JPS5540630A - Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide - Google Patents

Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide

Info

Publication number
JPS5540630A
JPS5540630A JP11365178A JP11365178A JPS5540630A JP S5540630 A JPS5540630 A JP S5540630A JP 11365178 A JP11365178 A JP 11365178A JP 11365178 A JP11365178 A JP 11365178A JP S5540630 A JPS5540630 A JP S5540630A
Authority
JP
Japan
Prior art keywords
phenol
tetramethylbutyl
pref
reacting
suspended state
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11365178A
Other languages
Japanese (ja)
Other versions
JPS5725544B2 (en
Inventor
Teruhiro Yamaguchi
Tadashi Kobayashi
Keisaburo Yamaguchi
Naomichi Murakami
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP11365178A priority Critical patent/JPS5540630A/en
Priority to AU50174/79A priority patent/AU530175B2/en
Priority to US06/070,614 priority patent/US4248804A/en
Priority to GB7930551A priority patent/GB2031414B/en
Priority to FR7922178A priority patent/FR2435468A1/en
Priority to IT25525/79A priority patent/IT1193500B/en
Priority to NLAANVRAGE7906700,A priority patent/NL186445C/en
Priority to DE2936288A priority patent/DE2936288C2/en
Publication of JPS5540630A publication Critical patent/JPS5540630A/en
Publication of JPS5725544B2 publication Critical patent/JPS5725544B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To prepare the title compound in high purity and yield, useful as a modifier of polyethylene, by reacting 4-(1,1,3,3-tetramethylbutyl) phenol with sulfur monochloride, at specific temperature conditions, in a suspended state, and separating the objective compound easily from the reaction mixture.
CONSTITUTION: The compound of formula is prepared by reacting (2moles of) 4- (1,1,3,3-tetramethylbutyl) phenol with (pref. 1mole of) sulfur monochloride, pref. in the presence of a catalytic amount of a Lewis acid, in an organic solvent (0.5W 1.0, pref. about 2W5vol.parts per 1wt.part of the phenol), especially an aliphatic or cycloaliphatic saturated hydrocarbon such as butane or pentane, in a suspended state, at -10W40°C.
COPYRIGHT: (C)1980,JPO&Japio
JP11365178A 1978-09-07 1978-09-18 Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide Granted JPS5540630A (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
JP11365178A JPS5540630A (en) 1978-09-18 1978-09-18 Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide
AU50174/79A AU530175B2 (en) 1978-09-07 1979-08-22 Preparation of 2,2:-bis(4-(1,1,3,3-tetramethylbutyl) -phenol)sulphide
US06/070,614 US4248804A (en) 1978-09-07 1979-08-29 Process for the preparation of 2,2'-bis[4-(1,1,3,3-tetramethylbutyl)phenol]sulfide
GB7930551A GB2031414B (en) 1978-09-07 1979-09-04 Process for the preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl)-phenol) sulphide
FR7922178A FR2435468A1 (en) 1978-09-07 1979-09-05 PROCESS FOR THE PREPARATION OF SULFIDE OF 2,2'-BIS (4- (1,1,3,3-TETRAMETHYLBUTYL) PHENOL)
IT25525/79A IT1193500B (en) 1978-09-07 1979-09-06 PROCESS FOR THE PREPARATION OF 2,2'-BIS / 4- (1,1,3,3-TETRAMETHYLBUTYL) FENOL / SULPHIDE
NLAANVRAGE7906700,A NL186445C (en) 1978-09-07 1979-09-07 PROCESS FOR PREPARING 2,2'-BIS (4- (1,1,3,3-TETRAMETHYLBUTYL) PHENOL) SULFIDE.
DE2936288A DE2936288C2 (en) 1978-09-07 1979-09-07 Process for the preparation of 2,2'-bis-[4-(1,1,3,3-tetramethylbutyl)phenol] sulfide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11365178A JPS5540630A (en) 1978-09-18 1978-09-18 Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide

Publications (2)

Publication Number Publication Date
JPS5540630A true JPS5540630A (en) 1980-03-22
JPS5725544B2 JPS5725544B2 (en) 1982-05-29

Family

ID=14617662

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11365178A Granted JPS5540630A (en) 1978-09-07 1978-09-18 Preparation of 2,2'-bis(4-(1,1,3,3-tetramethylbutyl) phenol) sulfide

Country Status (1)

Country Link
JP (1) JPS5540630A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02282060A (en) * 1989-04-22 1990-11-19 Koa Glass Kk Preventive structure of bottle cap from loosening and molding thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02282060A (en) * 1989-04-22 1990-11-19 Koa Glass Kk Preventive structure of bottle cap from loosening and molding thereof

Also Published As

Publication number Publication date
JPS5725544B2 (en) 1982-05-29

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