JPS5583727A - Purification of ortho ester - Google Patents
Purification of ortho esterInfo
- Publication number
- JPS5583727A JPS5583727A JP15710678A JP15710678A JPS5583727A JP S5583727 A JPS5583727 A JP S5583727A JP 15710678 A JP15710678 A JP 15710678A JP 15710678 A JP15710678 A JP 15710678A JP S5583727 A JPS5583727 A JP S5583727A
- Authority
- JP
- Japan
- Prior art keywords
- alkyl
- ortho ester
- aqueous alkali
- purification
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000002905 orthoesters Chemical class 0.000 title abstract 3
- 238000000746 purification Methods 0.000 title 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- 239000003513 alkali Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 238000006136 alcoholysis reaction Methods 0.000 abstract 1
- 125000003342 alkenyl group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 229940079593 drug Drugs 0.000 abstract 1
- LBAQSKZHMLAFHH-UHFFFAOYSA-N ethoxyethane;hydron;chloride Chemical compound Cl.CCOCC LBAQSKZHMLAFHH-UHFFFAOYSA-N 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000000543 intermediate Substances 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15710678A JPS5583727A (en) | 1978-12-19 | 1978-12-19 | Purification of ortho ester |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15710678A JPS5583727A (en) | 1978-12-19 | 1978-12-19 | Purification of ortho ester |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5583727A true JPS5583727A (en) | 1980-06-24 |
JPS6210215B2 JPS6210215B2 (enrdf_load_stackoverflow) | 1987-03-05 |
Family
ID=15642354
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15710678A Granted JPS5583727A (en) | 1978-12-19 | 1978-12-19 | Purification of ortho ester |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5583727A (enrdf_load_stackoverflow) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103130622A (zh) * | 2011-11-28 | 2013-06-05 | 重庆紫光化工股份有限公司 | 一种原甲酸三甲酯的制备方法 |
JP2014208698A (ja) * | 2007-04-11 | 2014-11-06 | 第一三共株式会社 | ノイラミン酸誘導体の製造方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS51108012A (en) * | 1975-03-19 | 1976-09-25 | Kuraray Co | Orutoesuteruno seizohoho |
-
1978
- 1978-12-19 JP JP15710678A patent/JPS5583727A/ja active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS51108012A (en) * | 1975-03-19 | 1976-09-25 | Kuraray Co | Orutoesuteruno seizohoho |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2014208698A (ja) * | 2007-04-11 | 2014-11-06 | 第一三共株式会社 | ノイラミン酸誘導体の製造方法 |
CN103130622A (zh) * | 2011-11-28 | 2013-06-05 | 重庆紫光化工股份有限公司 | 一种原甲酸三甲酯的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
JPS6210215B2 (enrdf_load_stackoverflow) | 1987-03-05 |
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