JPH11139834A - Reduced pressure defoaming device for molten glass - Google Patents

Reduced pressure defoaming device for molten glass

Info

Publication number
JPH11139834A
JPH11139834A JP30532697A JP30532697A JPH11139834A JP H11139834 A JPH11139834 A JP H11139834A JP 30532697 A JP30532697 A JP 30532697A JP 30532697 A JP30532697 A JP 30532697A JP H11139834 A JPH11139834 A JP H11139834A
Authority
JP
Japan
Prior art keywords
molten glass
vacuum degassing
riser
downcomer
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP30532697A
Other languages
Japanese (ja)
Other versions
JP3817868B2 (en
Inventor
Yusuke Takei
祐輔 竹居
Shun Kijima
駿 木島
Junji Tanigaki
淳史 谷垣
Shoji Imamaki
捷治 今牧
Masataka Matsuwaki
正隆 松脇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AGC Inc
Original Assignee
Asahi Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd
Priority to JP30532697A priority Critical patent/JP3817868B2/en
Priority to US09/164,356 priority patent/US6119484A/en
Priority to KR1019980041667A priority patent/KR100682778B1/en
Priority to TW087116447A priority patent/TW498058B/en
Priority to IDP981327A priority patent/ID20649A/en
Priority to DE69823560T priority patent/DE69823560T2/en
Priority to EP00122258A priority patent/EP1078891B1/en
Priority to EP04007832A priority patent/EP1439148A3/en
Priority to EP98118842A priority patent/EP0908417B2/en
Priority to DE69807812T priority patent/DE69807812T3/en
Publication of JPH11139834A publication Critical patent/JPH11139834A/en
Priority to US09/473,680 priority patent/US6405564B1/en
Priority to KR1020060029382A priority patent/KR100682779B1/en
Application granted granted Critical
Publication of JP3817868B2 publication Critical patent/JP3817868B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B5/00Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
    • C03B5/16Special features of the melting process; Auxiliary means specially adapted for glass-melting furnaces
    • C03B5/225Refining
    • C03B5/2252Refining under reduced pressure, e.g. with vacuum refiners

Abstract

PROBLEM TO BE SOLVED: To enable the drastic reduction of a cost, the increase in the capacity of the device, the elevation of a reduced pressure defoaming temp., etc., while ensuring a sufficient durability by forming a reduced pressure defoaming vessel of a molten glass and a riser and downcomer communicating therewith of electorforming bricks and forming the extension pipes of the riser and the downcomer of platinum or platinum alloys. SOLUTION: The reduced pressure defoaming device 10 continuously executes the reduced pressure defoaming treatment of the molten glass G in a melting vessel 20 and supplies the glass to a molding stage. The reduced pressure defoaming vessel 14 disposed in a reduced pressure housing 12 and the riser 16 and downcomer 18 for introducing and leading out the molten glass G into and out of the reduced pressure defoaming vessel 14 are formed of the electroforming bricks in at least the parts thereof in direct contact with the molten glass. The extension pipes 26, 28 which are disposed in communication with the bottom ends of the riser 16 and the downcomer 18 and are immersed into the molten glass are formed of the platinum or platinum alloys. The top ends of the extension pipes 26, 28 are flanged and the flanges are held and fixed by inserting the flanges into the joints of the electroforming bricks forming the riser 16 and the downcomer 18.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、連続的に供給され
る溶融ガラスから気泡を除去する、溶融ガラスの減圧脱
泡装置の技術分野に属する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention belongs to the technical field of a vacuum degassing apparatus for molten glass for removing air bubbles from a continuously supplied molten glass.

【0002】[0002]

【従来の技術】従来より、成形されたガラス製品の品質
を向上させるために、溶融炉で溶融した溶融ガラスを成
形装置で成形する前に溶融ガラス内に発生した気泡を除
去する減圧脱泡装置が用いられている。このような従来
の減圧脱泡装置を図3に示す。図3に示す減圧脱泡装置
100は、溶解槽112中の溶融ガラスGを減圧脱泡処
理して、次の処理槽に連続的に供給するプロセスに用い
られるものであって、真空吸引されている。減圧ハウジ
ング102内に水平に減圧脱泡槽104が収納配置さ
れ、その両端に垂直に取り付けられる上昇管106およ
び下降管108が収納配置されている。
2. Description of the Related Art Conventionally, in order to improve the quality of molded glass products, a vacuum degassing apparatus for removing air bubbles generated in a molten glass before molding the molten glass in a melting furnace by a molding apparatus. Is used. FIG. 3 shows such a conventional vacuum degassing apparatus. The vacuum degassing apparatus 100 shown in FIG. 3 is used for a process in which the molten glass G in the melting tank 112 is degassed under reduced pressure and is continuously supplied to the next processing tank. I have. A decompression degassing tank 104 is horizontally accommodated in a decompression housing 102, and an ascending pipe 106 and a descending pipe 108 vertically attached to both ends thereof are accommodated and arranged.

【0003】上昇管106は減圧脱泡槽104に連通
し、脱泡処理前の溶融ガラスGを溶解槽112から上昇
させて減圧脱泡槽104に導入する。下降管108は、
減圧脱泡槽104に連通し、脱泡処理後の溶融ガラスG
を減圧脱泡槽104から下降させて次の処理槽(図示せ
ず)に導出する。そして、減圧ハウジング102内にお
いて、減圧脱泡槽104、上昇管106および下降管1
08の周囲には、これらを断熱被覆する断熱用レンガな
どの断熱材110が配設されている。なお、減圧ハウジ
ング102は、金属製、例えばステンレス製であり、外
部から真空ポンプ(図示せず)等によって真空吸引さ
れ、内部が減圧され、内設される減圧脱泡槽104内を
所定の減圧、例えば1/20〜1/3気圧の減圧状態に
維持する。
The rising pipe 106 communicates with the vacuum degassing tank 104, and the molten glass G before defoaming is lifted from the melting tank 112 and introduced into the vacuum degassing tank 104. The downcomer 108 is
The molten glass G after the defoaming process is communicated with the vacuum degassing tank 104.
Is lowered from the vacuum degassing tank 104 and led out to the next processing tank (not shown). Then, in the decompression housing 102, the decompression degassing tank 104, the rising pipe 106 and the downcomer 1
Around the area 08, a heat insulating material 110 such as a heat insulating brick that covers the heat insulating material is provided. The decompression housing 102 is made of metal, for example, stainless steel, and is vacuum-sucked from the outside by a vacuum pump (not shown) or the like to decompress the inside, and a predetermined decompression inside the decompression degassing tank 104 provided therein. For example, the pressure is maintained at 1/20 to 1/3 atm.

【0004】従来の減圧脱泡装置100においては、高
温、例えば1200〜1400℃の温度の溶融ガラスG
を処理するように構成されているので、本出願人の出願
に係る特開平2−221129号公報に開示しているよ
うに、減圧脱泡槽104、上昇管106および下降管1
08などのように溶融ガラスGと直接接触する部分は、
通常白金または白金ロジウムのような白金合金などの貴
金属製円管で構成されている。ここで、これらを白金合
金などの貴金属製円管で構成するのは、溶融ガラスGが
高温であるばかりでなく、貴金属が溶融ガラスとの高温
反応性が低く、溶融ガラスとの反応による不均質化を生
じさせることがなく、高温での強度がある程度確保でき
るからである。特に、減圧脱泡槽104を貴金属製円管
で構成するのは、上記理由に加え、貴金属製円管自体に
電流を流して自己発熱させ、円筒内の溶融ガラスGを均
一に加熱し、溶融ガラスGの温度を所定の温度に保持す
るためである。
In the conventional vacuum degassing apparatus 100, the molten glass G at a high temperature, for example, at a temperature of 1200 to 1400 ° C.
Therefore, as disclosed in Japanese Unexamined Patent Application Publication No. 2-221129 filed by the present applicant, the vacuum degassing tank 104, the riser 106 and the downcomer 1
08, etc., the part which is in direct contact with the molten glass G,
Usually, it is formed of a circular pipe made of a noble metal such as platinum or a platinum alloy such as platinum rhodium. Here, these are made of a circular tube made of a noble metal such as a platinum alloy because not only the molten glass G has a high temperature, but also the noble metal has a low high-temperature reactivity with the molten glass, and is heterogeneous due to the reaction with the molten glass. This is because the formation at a high temperature can be ensured to a certain degree without causing the formation of a layer. In particular, in addition to the above-mentioned reason, the vacuum degassing tank 104 is composed of a precious metal circular tube. In addition to the above-mentioned reason, an electric current is applied to the precious metal circular tube itself to cause self-heating, and the molten glass G in the cylinder is uniformly heated and melted. This is for maintaining the temperature of the glass G at a predetermined temperature.

【0005】ところで、減圧脱泡槽104を貴金属で構
成すると、高温強度の点から円管とするのがよいが、白
金などの貴金属は高価であるため、肉厚を大きくできな
いため、コストおよび強度の両方の点から円管の直径に
は限界があり、あまり大きくできず、減圧脱泡槽104
で脱泡処理できる溶融ガラスGの流量にも限界があり、
大流量の減圧脱泡装置を構築できないという問題があっ
た。もちろん、円管状減圧脱泡槽104の全長を長くし
て流速を速くすることにより、脱泡処理量を増加させる
ことも考えられるが、処理量に比して、また溶解槽や成
形処理槽などに比べて、装置が長大化してしまうという
問題もあった。このため、減圧脱泡装置100における
溶融ガラスGの脱泡処理量(流量)を大きくできないと
いう問題もあった。
When the vacuum degassing tank 104 is made of a noble metal, it is preferable to use a circular tube from the viewpoint of high-temperature strength. However, since a noble metal such as platinum is expensive, its thickness cannot be increased, so that cost and strength are reduced. From both points, the diameter of the circular pipe is limited and cannot be so large,
There is also a limit on the flow rate of the molten glass G that can be defoamed by
There was a problem that a vacuum degassing apparatus with a large flow rate could not be constructed. Of course, it is conceivable to increase the total length of the cylindrical vacuum degassing tank 104 to increase the flow rate, thereby increasing the amount of degassing treatment. There is also a problem that the device becomes longer than in the case of the above. For this reason, there is also a problem that the degassing processing amount (flow rate) of the molten glass G in the vacuum degassing apparatus 100 cannot be increased.

【0006】なお、溶融ガラスGは、粉体原料を溶解反
応させることによって得られるので、溶解の点では、溶
解槽112の温度は高い方が好ましく、また、減圧脱泡
の点では溶融ガラスの粘度は低く、従って温度は高い方
が好ましい。しかしながら、高温強度の点から減圧脱泡
槽104などに貴金属合金を用いる必要がある一方で、
貴金属は高価なものであり、コストの点から円管の厚み
をあまり厚くできないため、白金などの貴金属を用いる
と、減圧脱泡装置100の入口での溶融ガラスGの温度
は、上述した所定温度(1200〜1400℃)に制限
されてしまっていた。
Since the molten glass G is obtained by melting and reacting the powdery raw material, it is preferable that the temperature of the melting tank 112 be higher in terms of melting, and that the molten glass G be reduced in terms of degassing under reduced pressure. It is preferred that the viscosity be low and therefore the temperature be high. However, while it is necessary to use a noble metal alloy in the vacuum degassing tank 104 and the like from the viewpoint of high temperature strength,
Since the noble metal is expensive and the thickness of the circular tube cannot be increased so much from the viewpoint of cost, if a noble metal such as platinum is used, the temperature of the molten glass G at the inlet of the vacuum degassing apparatus 100 becomes the above-mentioned predetermined temperature. (1200-1400 ° C.).

【0007】[0007]

【発明が解決しようとする課題】ところで、このような
問題に対し、減圧脱泡槽104、上昇管106および下
降管108を貴金属合金よりも安価な耐火物レンガで構
成し、貴金属合金の場合と同様に溶融ガラスを連続的に
減圧脱泡処理することができれば、白金などの貴金属合
金を用いる場合に比べて、コストの点から使用量を制限
したり、それに伴う強度低下の点から大きさを制限した
りする必要性はなくなり、装置設計の自由度が飛躍的に
向上することから、大流量の減圧脱泡装置の構築が可能
になるとともに、より高温での減圧脱泡処理も可能にな
るものと考えられる。
In order to solve such a problem, the vacuum degassing tank 104, the riser tube 106 and the downcomer tube 108 are made of refractory bricks which are less expensive than noble metal alloys. Similarly, if the molten glass can be continuously degassed under reduced pressure, compared to the case of using a noble metal alloy such as platinum, the amount used can be limited from the viewpoint of cost, and the size can be reduced from the viewpoint of reduced strength. The need for restriction is eliminated, and the degree of freedom in equipment design is dramatically improved, so that it is possible to construct a vacuum degassing apparatus with a large flow rate and also to perform vacuum degassing processing at higher temperatures. It is considered something.

【0008】しかしながら、減圧脱泡装置100のすべ
ての構成部分を耐火物レンガで作製しようとすると、以
下のような問題がある。すなわち、上昇管106や下降
管108の下端部分などの管状の開放端においては、下
端を支持するものが無いため、高重量の耐火物レンガを
目地材の接着力のみで支持することとなってしまい、十
分な強度が得られないし、その代わりに、長い円筒型の
耐火物レンガを製造しようとしても、コストが非常に高
くなる。このため、上昇管106や下降管108の下端
部分を耐火物レンガで作製するのは現実的には困難であ
るという問題がある。
However, if all components of the vacuum degassing apparatus 100 are to be made of refractory bricks, there are the following problems. In other words, at the tubular open end such as the lower end portion of the riser pipe 106 or the downcomer pipe 108, there is no support for the lower end, so that a heavy refractory brick is supported only by the adhesive force of the joint material. As a result, sufficient strength cannot be obtained, and instead, the cost becomes extremely high even if an attempt is made to produce a long cylindrical refractory brick. For this reason, there is a problem that it is practically difficult to make the lower end portions of the riser pipe 106 and the descender pipe 108 from refractory bricks.

【0009】また、このようにして上昇管106や下降
管108の下端を耐火物レンガで作製したとしても、目
地の部分で損傷や劣化が起こりやすいし、目地以外の部
分であっても、溶解槽112における溶融ガラスGと大
気との界面近傍の位置では、高温で、かつ、大気が存在
することから、耐火物が反応性に富み、選択的に劣化し
やすいという問題がある。このように目地部分や界面部
分が劣化していくと、上昇管106や下降管108の下
端部分が高さ方向に不均一な形状となり、割れなどの破
損を生じたり、最悪の場合、上昇管106や下降管10
8の下端部分の一部が破断して落下してしまうおそれが
あり、十分な耐久性が得られないという問題がある。さ
らに、破損した耐火物が溶融ガラスGに混入すれば、ガ
ラスの組成の均一性を保持できなくなるおそれもあると
いう問題もある。
Even if the lower ends of the riser pipes 106 and the downcomer pipes 108 are made of refractory bricks in this way, damage and deterioration are apt to occur at joints. At a position near the interface between the molten glass G and the atmosphere in the tank 112, since the temperature is high and the atmosphere is present, there is a problem that the refractory is rich in reactivity and easily deteriorates selectively. When the joints and the interface deteriorate as described above, the lower ends of the riser 106 and the downcomer 108 have an uneven shape in the height direction, causing breakage such as cracks, and in the worst case, the riser 106 and downcomer 10
There is a possibility that a part of the lower end portion of 8 may be broken and fall, and there is a problem that sufficient durability cannot be obtained. Further, if the broken refractory is mixed into the molten glass G, there is a problem that the uniformity of the glass composition may not be maintained.

【0010】本発明の目的は、前記従来技術の問題点を
解決することにあり、連続的に供給される溶融ガラスか
ら気泡を除去する、溶融ガラスの減圧脱泡装置におい
て、高温の溶融ガラスに対して十分な耐久性を確保しつ
つ、コストを大幅に低減でき、ひいては装置の大容量
化、減圧脱泡処理温度の高温化などを図ることができる
溶融ガラスの減圧脱泡装置を提供することにある。
SUMMARY OF THE INVENTION An object of the present invention is to solve the above-mentioned problems of the prior art. In a vacuum degassing apparatus for molten glass, which removes air bubbles from a continuously supplied molten glass, a high-temperature molten glass is used. To provide a vacuum degassing apparatus for molten glass that can significantly reduce costs while ensuring sufficient durability, and can increase the capacity of the apparatus and increase the temperature of the vacuum degassing process. It is in.

【0011】[0011]

【課題を解決するための手段】前記目的を達成するため
に、本発明は、真空吸引される減圧ハウジングと、この
減圧ハウジング内に設けられ、溶融ガラスの減圧脱泡を
行う減圧脱泡槽と、この減圧脱泡槽に連通して設けら
れ、前記減圧脱泡前の溶融ガラスを上昇させて前記減圧
脱泡槽に導入する上昇管と、前記減圧脱泡槽に連通して
設けられ、前記減圧脱泡後の溶融ガラスを前記減圧脱泡
槽から下降させて導出する下降管と、前記上昇管および
下降管の下端にそれぞれ連通して設けられる延長管とを
有し、前記上昇管、前記減圧脱泡槽および前記下降管
は、少なくとも前記溶融ガラスと直接接触する部分が電
鋳レンガで形成され、前記延長管は、白金または白金合
金で形成されたことを特徴とする溶融ガラスの減圧脱泡
装置を提供する。
SUMMARY OF THE INVENTION In order to achieve the above object, the present invention provides a decompression housing for vacuum suction, and a decompression tank for defoaming molten glass provided in the decompression housing. A rising pipe that is provided in communication with the vacuum degassing tank, raises the molten glass before the vacuum degassing and introduces the molten glass into the vacuum degassing tank, and is provided in communication with the vacuum degassing tank. The molten glass after the decompression and degassing has a downcomer pipe that descends from the decompression degassing tank and is extended therefrom, and an extension pipe provided in communication with lower ends of the riser pipe and the downcomer pipe, respectively. At least a portion of the vacuum degassing tank and the downcomer which is in direct contact with the molten glass is formed of electroformed brick, and the extension tube is formed of platinum or a platinum alloy. Provide a foaming device.

【0012】また、前記延長管は、その上端にフランジ
が形成され、このフランジが前記上昇管もしくは前記下
降管を形成する前記電鋳レンガの目地に挿入されて挟持
されることにより、前記上昇管もしくは前記下降管に固
定されたものであるのが好ましい。
Further, the extension pipe has a flange formed at an upper end thereof, and the flange is inserted into a joint of the electroformed brick forming the riser pipe or the downcomer pipe so as to be clamped, thereby forming the riser pipe. Alternatively, it is preferably fixed to the downcomer tube.

【0013】[0013]

【発明の実施の形態】以下、本発明の溶融ガラスの減圧
脱泡装置について、添付の図面に示される好適実施例を
もとに詳細に説明する。
BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, a vacuum degassing apparatus for molten glass of the present invention will be described in detail based on a preferred embodiment shown in the accompanying drawings.

【0014】図1に、本発明の溶融ガラスの減圧脱泡装
置の概略断面図を示す。図1に示すように、減圧脱泡装
置10は、溶解槽20内の溶融ガラスGを減圧脱泡処理
して、図示しない次の処理槽、例えば、フロートバスな
どの板状の成形処理槽や瓶などの成形作業槽などに連続
的に供給するプロセスに用いられるもので、基本的に、
減圧ハウジング12、減圧脱泡槽14、上昇管16、下
降管18および延長管26,28を有する。減圧ハウジ
ング12は、減圧脱泡槽14の気密性を確保するための
ものであり、略門型に形成される。この減圧ハウジング
12は、減圧脱泡槽14に必要とされる気密性および強
度を有するものであれば、その材質、構造は特に限定さ
れるものではないが、金属製、特にステンレス製とする
のが好ましい。このような減圧ハウジング12は、外部
から真空ポンプ(図示せず)等によって真空吸引され、
内部が減圧され、内設される減圧脱泡槽14内を所定の
減圧、例えば1/20〜1/3気圧の減圧状態に維持す
るように構成される。
FIG. 1 is a schematic sectional view of a vacuum degassing apparatus for molten glass according to the present invention. As shown in FIG. 1, the vacuum degassing apparatus 10 performs a degassing process on the molten glass G in the melting tank 20 under reduced pressure, and a next processing tank not shown, for example, a plate-shaped forming processing tank such as a float bath, It is used for the process of continuously supplying to a molding work tank such as a bottle. Basically,
It has a decompression housing 12, a decompression degassing tank 14, an ascending pipe 16, a descending pipe 18, and extension pipes 26 and 28. The decompression housing 12 is for ensuring the airtightness of the decompression degassing tank 14, and is formed in a substantially portal shape. The material and structure of the decompression housing 12 are not particularly limited as long as it has the airtightness and strength required for the decompression and degassing tank 14. Is preferred. Such a decompression housing 12 is vacuum-sucked from the outside by a vacuum pump (not shown) or the like,
The inside is depressurized, and the inside of the decompression degassing tank 14 provided therein is maintained at a predetermined reduced pressure, for example, a reduced pressure of 1/20 to 1/3 atm.

【0015】減圧ハウジング12の上部内には減圧脱泡
槽14が設けられる。また、減圧脱泡槽14の左端部に
は上昇管16が連通され、減圧脱泡槽14の右端部には
下降管18が連通される。なお、上昇管16および下降
管18はそれぞれ減圧ハウジング12の脚部12a,1
2b(以下、それぞれハウジング脚部12a,12bと
する)内に配設されている。
A vacuum degassing tank 14 is provided in the upper part of the pressure reducing housing 12. A rising pipe 16 communicates with the left end of the vacuum degassing tank 14, and a downcomer pipe 18 communicates with the right end of the vacuum degassing tank 14. The riser pipe 16 and the lowering pipe 18 are respectively connected to the legs 12a, 1
2b (hereinafter, referred to as housing legs 12a and 12b, respectively).

【0016】本発明の減圧脱泡装置10においては、減
圧脱泡槽14、上昇管16および下降管18がいずれも
電鋳レンガ30で形成される。すなわち、減圧脱泡装置
10における溶融ガラスGと直接接触する主要部分を電
鋳レンガ30で形成することにより、従来から用いられ
てきた白金合金製のものよりも、コストが大幅に低減
し、従って自由な形状で、かつ、自由な厚さに設計する
ことが可能となることから、減圧脱泡装置10の大容量
化が実現するとともに、より高温での減圧脱泡処理も行
えるようになる。また、電鋳レンガであれば、一般のレ
ンガと比べ高温での耐久性に優れ、成分の溶出も最小限
にすることができることから、溶融ガラスの均一性を保
つことができる。
In the vacuum degassing apparatus 10 of the present invention, the vacuum degassing tank 14, the riser pipe 16 and the downcomer pipe 18 are all formed of electroformed bricks 30. In other words, by forming the main part of the vacuum degassing apparatus 10 which is in direct contact with the molten glass G with the electroformed brick 30, the cost is significantly reduced as compared with a conventionally used platinum alloy, and accordingly, Since it is possible to design a free shape and a free thickness, it is possible to increase the capacity of the vacuum degassing apparatus 10 and to perform vacuum degassing at a higher temperature. In addition, electroformed bricks have higher durability at high temperatures than ordinary bricks and can minimize elution of components, so that the uniformity of molten glass can be maintained.

【0017】従って、減圧脱泡槽14、上昇管16およ
び下降管18の形状は少なくとも筒状であれば特に限定
されず、例えば、その断面形状は円状のみならず角状で
あってもよい。電鋳レンガ30を用いて減圧脱泡槽1
4、上昇管16および下降管18を構築する方法は、特
に制限的ではなく、例えば小さい直方体の電鋳レンガ3
0を積み上げ、その間の目地の部分を目地材で埋めて、
所定長の筒状管を形成してもよいし、円筒状もしくは角
筒状に鋳込み成形した筒状の電鋳レンガ30を一列に積
み重ねて、その間の目地の部分を目地材で埋め、所定長
の筒状管を形成してもよい。
Accordingly, the shapes of the vacuum degassing tank 14, the riser pipe 16 and the descender pipe 18 are not particularly limited as long as they are at least cylindrical. For example, the cross-sectional shape may be not only circular but also angular. . Vacuum degassing tank 1 using electroformed brick 30
The method of constructing the riser pipe 16 and the descender pipe 18 is not particularly limited, and for example, a small rectangular electroformed brick 3
Pile up 0, fill the joint part between them with joint material,
A cylindrical tube of a predetermined length may be formed, or cylindrical electroformed bricks 30 cast and formed into a cylindrical or square tube shape are stacked in a line, and the joint portion therebetween is filled with a joint material. May be formed.

【0018】なお、電鋳レンガ30としては、耐火原料
を電気溶融した後、所定形状に鋳込み成形したレンガで
あれば特に限定されず、従来公知の各種の電鋳レンガを
使用すればよい。中でも、耐蝕性が高く、素地からの発
泡も少ない点で、アルミナ系電鋳耐火物、ジルコニア系
電鋳耐火物、AZS(Al2 3 −ZrO2 −Si
2 )系電鋳耐火物等が好適に例示され、具体的には、
マースナイト(MB−G)、ZB−X950、ジルコナ
イト(ZB)(いずれも旭硝子(株)製)等が挙げられ
る。
The electroformed brick 30 is made of a refractory raw material.
After electro-melting, the brick is cast into a predetermined shape
It is not particularly limited as long as there are various conventionally known electroformed bricks.
Just use it. Above all, corrosion resistance is high,
Alumina-based electrocast refractories, zirconia-based
Electroformed refractories, AZS (AlTwoOThree-ZrOTwo-Si
O Two) -Based electroformed refractories and the like are preferably exemplified.
Marsnite (MB-G), ZB-X950, Zircona
(ZB) (all manufactured by Asahi Glass Co., Ltd.) and the like.
You.

【0019】そして、減圧脱泡槽14の周囲には減圧脱
泡槽14を被覆する断熱用のレンガ32(以下、断熱レ
ンガ32とする)が配設され、上昇管16および下降管
18の周囲にもそれぞれを被覆する断熱レンガ32が配
設される。断熱レンガ32としては、公知の種々のレン
ガを使用すればよく、特に限定されない。このように配
設された断熱レンガ32は、その外側が減圧ハウジング
12に覆われることにより減圧ハウジング12内に収容
される。
Around the vacuum degassing tank 14, a brick 32 for heat insulation (hereinafter referred to as an insulating brick 32) for covering the vacuum degassing tank 14 is provided. A heat insulating brick 32 for covering each of them is also provided. Various known bricks may be used as the heat insulating bricks 32, and there is no particular limitation. The heat insulating brick 32 arranged in this manner is accommodated in the decompression housing 12 by covering the outside thereof with the decompression housing 12.

【0020】また、減圧脱泡槽14、上昇管16および
下降管18の周囲には、必要に応じて、断熱レンガ32
とともに、加熱ヒータを設けて加熱可能な構成としても
よいし、冷却水を通過可能にして冷却可能な構成として
もよい。
Insulation bricks 32 may be provided around the vacuum degassing tank 14, the riser pipe 16 and the descender pipe 18 if necessary.
In addition, a configuration may be adopted in which a heater can be provided to enable heating, or a configuration in which cooling water is allowed to pass and cooling is possible.

【0021】ここで、上昇管16の下端部は、上流ピッ
ト22の開放端に嵌入され、上流ピット22内の溶融ガ
ラスGに浸漬される必要がある。また、下降管18の下
端部も同様に、下流ピット24の開放端に嵌入され、下
流ピット24内の溶融ガラスG内に浸漬される必要があ
る。ところで、本発明の減圧脱泡装置10は、上述した
ように、主要部分が電鋳レンガ28で構成されるもので
ある。
Here, the lower end of the riser 16 must be fitted into the open end of the upstream pit 22 and immersed in the molten glass G in the upstream pit 22. Similarly, the lower end of the downcomer pipe 18 needs to be fitted into the open end of the downstream pit 24 and immersed in the molten glass G in the downstream pit 24. By the way, as described above, the main part of the vacuum degassing apparatus 10 of the present invention is constituted by the electroformed brick 28.

【0022】しかしながら、前述したように、上昇管1
6の下端部であって上流ピット22に嵌入させて溶融ガ
ラスGに浸漬する部分までを電鋳レンガ30で作製しよ
うとしても、強度やコストの点から現実的には困難であ
るし、仮に電鋳レンガ30で作製したとしても、目地部
分や界面部分が劣化しやすく、割れなどの破損を生じる
おそれがあり、十分な耐久性が得られないという問題が
ある。また、下降管18の下端部であって、下流ピット
24の開放端に嵌入させて溶融ガラスGに浸漬する部分
を電鋳レンガ30で作製する場合においても、上記同様
の問題がある。
However, as described above, the riser 1
It is practically difficult from the viewpoint of strength and cost to make the lower end of 6 and the portion that is fitted into the upstream pit 22 and immersed in the molten glass G with the electroformed brick 30. Even if it is made of cast brick 30, joint portions and interface portions are liable to be deteriorated, and there is a possibility that damage such as cracks may occur, and there is a problem that sufficient durability cannot be obtained. The same problem as described above also occurs when the lower end of the downcomer 18 is made of the electroformed brick 30 so as to be fitted into the open end of the downstream pit 24 and immersed in the molten glass G.

【0023】これに対し、本発明は、図1に示されるよ
うに、上昇管16および下降管18の下端部に白金また
は白金合金製の延長管26,28を設け、この延長管2
6,28をそれぞれ上流ピット20および下流ピット2
4内に嵌入し、内部の溶融ガラスGに浸漬する構成とし
たものである。このような構成とすることで、電鋳レン
ガ製の上昇管16および下降管18を直接溶融ガラスG
に浸漬する必要がなくなり、上流ピット20および下流
ピット24内における、溶融ガラスGに対する耐久性を
大幅に向上することができ、上記問題を解決することが
できる。
On the other hand, according to the present invention, as shown in FIG. 1, extension pipes 26 and 28 made of platinum or a platinum alloy are provided at the lower ends of the riser pipe 16 and the descender pipe 18, and
6 and 28 to upstream pit 20 and downstream pit 2 respectively
4, and is immersed in the molten glass G inside. With such a configuration, the riser tube 16 and the descender tube 18 made of electroformed brick are directly connected to the molten glass G.
Therefore, it is not necessary to immerse the molten glass G in the upstream pit 20 and the downstream pit 24, so that the durability against the molten glass G can be greatly improved, and the above problem can be solved.

【0024】具体的には、図2に示されるように、上昇
管16の下端部に白金または白金合金製の延長管26が
連通して設けられる。なお、上昇管16側の延長管26
と下降管18側の延長管28は同一に構成されているの
で、上昇管16側の延長管26についてのみ説明し、下
降管18側の延長管28の説明は省略する。
More specifically, as shown in FIG. 2, an extension pipe 26 made of platinum or a platinum alloy is provided at the lower end of the riser pipe 16 so as to communicate therewith. The extension pipe 26 on the riser pipe 16 side
Since the extension pipe 28 on the downcomer 18 side is configured identically, only the extension pipe 26 on the ascending pipe 16 will be described, and the description of the extension pipe 28 on the downcomer 18 will be omitted.

【0025】延長管26は、円筒形状の筒体26aと、
この筒体26aの一端に形成される固定用フランジ26
bと、この固定用フランジ26bから所定間隔離間して
形成されるシール用フランジ26cとを有する管であ
り、白金または白金合金製である。筒体26aの内径
は、上昇管16にスムーズに連通するように、上昇管1
6の内径とおよそ同等の大きさに構成すればよい。
The extension pipe 26 has a cylindrical body 26a,
Fixing flange 26 formed at one end of this cylindrical body 26a
b and a sealing flange 26c formed at a predetermined distance from the fixing flange 26b, and is made of platinum or a platinum alloy. The inner diameter of the cylindrical body 26a is such that the riser tube 1 is smoothly communicated with the riser tube 16.
6 may be configured to be approximately the same size as the inner diameter.

【0026】固定用フランジ26bは、上昇管16を構
成する電鋳レンガ30,30間、すなわち目地に挿入さ
れることにより、その上端が上昇管16に固定されうる
ように形成される。なお、延長管26の上昇管16への
固定は、固定用フランジ26bに限らず、種々の方法に
より行ってもよいが、固定用フランジ26bを用いて固
定する構成とするのが好ましい。すなわち、筒体26a
の上端に固定用フランジ26bを有しない場合には、筒
体26aの外側と電鋳レンガ30との間に溶融ガラスG
が浸入し、断熱レンガ32および断熱材38が浸食さ
れ、ハウジング脚部12aの底面近傍の熱伝導率が上昇
してハウジング外壁面の温度が上がりハウジングが変形
するおそれがあるが、筒体26aの上端に固定用フラン
ジ26bを形成することにより、このような問題も解消
する。これにより、ハウジング脚部12aの温度上昇、
およびこれに伴う下方への歪みを防止し、ハウジング脚
部12a内の電鋳レンガ30や断熱レンガ32の目地の
ずれや緩みに起因する溶融ガラスGの漏れ、ひいてはハ
ウジング脚部12aの過度な温度上昇を防止することが
できる。従って、このような部分的な温度上昇に起因す
る、装置全体の熱応力変形、および溶融ガラスGの漏れ
の増大による加速度的な温度上昇も防止できる。
The fixing flange 26b is formed so that the upper end thereof can be fixed to the riser tube 16 by being inserted between the electroformed bricks 30 constituting the riser tube 16, that is, the joint. The fixing of the extension pipe 26 to the riser pipe 16 is not limited to the fixing flange 26b, and may be performed by various methods. However, it is preferable that the extension pipe 26 be fixed using the fixing flange 26b. That is, the cylindrical body 26a
Is not provided with a fixing flange 26b at the upper end of the molten glass G between the outside of the cylindrical body 26a and the electroformed brick 30.
Penetrates, the heat insulating brick 32 and the heat insulating material 38 are eroded, the thermal conductivity near the bottom surface of the housing leg 12a increases, the temperature of the housing outer wall surface increases, and the housing may be deformed. By forming the fixing flange 26b at the upper end, such a problem is also solved. This increases the temperature of the housing leg 12a,
And the accompanying downward distortion is prevented, and the molten glass G leaks due to displacement or looseness of the joint between the electroformed brick 30 and the insulating brick 32 in the housing leg 12a, and furthermore, the excessive temperature of the housing leg 12a. Ascent can be prevented. Accordingly, it is possible to prevent thermal stress deformation of the entire apparatus due to such a partial temperature rise and accelerated temperature rise due to an increase in leakage of the molten glass G.

【0027】一方、シール用フランジ26cは、延長管
26が下降管18の下端に設けられた際に、後述するシ
ール部材34とともにハウジング脚部12aの下端を外
側から閉塞して、減圧ハウジング12内の気密性を確保
するためのものである。また、このシール用フランジ2
6cを電極として、白金または白金合金製の延長管26
を自己発熱させて適正温度に保持する構成としてもよ
い。なお、ハウジング脚部12aの下端において気密性
を確保するための機構としては、シール用フランジ26
cを用いる方法に限定されず、種々の機構が使用可能で
ある。延長管26の上昇管16への固定は上述のように
固定用フランジ26bに受け持たせるのが好ましいが、
シール用フランジ26cに真空シールと延長管26の自
重を担持する役目を兼用させ、固定用フランジ26bは
電鋳レンガ30aに囲まれた通路内での延長管外面の煉
瓦内面からの遊離を防止する役目に限ってもよく、この
場合は固定用フランジ26bは延長管26の水平方向の
微小な偏芯を防止する役目を担うことになるとともに、
延長管外面と煉瓦内面間に溶融ガラスGが浸入すること
を防ぐ役目も担う。
On the other hand, when the extension pipe 26 is provided at the lower end of the downcomer pipe 18, the sealing flange 26c closes the lower end of the housing leg 12a from the outside together with a sealing member 34 described later, and The purpose is to ensure the airtightness. In addition, this sealing flange 2
6c as an electrode, an extension tube 26 made of platinum or a platinum alloy
May be configured to generate heat by itself and maintain an appropriate temperature. A mechanism for ensuring airtightness at the lower end of the housing leg 12a includes a sealing flange 26.
Not limited to the method using c, various mechanisms can be used. It is preferable that the extension pipe 26 is fixed to the riser pipe 16 by the fixing flange 26b as described above.
The sealing flange 26c also serves to carry the vacuum seal and the weight of the extension tube 26, and the fixing flange 26b prevents the outer surface of the extension tube from separating from the inner surface of the brick in the passage surrounded by the electroformed brick 30a. It may be limited to the role, and in this case, the fixing flange 26b plays a role of preventing the horizontal eccentricity of the extension pipe 26 from being slightly eccentric.
It also serves to prevent molten glass G from entering between the outer surface of the extension tube and the inner surface of the brick.

【0028】このような延長管26,28に用いる白金
または白金合金としては、その組成は特に限定されるも
のではないが、白金を70wt%〜98wt%含有し、
Rhを2wt%以上含有する白金合金であるのが、高温
強度が特に優れる点で好ましい。
The composition of the platinum or platinum alloy used for the extension tubes 26 and 28 is not particularly limited, but contains platinum in an amount of 70 wt% to 98 wt%.
A platinum alloy containing 2 wt% or more of Rh is preferable because the high-temperature strength is particularly excellent.

【0029】このように構成された延長管26は、固定
用フランジ26bが上昇管16の下端近傍の電鋳レンガ
30の間の目地部分に挿入されて挟持されるとともに、
シール用フランジ26cと減圧ハウジング12との間
に、シール部材34が配設され、ハウジング脚部12a
下端における気密性が確保される。なお、シール部材3
4としては、気密性および耐熱性を有するものであれば
特に限定されず、ハウジング12の内部も高々1/20
気圧に減圧すればよいので、真空装置に用いられる通常
の真空シール材料の中から耐熱性のものを選択すればよ
い。
In the extension pipe 26 thus configured, the fixing flange 26b is inserted into the joint between the electroformed bricks 30 near the lower end of the riser pipe 16, and is clamped.
A sealing member 34 is disposed between the sealing flange 26c and the decompression housing 12, and the housing leg 12a
Airtightness at the lower end is ensured. In addition, the sealing member 3
4 is not particularly limited as long as it has airtightness and heat resistance.
Since the pressure may be reduced to the atmospheric pressure, a heat-resistant material may be selected from ordinary vacuum sealing materials used for a vacuum device.

【0030】ところで、上述のように延長管26は固定
用フランジ26bが電鋳レンガ30の目地に挟持される
が、この際の挟持力は、電鋳レンガ30の自重により確
保されることとなる。従って、固定用フランジ26b上
に積載される電鋳レンガ30が少ない場合には、溶融ガ
ラスGによる膨張および収縮に伴って目地が開いて挟持
力が低下し、固定用フランジ26bを十分に挟持するこ
とができず、溶融ガラスGが漏れ出すおそれがある。こ
のため、延長管26の上方には、図2に示されるよう
に、補強部材36を設け、固定用フランジ26bの電鋳
レンガ30による挟持力を補強する構成としてもよい。
なお、補強部材36としては、固定用フランジ26bの
上方の電鋳レンガ30を下方に押圧することができるも
のであればよく、その材質および構造は特に限定される
ものではない。例えば、固定用フランジ26b上に電鋳
レンガ30が高く積載されている場合には、補強部材3
6を有しなくてもその自重により固定用フランジ26b
を強固に挟持することができる。
By the way, as described above, the fixing flange 26b of the extension tube 26 is sandwiched between the joints of the electroformed bricks 30, and the clamping force at this time is secured by the own weight of the electroformed bricks 30. . Therefore, when the number of the electroformed bricks 30 loaded on the fixing flange 26b is small, the joint is opened due to the expansion and contraction by the molten glass G, and the holding force is reduced, and the fixing flange 26b is sufficiently held. And the molten glass G may leak out. For this reason, as shown in FIG. 2, a reinforcing member 36 may be provided above the extension pipe 26 to reinforce the clamping force of the fixing flange 26b by the electroformed brick 30.
The reinforcing member 36 may be any material that can press the electroformed brick 30 above the fixing flange 26b downward, and the material and structure thereof are not particularly limited. For example, when the electroformed brick 30 is stacked high on the fixing flange 26b, the reinforcing member 3
6 does not have the fixing flange 26b due to its own weight.
Can be firmly held.

【0031】また、図2に示されるように、ハウジング
脚部12a内の最下端に設けられた電鋳レンガ30a
は、延長管26に面した内側部分であって、ハウジング
脚部12aの底面に面した下側隅部分が円周に沿って切
り欠かれて形成され、この切欠部に断熱材38が配設さ
れるのが好ましい。すなわち、ハウジング脚部12aの
底面のうち、延長管26の周囲近傍は最も加熱されやす
いことから、過度に温度上昇して、歪みや変形を生じ、
目地からの溶融ガラスGの断熱レンガ層32への漏れを
誘発するおそれがある。このため、延長管26の近傍に
断熱材38を配設することにより、このハウジング脚部
12a底面の過度な温度上昇を防止し、この部分におけ
る耐久性をさらに向上させることができる。また、電鋳
レンガ30aの下側部分にのみ断熱材38を配設する構
成であるので、電鋳レンガ30aの上側部分において十
分な強度を確保し、固定用フランジ26bを強固に挟持
することができる。なお、断熱材38としては、電鋳レ
ンガ30よりも断熱性が高い材料であれば特に限定され
ない。
As shown in FIG. 2, an electroformed brick 30a provided at the lowermost end in the housing leg 12a.
Is formed by cutting out an inner portion facing the extension tube 26 and a lower corner portion facing the bottom surface of the housing leg 12a along a circumference, and a heat insulating material 38 is provided in the cutout portion. Preferably. That is, since the vicinity of the extension tube 26 on the bottom surface of the housing leg portion 12a is most easily heated, the temperature rises excessively, causing distortion and deformation,
Leakage of the molten glass G from the joint to the insulating brick layer 32 may be induced. Therefore, by disposing the heat insulating material 38 near the extension pipe 26, an excessive rise in temperature of the bottom surface of the housing leg 12a can be prevented, and the durability in this portion can be further improved. Further, since the heat insulating material 38 is provided only on the lower portion of the electroformed brick 30a, it is possible to secure sufficient strength in the upper portion of the electroformed brick 30a and firmly clamp the fixing flange 26b. it can. The heat insulating material 38 is not particularly limited as long as the material has higher heat insulating properties than the electroformed brick 30.

【0032】このようにして、上昇管16の下端部であ
って上流ピット22内の溶融ガラスGに浸漬する部分
や、下降管18の下端部であって下流ピット24内の溶
融ガラスGに浸漬する部分を白金または白金合金で形成
することにより、上昇管16の下端部および下降管18
の下端部の劣化や破損を防止し、溶融ガラスGに対して
十分な耐久性を確保できる。
In this way, the lower end of the riser pipe 16 and the portion immersed in the molten glass G in the upstream pit 22 and the lower end of the downcomer pipe 18 immersed in the molten glass G in the downstream pit 24 The lower portion of the riser 16 and the lowerer 18 are formed by forming the portion to be made of platinum or a platinum alloy.
The lower end of the glass can be prevented from being deteriorated or damaged, and sufficient durability can be ensured for the molten glass G.

【0033】ところで、ハウジング脚部12aには、緩
衝機構40を設け、電鋳レンガ30や断熱レンガ32の
上下方向への熱膨張および収縮に応じて伸縮可能な構成
とするのが好ましい。こうすることにより、上昇管16
を構成する電鋳レンガ30や、その周辺の断熱レンガ3
2が熱膨張した場合には、緩衝機構40に上昇管16の
熱膨張を吸収させることができる一方、これらのレンガ
が収縮した場合には、その収縮に追随させるようにハウ
ジング脚部12aを収縮させ、収縮に起因する目地の開
きを防止して溶融ガラスGの漏れを有効に防ぐことがで
きる。従って、減圧ハウジング12の破損や、これに伴
う減圧度の低下を防止し、装置の耐久性および安全性の
向上が図れる。
Incidentally, it is preferable that a buffer mechanism 40 is provided on the housing leg portion 12a so as to be able to expand and contract according to the thermal expansion and contraction of the electroformed brick 30 and the heat insulating brick 32 in the vertical direction. By doing so, the riser 16
Bricks 30 and the surrounding insulating bricks 3
When the thermal expansion of the bricks 2 occurs, the buffer mechanism 40 can absorb the thermal expansion of the riser tube 16. On the other hand, when these bricks contract, the housing legs 12a are contracted so as to follow the contraction. This can prevent the joint from opening due to shrinkage and effectively prevent the molten glass G from leaking. Therefore, damage to the decompression housing 12 and a decrease in the degree of decompression caused by the damage can be prevented, and the durability and safety of the device can be improved.

【0034】具体的には、図2に示すように、緩衝機構
40は、筒状ベローズ42と、押し上げ手段44とを有
する。筒状ベローズ42は、ハウジング脚部12aが水
平方向に切断分離され、この一旦分離されたハウジング
脚部12aの上側の部分(以下、上側部13aとする)
と、下側の部分(以下、下側部13bとする)とを気密
かつ伸縮可能に連結するための部材である。筒状ベロー
ズ42の材質は特に限定されるものではないが、減圧ハ
ウジング12と同様に金属製、特にステンレス製とする
のが好ましい。
Specifically, as shown in FIG. 2, the buffer mechanism 40 has a cylindrical bellows 42 and push-up means 44. The tubular bellows 42 has the housing legs 12a cut and separated in the horizontal direction, and the upper portion of the once separated housing legs 12a (hereinafter referred to as the upper portion 13a).
And a lower portion (hereinafter, referred to as a lower portion 13b) in a gas-tight and expandable manner. The material of the cylindrical bellows 42 is not particularly limited, but is preferably made of metal, particularly stainless steel, as in the case of the decompression housing 12.

【0035】押し上げ手段44は、ハウジング脚部12
aの下側部13bを上方に付勢できるものであれば特に
限定されず、種々の機構が採用可能である。例えば、図
2に示すように、上側部13aと下側部13bとに、互
いに対をなして固定される2個の連結部材46,48
と、下端が下側の連結部材48に固定され、上側の連結
部材46の通過孔を挿通するように設けられる棒材50
と、両連結部材46,48間を連結し、下側部13bを
上方に付勢する付勢部材52とから構成すればよい。な
お、付勢部材52としては、特に限定されないが、コイ
ルばねが好ましく例示される。このように構成すること
により、電鋳レンガ30や断熱レンガ32の熱膨張を付
勢部材52の付勢力に抗して下方に逃がすことができ、
熱膨張に起因する装置の歪みや損傷を防止し、装置の安
全性を高めることができる。また、電鋳レンガ30や断
熱レンガ32が収縮しても、下側部13bを追随させ
て、目地の開きを防止することもできる。なお、このよ
うな押し上げ手段44は、一本の筒状ベローズ42に対
して複数箇所設ける構成とするのが好ましい。また、ハ
ウジング脚部12aの下端部分は、リブ等で補強する構
成としてもよい。
The push-up means 44 is connected to the housing leg 12.
The mechanism is not particularly limited as long as it can urge the lower portion 13b upward, and various mechanisms can be adopted. For example, as shown in FIG. 2, two connecting members 46 and 48 fixed to the upper part 13a and the lower part 13b in pairs with each other.
And a bar 50 whose lower end is fixed to the lower connecting member 48 and is provided so as to pass through the through hole of the upper connecting member 46.
And an urging member 52 that connects the two connecting members 46 and 48 and urges the lower portion 13b upward. The urging member 52 is not particularly limited, but is preferably a coil spring. With this configuration, the thermal expansion of the electroformed brick 30 and the insulating brick 32 can be released downward against the urging force of the urging member 52,
Distortion and damage of the device caused by thermal expansion can be prevented, and the safety of the device can be enhanced. Further, even if the electroformed brick 30 or the heat insulating brick 32 shrinks, the opening of the joint can be prevented by following the lower portion 13b. It is preferable that a plurality of such push-up means 44 be provided for one tubular bellows 42. Further, the lower end of the housing leg 12a may be reinforced with a rib or the like.

【0036】このような本発明の減圧脱泡装置10で溶
融ガラスGを脱泡処理して次の処理炉に連続的に供給す
るプロセス例を以下に示す。まず、図示しない真空ポン
プで減圧ハウジング12内および減圧脱泡槽14内を真
空吸引状態に維持する。この状態で、溶解槽20で溶融
されたガラスGは上流ピット22を通って延長管26お
よび上昇管16を介して上昇して減圧脱泡槽14内に導
かれ、溶融ガラスGは減圧脱泡槽14内で減圧条件下に
おいて脱泡処理される。そして、脱泡処理された溶融ガ
ラスGは下降管18および延長管28を介して下流ピッ
ト24に導かれる。
An example of a process in which the molten glass G is degassed by the vacuum degassing apparatus 10 of the present invention and is continuously supplied to the next processing furnace will be described below. First, the inside of the vacuum housing 12 and the vacuum degassing tank 14 are maintained in a vacuum suction state by a vacuum pump (not shown). In this state, the glass G melted in the melting tank 20 rises through the upstream pit 22 through the extension pipe 26 and the riser pipe 16 and is guided into the vacuum degassing tank 14, where the molten glass G is degassed under reduced pressure. A defoaming treatment is performed in the tank 14 under reduced pressure conditions. Then, the defoamed molten glass G is guided to the downstream pit 24 via the downcomer pipe 18 and the extension pipe 28.

【0037】以上、本発明の溶融ガラスの減圧脱泡装置
について詳細に説明したが、本発明は上記実施例に限定
されず、本発明の要旨を逸脱しない範囲において、各種
の改良および変更を行ってもよいのはもちろんである。
Although the vacuum degassing apparatus for molten glass of the present invention has been described in detail above, the present invention is not limited to the above-described embodiment, and various improvements and modifications can be made without departing from the spirit of the present invention. Of course, you may.

【0038】[0038]

【発明の効果】以上、詳細に説明したように、本発明に
よれば、連続的に供給される溶融ガラスから気泡を除去
する、溶融ガラスの減圧脱泡装置において、高温の溶融
ガラスに対して十分な耐久性を確保しつつ、コストを大
幅に低減でき、ひいては装置の大容量化、減圧脱泡処理
温度の高温化などを図ることが可能である。従って、大
流量の溶融ガラスの減圧脱泡処理を高効率で行う用途に
極めて好適である。
As described in detail above, according to the present invention, in a vacuum degassing apparatus for molten glass for removing bubbles from a continuously supplied molten glass, a high-temperature molten glass can be used. While ensuring sufficient durability, the cost can be significantly reduced, and the capacity of the apparatus can be increased, and the temperature of the vacuum degassing process can be increased. Therefore, it is very suitable for applications in which high-efficiency degassing treatment of molten glass with a large flow rate is performed.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の減圧脱泡装置の一例を示す概略断面図
である。
FIG. 1 is a schematic sectional view showing an example of a vacuum degassing apparatus of the present invention.

【図2】図1に示される減圧脱泡装置における、上昇管
と延長管との連結部分を示す概略断面図である。
FIG. 2 is a schematic sectional view showing a connecting portion between a riser tube and an extension tube in the vacuum degassing apparatus shown in FIG.

【図3】従来における減圧脱泡装置の一例を示す概略断
面図である。
FIG. 3 is a schematic sectional view showing an example of a conventional vacuum degassing apparatus.

【符号の説明】[Explanation of symbols]

10 (溶融ガラスの)減圧脱泡装置 12 減圧ハウジング 14 減圧脱泡槽 16 上昇管 18 下降管 20 溶解槽 22 上流ピット 24 下流ヒット 26,28 延長管 26a 筒体 26b 固定用フランジ 26c シール用フランジ 30 電鋳レンガ 32 断熱レンガ 34 シール部材 36 補強部材 38 断熱材 40 緩衝機構 42 筒状ベローズ 44 押し上げ手段 46,48 連結手段 50 棒材 52 付勢部材 DESCRIPTION OF SYMBOLS 10 Vacuum degassing apparatus (of molten glass) 12 Vacuum decompression housing 14 Vacuum degassing tank 16 Ascending pipe 18 Downcoming pipe 20 Melting tank 22 Upstream pit 24 Downstream hit 26, 28 Extension pipe 26a Cylindrical body 26b Fixing flange 26c Sealing flange 30 Electroformed brick 32 Insulated brick 34 Sealing member 36 Reinforcing member 38 Insulating material 40 Buffering mechanism 42 Cylindrical bellows 44 Pushing-up means 46, 48 Connecting means 50 Bar 52 Energizing member

───────────────────────────────────────────────────── フロントページの続き (72)発明者 今牧 捷治 神奈川県横浜市鶴見区末広町1丁目1番地 旭硝子株式会社京浜工場内 (72)発明者 松脇 正隆 神奈川県横浜市鶴見区末広町1丁目1番地 旭硝子株式会社京浜工場内 ──────────────────────────────────────────────────続 き Continued on the front page (72) Inventor Shoji Imamaki 1-1-1, Suehirocho, Tsurumi-ku, Yokohama-shi, Kanagawa Prefecture Inside Keihin Plant of Asahi Glass Co., Ltd. (72) Inventor Masataka Matsuwaki 1 Suehirocho, Tsurumi-ku, Yokohama-shi, Kanagawa 1-chome Inside the Keihin Plant of Asahi Glass Co., Ltd.

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】真空吸引される減圧ハウジングと、 この減圧ハウジング内に設けられ、溶融ガラスの減圧脱
泡を行う減圧脱泡槽と、 この減圧脱泡槽に連通して設けられ、前記減圧脱泡前の
溶融ガラスを上昇させて前記減圧脱泡槽に導入する上昇
管と、 前記減圧脱泡槽に連通して設けられ、前記減圧脱泡後の
溶融ガラスを前記減圧脱泡槽から下降させて導出する下
降管と、 前記上昇管および下降管の下端にそれぞれ連通して設け
られる延長管とを有し、 前記上昇管、前記減圧脱泡槽および前記下降管は、少な
くとも前記溶融ガラスと直接接触する部分が電鋳レンガ
で形成され、前記延長管は、白金または白金合金で形成
されたことを特徴とする溶融ガラスの減圧脱泡装置。
A vacuum housing for vacuum suction; a vacuum degassing tank provided in the vacuum housing for vacuum degassing of the molten glass; and a vacuum degassing tank provided in communication with the vacuum degassing tank. An ascending pipe that raises the molten glass before foaming and introduces the molten glass into the vacuum degassing tank, is provided in communication with the vacuum degassing tank, and lowers the molten glass after the vacuum degassing from the vacuum degassing tank. And an extension pipe provided in communication with lower ends of the riser and the downcomer, respectively, wherein the riser, the vacuum degassing tank and the downcomer are at least directly connected to the molten glass. A degassing apparatus for depressurizing molten glass, wherein a portion to be contacted is formed of electroformed brick, and said extension tube is formed of platinum or a platinum alloy.
【請求項2】前記延長管は、その上端にフランジが形成
され、このフランジが前記上昇管もしくは前記下降管を
形成する前記電鋳レンガの目地に挿入されて挟持される
ことにより、前記上昇管もしくは前記下降管に固定され
たものである請求項1または2に記載の溶融ガラスの減
圧脱泡装置。
2. The extension pipe has a flange formed at an upper end thereof, and the flange is inserted into a joint of the electroformed brick forming the riser pipe or the downcomer pipe to be clamped, thereby forming the riser pipe. The vacuum degassing apparatus for molten glass according to claim 1 or 2, wherein the apparatus is fixed to the downcomer.
JP30532697A 1997-10-06 1997-11-07 Vacuum degassing equipment for molten glass Expired - Fee Related JP3817868B2 (en)

Priority Applications (12)

Application Number Priority Date Filing Date Title
JP30532697A JP3817868B2 (en) 1997-11-07 1997-11-07 Vacuum degassing equipment for molten glass
US09/164,356 US6119484A (en) 1997-10-06 1998-10-01 Vacuum degassing apparatus for molten glass
KR1019980041667A KR100682778B1 (en) 1997-10-06 1998-10-02 Vacuum degassing apparatus for molten glass
TW087116447A TW498058B (en) 1997-10-06 1998-10-02 Vacuum degassing apparatus for molten glass
IDP981327A ID20649A (en) 1997-10-06 1998-10-05 REASON FOR THE DECREASE OF GAS HAMPA FOR GLASS RELEASE
EP00122258A EP1078891B1 (en) 1997-10-06 1998-10-06 Parallel arrangement of a vacuum degassing apparatus for molten glass
DE69823560T DE69823560T2 (en) 1997-10-06 1998-10-06 Parallel arrangement of a vacuum degassing device for molten glass
EP04007832A EP1439148A3 (en) 1997-10-06 1998-10-06 Apparatus for degassing molten glass under reduced pressure
EP98118842A EP0908417B2 (en) 1997-10-06 1998-10-06 Vacuum degassing apparatus for molten glass
DE69807812T DE69807812T3 (en) 1997-10-06 1998-10-06 Vacuum degassing apparatus for molten glass
US09/473,680 US6405564B1 (en) 1997-10-06 1999-12-29 Vacuum degassing apparatus for molten glass
KR1020060029382A KR100682779B1 (en) 1997-10-06 2006-03-31 Vacuum degassing apparatus for molten glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP30532697A JP3817868B2 (en) 1997-11-07 1997-11-07 Vacuum degassing equipment for molten glass

Publications (2)

Publication Number Publication Date
JPH11139834A true JPH11139834A (en) 1999-05-25
JP3817868B2 JP3817868B2 (en) 2006-09-06

Family

ID=17943772

Family Applications (1)

Application Number Title Priority Date Filing Date
JP30532697A Expired - Fee Related JP3817868B2 (en) 1997-10-06 1997-11-07 Vacuum degassing equipment for molten glass

Country Status (1)

Country Link
JP (1) JP3817868B2 (en)

Cited By (8)

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Publication number Priority date Publication date Assignee Title
JP2001080922A (en) * 1999-09-08 2001-03-27 Nippon Electric Glass Co Ltd Supply method and supply device for molten glass
US6948338B2 (en) 2001-09-14 2005-09-27 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
WO2006095523A1 (en) * 2005-03-08 2006-09-14 Asahi Glass Company, Limited Platinum or platinum alloy structure and glass puroduction apparatus making use of the same
WO2008026606A1 (en) 2006-08-29 2008-03-06 Asahi Glass Company, Limited Molten glass conduit structure and vacuum deaerator utilizing the same
WO2012002031A1 (en) 2010-06-30 2012-01-05 旭硝子株式会社 Molten glass vacuum degassing apparatus, vacuum degassing method, and apparatus and method for manufacturing glass product
WO2012017963A1 (en) 2010-08-04 2012-02-09 旭硝子株式会社 Molten glass duct structure, vacuum defoaming device provided therewith, vacuum defoaming method of molten glass, and glass product manufacturing method
WO2012133897A1 (en) 2011-03-31 2012-10-04 旭硝子株式会社 Vacuum degassig apparatus, apparatus for producing glassware, and method for producing glassware
JP2016050149A (en) * 2014-08-29 2016-04-11 AvanStrate株式会社 Method for manufacturing glass plate and device for manufacturing glass plate

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001080922A (en) * 1999-09-08 2001-03-27 Nippon Electric Glass Co Ltd Supply method and supply device for molten glass
US6948338B2 (en) 2001-09-14 2005-09-27 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
WO2006095523A1 (en) * 2005-03-08 2006-09-14 Asahi Glass Company, Limited Platinum or platinum alloy structure and glass puroduction apparatus making use of the same
EP1857420A1 (en) * 2005-03-08 2007-11-21 Asahi Glass Company, Limited Platinum or platinum alloy structure and glass puroduction apparatus making use of the same
EP1857420A4 (en) * 2005-03-08 2010-10-27 Asahi Glass Co Ltd Platinum or platinum alloy structure and glass puroduction apparatus making use of the same
US8136373B2 (en) 2006-08-29 2012-03-20 Asahi Glass Company, Limited Conduit structure for molten glass and vacuum degassing apparatus using the conduit structure
WO2008026606A1 (en) 2006-08-29 2008-03-06 Asahi Glass Company, Limited Molten glass conduit structure and vacuum deaerator utilizing the same
WO2012002031A1 (en) 2010-06-30 2012-01-05 旭硝子株式会社 Molten glass vacuum degassing apparatus, vacuum degassing method, and apparatus and method for manufacturing glass product
JP5772823B2 (en) * 2010-06-30 2015-09-02 旭硝子株式会社 Vacuum degassing apparatus and vacuum degassing method for molten glass, and glass product manufacturing apparatus and manufacturing method
WO2012017963A1 (en) 2010-08-04 2012-02-09 旭硝子株式会社 Molten glass duct structure, vacuum defoaming device provided therewith, vacuum defoaming method of molten glass, and glass product manufacturing method
US9073772B2 (en) 2010-08-04 2015-07-07 Asahi Glass Company, Limited Conduit structure for molten glass, vacuum degassing apparatus, vacuum degassing method for molten glass and process for producing glass products employing said conduit structure
WO2012133897A1 (en) 2011-03-31 2012-10-04 旭硝子株式会社 Vacuum degassig apparatus, apparatus for producing glassware, and method for producing glassware
JP5888325B2 (en) * 2011-03-31 2016-03-22 旭硝子株式会社 Vacuum degassing apparatus, glass product manufacturing apparatus, and glass product manufacturing method
US9505645B2 (en) 2011-03-31 2016-11-29 Asahi Glass Company, Limited Vacuum degassing apparatus, apparatus for producing glassware, and method for producing glassware
JP2016050149A (en) * 2014-08-29 2016-04-11 AvanStrate株式会社 Method for manufacturing glass plate and device for manufacturing glass plate

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