222U (en) * | 1987-07-28 | 1989-02-02 | ||
JPH0286950A (en) * | 1988-09-20 | 1990-03-27 | Mazda Motor Corp | Intake air system for engine |
-
1979
- 1979-09-14 JP JP11738879A patent/JPS6045864B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS6045864B2 (en) | 1985-10-12 |
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