JPS56133277A - 3,4,5,6,7-pentachloro-1,2-benzoisothiazole-1,1-dioxide and its preparation - Google Patents
3,4,5,6,7-pentachloro-1,2-benzoisothiazole-1,1-dioxide and its preparationInfo
- Publication number
- JPS56133277A JPS56133277A JP3638680A JP3638680A JPS56133277A JP S56133277 A JPS56133277 A JP S56133277A JP 3638680 A JP3638680 A JP 3638680A JP 3638680 A JP3638680 A JP 3638680A JP S56133277 A JPS56133277 A JP S56133277A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- benzoisothiazole
- pentachloro
- dioxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Abstract
NEW MATERIAL:3,4,5,6,7-Pentachloro-1, 2-benzoisothiazole-1, 1-dioxide of formula I.
USE: Useful as an intermediate of pesticides, pharmaceuticals, pigments, etc. especially as an intermediate of bisazomethine pigments.
PROCESS: The compound of formula II is made to react with methanol in the presence of a mineral acid as a catalyst, and the resulting novel compound of formula III is made to react with sodium hydroxide, etc. The reaction product is successively reacted with a chlorinating agent to afford the compound of formula V, which is reacted with ammonia water added thereto in a proper inert solvent at 10°C W room temp. Neutralization of the precipitated compound with hydrochloric acid, etc. gives the compound of formula VI, which can be converted to the objective compound of formula I by reacting with phosphorus pentachloride or phosgen in the presence of a catalyst in an organic solvent such as ethylene glycol.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP3638680A JPS56133277A (en) | 1980-03-22 | 1980-03-22 | 3,4,5,6,7-pentachloro-1,2-benzoisothiazole-1,1-dioxide and its preparation |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP3638680A JPS56133277A (en) | 1980-03-22 | 1980-03-22 | 3,4,5,6,7-pentachloro-1,2-benzoisothiazole-1,1-dioxide and its preparation |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS56133277A true JPS56133277A (en) | 1981-10-19 |
Family
ID=12468400
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP3638680A Pending JPS56133277A (en) | 1980-03-22 | 1980-03-22 | 3,4,5,6,7-pentachloro-1,2-benzoisothiazole-1,1-dioxide and its preparation |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56133277A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113264900A (en) * | 2021-06-07 | 2021-08-17 | 南京中医药大学 | Preparation method and medical application of benzisothiazole and benzothiophene |
-
1980
- 1980-03-22 JP JP3638680A patent/JPS56133277A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113264900A (en) * | 2021-06-07 | 2021-08-17 | 南京中医药大学 | Preparation method and medical application of benzisothiazole and benzothiophene |
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