JPS54135747A - Preparation of cyclohexylmercaptan - Google Patents
Preparation of cyclohexylmercaptanInfo
- Publication number
- JPS54135747A JPS54135747A JP4368578A JP4368578A JPS54135747A JP S54135747 A JPS54135747 A JP S54135747A JP 4368578 A JP4368578 A JP 4368578A JP 4368578 A JP4368578 A JP 4368578A JP S54135747 A JPS54135747 A JP S54135747A
- Authority
- JP
- Japan
- Prior art keywords
- reacted
- formula
- cyclohexanol
- give
- cyclohexylmercaptan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain the title compound at low cost, high yield and purity, in a simple process, without causing pollution, by reacting cyclohexanone or cyclohexanol with H2S in the gaseous phase in the presence of a specific catalyst.
CONSTITUTION: Cyclohexanone of formula I is reacted with H2S in the gaseous phase in the presence of H2 and a catalyst, e.g. a metal oxide or sulfide, or Ni, containing at least one type of metal of Group VIB or VIII in the periodic table at 100W300°C to give cyclohexylmercaptan of formula III. Alternatively, cyclohexanol of formula II is reacted with H2S in the absence of H2. The by-product cyclohexene is also reacted with H2S under the similar reaction conditions to give the compound of formula III.
USE: Polymerization modifiers and raw materials for rubber chemicals.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4368578A JPS54135747A (en) | 1978-04-13 | 1978-04-13 | Preparation of cyclohexylmercaptan |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4368578A JPS54135747A (en) | 1978-04-13 | 1978-04-13 | Preparation of cyclohexylmercaptan |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS54135747A true JPS54135747A (en) | 1979-10-22 |
Family
ID=12670690
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP4368578A Pending JPS54135747A (en) | 1978-04-13 | 1978-04-13 | Preparation of cyclohexylmercaptan |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS54135747A (en) |
-
1978
- 1978-04-13 JP JP4368578A patent/JPS54135747A/en active Pending
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