JPH11130444A - Reduced pressure deforming apparatus for molten glass - Google Patents

Reduced pressure deforming apparatus for molten glass

Info

Publication number
JPH11130444A
JPH11130444A JP29809897A JP29809897A JPH11130444A JP H11130444 A JPH11130444 A JP H11130444A JP 29809897 A JP29809897 A JP 29809897A JP 29809897 A JP29809897 A JP 29809897A JP H11130444 A JPH11130444 A JP H11130444A
Authority
JP
Japan
Prior art keywords
vacuum degassing
molten glass
reduced pressure
degassing tank
tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP29809897A
Other languages
Japanese (ja)
Inventor
Yusuke Takei
祐輔 竹居
Shun Kijima
駿 木島
Junji Tanigaki
淳史 谷垣
Shoji Imamaki
捷治 今牧
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AGC Inc
Original Assignee
Asahi Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd
Priority to JP29809897A priority Critical patent/JPH11130444A/en
Publication of JPH11130444A publication Critical patent/JPH11130444A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B5/00Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
    • C03B5/16Special features of the melting process; Auxiliary means specially adapted for glass-melting furnaces
    • C03B5/225Refining
    • C03B5/2252Refining under reduced pressure, e.g. with vacuum refiners

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Degasification And Air Bubble Elimination (AREA)

Abstract

PROBLEM TO BE SOLVED: To prevent the distortion and deterioration occurring in the thermal expansion of a reduced pressure housing and a reduced pressure deforming vessel and to improve the durability, etc., of the apparatus by dividing the main body part of the reduced pressure housing of a reduced pressure deforming apparatus to a riser housing section and a downcomer housing section and hermetically and expandably and contractably connecting respective disassembled disassembly pieces by means of buffer member. SOLUTION: This apparatus comprises a cylindrical reduced pressure deforming vessel 14 which executes reduced pressure deforming of the molten glass G, the riser 16 and downcomer 18 which are respectively disposed to communicate with the reduced pressure deforming vessel 14 and introduce the molten glass prior to reduced pressure deforming to the reduced pressure deforming vessel 14 and lead the molten glass after reduced pressure deforming out of the reduced pressure deforming 14, a main body section 12a which houses the reduced pressure deforming vessel 14, a riser housing section 12b which houses part of the riser 16 and a downcomer housing section 12c which houses part of the downcomer 18. The apparatus includes the reduced pressure housing 12 for executing vacuum suction. The main body section 12a of the reduced pressure housing 12 is disassembled at >=1 points between the riser housing section 12b and the downcomer housing section 12c. The respective disassembly pieces are connected hermetically and expandably and contractably connected by buffer members 36.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、連続的に供給され
る溶融ガラスから気泡を除去する、溶融ガラスの減圧脱
泡装置の技術分野に属する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention belongs to the technical field of a vacuum degassing apparatus for molten glass for removing air bubbles from a continuously supplied molten glass.

【0002】[0002]

【従来の技術】従来より、成形されたガラス製品の品質
を向上させるために、溶融炉で溶融したガラスを成形装
置で成形する前に溶融ガラス内に発生した気泡を除去す
る減圧脱泡装置が用いられている。このような従来の減
圧脱泡装置を図4に示す。図4に示す減圧脱泡装置10
0は、溶解槽112中の溶融ガラスGを減圧脱泡処理し
て、次の処理槽に連続的に供給するプロセスに用いられ
るものであって、真空吸引されている。減圧ハウジング
102内に水平に減圧脱泡槽104が収納配置され、そ
の両端に垂直に取り付けられる上昇管106および下降
管108が収納配置されている。
2. Description of the Related Art Conventionally, in order to improve the quality of molded glass products, a vacuum degassing apparatus for removing bubbles generated in molten glass before forming the glass melted in a melting furnace with a forming apparatus has been known. Used. FIG. 4 shows such a conventional vacuum degassing apparatus. The vacuum degassing apparatus 10 shown in FIG.
Numeral 0 is used in a process of defoaming the molten glass G in the melting tank 112 under reduced pressure and continuously supplying the molten glass G to the next processing tank. A decompression degassing tank 104 is horizontally accommodated in a decompression housing 102, and an ascending pipe 106 and a descending pipe 108 vertically attached to both ends thereof are accommodated and arranged.

【0003】上昇管106は減圧脱泡槽104に連通
し、脱泡処理前の溶融ガラスGを溶解槽112から上昇
させて減圧脱泡槽104に導入する。下降管108は、
減圧脱泡槽104に連通し、脱泡処理後の溶融ガラスG
を減圧脱泡槽104から下降させて次の処理槽(図示せ
ず)に導出する。そして、減圧ハウジング102内にお
いて、減圧脱泡槽104、上昇管106および下降管1
08の周囲には、これらを断熱被覆する断熱用耐火レン
ガなどの断熱材110が配設されている。なお、減圧ハ
ウジング102は、金属製、例えばステンレス製であ
り、外部から真空ポンプ(図示せず)等によって真空吸
引され、内部が減圧され、内設される減圧脱泡槽104
内を所定の減圧、例えば1/20〜1/3気圧の減圧状
態に維持する。
The rising pipe 106 communicates with the vacuum degassing tank 104, and the molten glass G before defoaming is lifted from the melting tank 112 and introduced into the vacuum degassing tank 104. The downcomer 108 is
The molten glass G after the defoaming process is communicated with the vacuum degassing tank 104.
Is lowered from the vacuum degassing tank 104 and led out to the next processing tank (not shown). Then, in the decompression housing 102, the decompression degassing tank 104, the rising pipe 106 and the downcomer 1
Around the area 08, a heat insulating material 110 such as a refractory brick for heat insulation that covers the heat insulating material is provided. The decompression housing 102 is made of metal, for example, stainless steel, is vacuum-sucked from the outside by a vacuum pump (not shown) or the like, decompresses the inside, and has a decompression degassing tank 104 installed therein.
The inside is maintained at a predetermined reduced pressure, for example, a reduced pressure of 1/20 to 1/3 atm.

【0004】従来の減圧脱泡装置100においては、高
温、例えば1200〜1400℃の温度の溶融ガラスG
を処理するように構成されているので、本出願人の出願
に係る特開平2−221129号公報に開示されている
ように、減圧脱泡槽104、上昇管106および下降管
108などのように溶融ガラスGと直接接触する部分
は、通常白金または白金ロジウムのような白金合金など
の貴金属製円管で構成されている。ここで、これらを白
金合金などの貴金属製円管で構成するのは、溶融ガラス
Gが高温であるばかりでなく、貴金属が溶融ガラスとの
高温反応性が低く、溶融ガラスとの反応による不均質化
を生じさせることがなく、高温での強度がある程度確保
できるからである。特に、減圧脱泡槽104を貴金属製
円管で構成するのは、上記理由に加え、貴金属製円管自
体に電流を流して自己発熱させ、円筒内の溶融ガラスG
を均一に加熱し、溶融ガラスGの温度を所定の温度に保
持するためである。
In the conventional vacuum degassing apparatus 100, the molten glass G at a high temperature, for example, at a temperature of 1200 to 1400 ° C.
As described in Japanese Unexamined Patent Application Publication No. 2-221129 filed by the present applicant, a vacuum degassing tank 104, an ascending pipe 106, a descending pipe 108, etc. The portion that is in direct contact with the molten glass G is usually formed of a circular pipe made of a noble metal such as platinum or a platinum alloy such as platinum rhodium. Here, these are made of a circular tube made of a noble metal such as a platinum alloy because not only the molten glass G has a high temperature, but also the noble metal has a low high-temperature reactivity with the molten glass, and is heterogeneous due to the reaction with the molten glass. This is because the formation at a high temperature can be ensured to a certain degree without causing the formation of a layer. In particular, in addition to the above-mentioned reason, the vacuum degassing tank 104 is formed of a precious metal circular tube.
Is uniformly heated to maintain the temperature of the molten glass G at a predetermined temperature.

【0005】ところで、減圧脱泡槽104を貴金属で構
成すると、高温強度の点から円管とするのがよいが、白
金などの貴金属は高価であるため、肉厚を大きくできな
いため、コストおよび強度の両方の点から円管の直径に
は限界があり、あまり大きくできず、減圧脱泡槽104
で脱泡処理できる溶融ガラスGの流量にも限界があり、
大流量の減圧脱泡装置を構築できないという問題があっ
た。もちろん、円管状減圧脱泡槽104の全長を長くし
て流速を速くすることにより、脱泡処理量を増加させる
ことも考えられるが、処理量に比して、また溶解槽や成
形処理槽などに比べて、装置が長大化してしまうという
問題もあった。このため、減圧脱泡装置100における
溶融ガラスGの脱泡処理量(流量)を大きくできないと
いう問題もあった。
When the vacuum degassing tank 104 is made of a noble metal, it is preferable to use a circular tube from the viewpoint of high-temperature strength. However, since a noble metal such as platinum is expensive, its thickness cannot be increased, so that cost and strength are reduced. From both points, the diameter of the circular pipe is limited and cannot be so large,
There is also a limit on the flow rate of the molten glass G that can be defoamed by
There was a problem that a vacuum degassing apparatus with a large flow rate could not be constructed. Of course, it is conceivable to increase the total length of the cylindrical vacuum degassing tank 104 to increase the flow rate, thereby increasing the amount of degassing treatment. There is also a problem that the device becomes longer than in the case of the above. For this reason, there is also a problem that the degassing processing amount (flow rate) of the molten glass G in the vacuum degassing apparatus 100 cannot be increased.

【0006】なお、溶融ガラスGは、粉体原料を溶解反
応させることによって得られるので、溶解の点では、溶
解槽112の温度は高い方が好ましく、また、減圧脱泡
の点では溶融ガラスの粘度は低く、従って温度は高い方
が好ましい。しかしながら、高温強度の点から減圧脱泡
槽104などに貴金属合金を用いる必要がある一方で、
貴金属は高価なものであり、コストの点から円管の厚み
をあまり厚くできないため、白金などの貴金属を用いる
と、減圧脱泡装置100の入口での溶融ガラスGの温度
は、上述した所定温度(1200〜1400℃)に制限
されてしまっていた。
Since the molten glass G is obtained by melting and reacting the powdery raw material, it is preferable that the temperature of the melting tank 112 be higher in terms of melting, and that the molten glass G be reduced in terms of degassing under reduced pressure. It is preferred that the viscosity be low and therefore the temperature be high. However, while it is necessary to use a noble metal alloy in the vacuum degassing tank 104 and the like from the viewpoint of high temperature strength,
Since the noble metal is expensive and the thickness of the circular tube cannot be increased so much from the viewpoint of cost, if a noble metal such as platinum is used, the temperature of the molten glass G at the inlet of the vacuum degassing apparatus 100 becomes the above-mentioned predetermined temperature. (1200-1400 ° C.).

【0007】[0007]

【発明が解決しようとする課題】ところで、このような
問題に対し、減圧脱泡槽104、上昇管106および下
降管108を貴金属合金よりも安価な耐火物で構成し、
貴金属合金の場合と同様に溶融ガラスを連続的に減圧脱
泡処理することができれば、白金などの貴金属合金を用
いる場合に比べて、コストの点から使用量を制限した
り、それに伴う強度低下の点から大きさを制限したりす
る必要性はなくなり、装置設計の自由度が飛躍的に向上
することから、大流量の減圧脱泡装置の構築が可能にな
るとともに、より高温での減圧脱泡処理も可能になるも
のと考えられる。
In order to solve such a problem, the vacuum degassing tank 104, the riser pipe 106 and the descender pipe 108 are made of a refractory which is less expensive than a noble metal alloy.
If the molten glass can be continuously depressurized and degassed as in the case of precious metal alloys, the amount of use can be limited from the viewpoint of cost compared to the case of using precious metal alloys such as platinum, and the reduction in strength accompanying it can be reduced. It is no longer necessary to limit the size from the point of view, and the degree of freedom in equipment design is dramatically improved, so that it is possible to construct a vacuum degassing apparatus with a large flow rate and to decompress at a higher temperature. It is believed that processing will also be possible.

【0008】しかしながら、耐火物で減圧脱泡槽などを
構成した場合においても、白金合金製の場合と同様に、
加熱により熱膨張が起こるという問題がある。この減圧
脱泡槽自体の熱膨張を効率的に吸収して装置内の歪みを
除去する方法として、白金合金製の場合には、減圧脱泡
槽を構成する白金合金製円筒自体に複数個のフランジを
設けることにより熱膨張に応じて伸縮可能な構成とする
ことで対応していた。これに対し、上述の耐火物製とす
る場合には、展延性に乏しい耐火物自体で蛇腹を構成す
ることができないため、熱膨張をいかにして逃がすかが
問題となる。また、もし熱膨張を十分に逃がすことがで
きないと、装置内に歪みが生じてしまい、最悪の場合に
は、破損に至る、特に、減圧脱泡槽と上昇管、下降管の
接合部に歪みが生じると、破損しやすいなど、装置の安
全性を損なうおそれがあるという問題がある。
However, even when a vacuum degassing tank or the like is made of a refractory material, as in the case of a platinum alloy,
There is a problem that thermal expansion occurs due to heating. As a method of efficiently absorbing the thermal expansion of the vacuum degassing tank itself and removing distortion in the apparatus, in the case of a platinum alloy, a plurality of platinum alloy cylinders themselves constituting the vacuum degassing tank are used. This has been dealt with by providing a flange so as to be able to expand and contract according to thermal expansion. On the other hand, in the case of the above-mentioned refractory, since the bellows cannot be constituted by the refractory having poor ductility itself, there is a problem how to escape the thermal expansion. Also, if the thermal expansion cannot be sufficiently released, distortion will occur in the device, and in the worst case, it will lead to breakage, especially at the joint between the vacuum degassing tank and the ascending pipe, descending pipe. When this occurs, there is a problem that the safety of the device may be impaired, for example, the device is easily damaged.

【0009】さらに、減圧脱泡槽等を構成する耐火物が
一旦熱膨張し、その後温度が低下して収縮するような、
熱膨張係数の温度依存性が特異な挙動を示す酸化ジルコ
ニウムを含む耐火物のような場合には、耐火物が熱膨張
後の位置を保持したままで収縮することから、収縮分が
隙間を形成して目地が開いてしまい、この開いた目地か
ら溶融ガラスが漏れ出すおそれがあるという問題もあ
る。
Further, the refractory constituting the vacuum degassing tank or the like once thermally expands and then contracts due to a decrease in temperature.
In the case of refractories containing zirconium oxide, whose temperature dependence of the thermal expansion coefficient behaves in a unique way, the refractory contracts while maintaining its position after thermal expansion, so the shrinkage forms a gap. As a result, the joint is opened, and there is a problem that molten glass may leak from the opened joint.

【0010】本発明の目的は、前記従来技術の問題点を
解決することにあり、連続的に供給される溶融ガラスか
ら気泡を除去する、溶融ガラスの減圧脱泡装置におい
て、高温の溶融ガラスに対して十分な耐久性を有し、安
全性に優れた溶融ガラスの減圧脱泡装置を提供すること
にある。
SUMMARY OF THE INVENTION An object of the present invention is to solve the above-mentioned problems of the prior art. In a vacuum degassing apparatus for molten glass, which removes air bubbles from a continuously supplied molten glass, a high-temperature molten glass is used. It is an object of the present invention to provide a vacuum degassing apparatus for molten glass having sufficient durability and excellent safety.

【0011】[0011]

【課題を解決するための手段】前記目的を達成するため
に、本発明は、溶融ガラスの減圧脱泡を行う筒状の減圧
脱泡槽と、この減圧脱泡槽に連通して設けられ、前記減
圧脱泡前の溶融ガラスを前記減圧脱泡槽に導入する導入
手段と、前記減圧脱泡槽に連通して設けられ、前記減圧
脱泡後の溶融ガラスを前記減圧脱泡槽から導出する導出
手段と、前記減圧脱泡槽を収容する本体部、前記導入手
段の一部を収容する導入手段収容部、および前記導出手
段の一部を収容する導出手段収容部から構成され、真空
吸引される減圧ハウジングとを具備し、前記減圧ハウジ
ングは、その本体部が前記導入手段収容部と前記導出手
段収容部の間の少なくとも1か所で分割され、この分割
された各分割片を気密かつ伸縮可能に連結する緩衝部材
を有することを特徴とする溶融ガラスの減圧脱泡装置を
提供する。
In order to achieve the above object, the present invention provides a cylindrical vacuum degassing tank for performing vacuum degassing of molten glass, and is provided in communication with the vacuum degassing tank. Introducing means for introducing the molten glass before the vacuum degassing into the vacuum degassing tank, and provided in communication with the vacuum degassing tank, and leading the molten glass after the vacuum degassing from the vacuum degassing tank. A deriving unit, a main unit that stores the vacuum degassing tank, an introducing unit receiving unit that partially stores the introducing unit, and a deriving unit receiving unit that partially stores the deriving unit. And a main body portion of the decompression housing is divided at least at one portion between the introduction means accommodating section and the derivation means accommodating section, and each of the divided pieces is airtight and stretchable. It is characterized by having a shock-absorbing member Providing vacuum degassing apparatus for molten glass to.

【0012】ここで、前記減圧脱泡槽の長手方向の一方
の側端に設けられ、前記減圧脱泡槽を固定する固定手段
と、前記減圧脱泡槽の長手方向の他方の側端に設けら
れ、前記減圧脱泡槽を前記固定手段に向かって付勢する
付勢手段とを有するのが好ましい。
[0012] Here, fixing means provided at one longitudinal end of the vacuum degassing tank for fixing the vacuum degassing tank, and fixing means provided at the other longitudinal end of the vacuum degassing tank. And a biasing means for biasing the vacuum degassing tank toward the fixing means.

【0013】また、前記減圧ハウジングの本体部を構成
する前記分割片のうち、前記固定手段が設けられた分割
片を、前記減圧ハウジングが所定の高さとなるように支
持する支持手段と、他の分割片を、前記減圧脱泡槽の長
手方向に移動可能に、かつ、前記減圧ハウジングが前記
所定高さとなるように支持する可動支持手段とを有する
のが好ましい。
[0013] Further, of the divided pieces constituting the main body portion of the decompression housing, a support means for supporting the divided piece provided with the fixing means so that the decompression housing has a predetermined height, and It is preferable to have movable support means for supporting the divided piece so as to be movable in the longitudinal direction of the vacuum degassing tank and for supporting the vacuum housing at the predetermined height.

【0014】また、前記導入手段は、前記減圧脱泡前の
溶融ガラスを前記減圧脱泡槽に上昇させて導入する上昇
管であり、前記導出手段は、前記減圧脱泡後の溶融ガラ
スを前記減圧脱泡槽から下降させて導出する下降管であ
り、さらに、前記上昇管および前記下降管の少なくとも
いずれか一方の上端面が半球面状に形成され、前記減圧
脱泡槽における前記半球面と接する部分が、前記半球面
と嵌合可能な半球面状に形成されるのが好ましい。
Further, the introduction means is a riser pipe which raises and introduces the molten glass before the vacuum degassing into the vacuum degassing tank, and the lead-out means sets the molten glass after the vacuum degassing and degassing. It is a downcomer that descends from the vacuum degassing tank and leads out, and further, at least one of the upper surface of the riser and the downcomer is formed in a hemispherical shape, and the hemispherical surface in the vacuum degassing vessel. It is preferable that the contact portion is formed in a hemispherical shape that can be fitted to the hemispherical surface.

【0015】さらに、前記導入手段、前記減圧脱泡槽お
よび前記導出手段は、少なくとも前記溶融ガラスと直接
接触する主要部分が電鋳耐火物で形成されるのが好まし
い。
Further, it is preferable that at least a main part of the introducing means, the vacuum degassing tank and the deriving means, which is in direct contact with the molten glass, is formed of an electroformed refractory.

【0016】[0016]

【発明の実施の形態】以下、本発明の溶融ガラスの減圧
脱泡装置について、添付の図面に示される好適実施例を
もとに詳細に説明する。
BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, a vacuum degassing apparatus for molten glass of the present invention will be described in detail based on a preferred embodiment shown in the accompanying drawings.

【0017】図1に、本発明の溶融ガラスの減圧脱泡装
置の概略断面図を示す。図1に示すように、減圧脱泡装
置10は、溶解槽20内の溶融ガラスGを減圧脱泡処理
して、図示しない次の処理槽、例えば、フロートバスな
どの板材の成形処理槽や瓶などの成形作業槽などに連続
的に供給するプロセスに用いられるもので、基本的に、
減圧ハウジング12、減圧脱泡槽14、上昇管16およ
び下降管18を有する。減圧ハウジング12は、減圧脱
泡槽14の気密性を確保するためのものであり、略門型
に形成され、本体部12aと、上昇管収容部12bと、
下降管収容部12cとを有する。この減圧ハウジング1
2は、減圧脱泡槽14に必要とされる気密性および強度
を有するものであれば、その材質、構造は特に限定され
るものではないが、金属製、特にステンレス製とするの
が好ましい。このような減圧ハウジング12は、外部か
ら真空ポンプ(図示せず)等によって真空吸引され、内
部が減圧され、内設される減圧脱泡槽14内を所定の減
圧、例えば1/20〜1/3気圧の減圧状態に維持する
ように構成される。
FIG. 1 is a schematic sectional view of a vacuum degassing apparatus for molten glass of the present invention. As shown in FIG. 1, the vacuum degassing apparatus 10 performs a degassing process on the molten glass G in the melting tank 20 under reduced pressure to form a next processing tank (not shown), for example, a plate material forming processing tank such as a float bath or a bottle. It is used in the process of continuously supplying to molding work tanks and the like.
It has a decompression housing 12, a decompression degassing tank 14, an ascending pipe 16 and a descending pipe 18. The decompression housing 12 is for ensuring the airtightness of the decompression degassing tank 14, is formed in a substantially portal shape, and includes a main body 12a, an ascending pipe housing 12b,
And a downcomer receiving section 12c. This decompression housing 1
2 is not particularly limited in its material and structure as long as it has the airtightness and strength required for the vacuum degassing tank 14, but is preferably made of metal, particularly stainless steel. Such a decompression housing 12 is vacuum-evacuated from the outside by a vacuum pump (not shown) or the like, and the inside thereof is decompressed. It is configured to maintain a reduced pressure of 3 atm.

【0018】減圧ハウジング12の本体部12a内には
減圧脱泡槽14が設けられる。また、減圧脱泡槽14の
左端部には上昇管16が連通され、減圧脱泡槽14の右
端部には下降管18が連通される。なお、上昇管16お
よび下降管18の主要部分はそれぞれ減圧ハウジング1
2の上昇管収容部12b、下降管収容部12c内に収容
され、上昇管16および下降管18の下端部分は減圧ハ
ウジング12外に延出するようにして設けられる。
A vacuum degassing tank 14 is provided in the main body 12a of the pressure reducing housing 12. A rising pipe 16 communicates with the left end of the vacuum degassing tank 14, and a downcomer pipe 18 communicates with the right end of the vacuum degassing tank 14. The main parts of the riser pipe 16 and the lowering pipe 18 are respectively connected to
The lower end portions of the ascending pipe 16 and the descending pipe 18 are accommodated in the ascending tube accommodating portion 12b and the descending tube accommodating portion 12c, respectively.

【0019】本発明の減圧脱泡装置10においては、減
圧脱泡槽14、上昇管16および下降管18の材質は特
に限定されず、白金または白金ロジウム、白金パラジウ
ム等の白金合金などの貴金属合金や、電鋳耐火物などが
挙げられるが、中でも電鋳耐火物を用いるのが好まし
い。すなわち、減圧脱泡装置10における溶融ガラスG
と直接接触する主要部分を電鋳耐火物で形成することに
より、従来から用いられてきた貴金属合金製のものより
も、コストが大幅に低減し、従って自由な形状で、か
つ、自由な厚さに設計することが可能となることから、
減圧脱泡装置10の大容量化が実現するとともに、より
高温での減圧脱泡処理も行えるようになるからである。
In the vacuum degassing apparatus 10 of the present invention, the materials of the vacuum degassing tank 14, the riser tube 16 and the downcomer tube 18 are not particularly limited, and noble metal alloys such as platinum or platinum alloys such as platinum rhodium and platinum palladium are used. And electroformed refractories. Among them, it is preferable to use electroformed refractories. That is, the molten glass G in the vacuum degassing apparatus 10
By forming the main part that is in direct contact with the electroformed refractory, the cost is greatly reduced compared to the conventionally used one made of a precious metal alloy, and therefore, the free shape and the free thickness Because it becomes possible to design
This is because the capacity of the vacuum degassing apparatus 10 can be increased and the vacuum degassing process at a higher temperature can be performed.

【0020】従って、減圧脱泡槽14、上昇管16およ
び下降管18の形状は少なくとも筒状であれば特に限定
されず、例えば、その断面形状は円状のみならず矩形状
であってもよい。電鋳耐火物を用いて減圧脱泡槽14、
上昇管16および下降管18を構築する方法は、特に制
限的ではなく、例えば小さい直方体の電鋳レンガを互い
違いに3次元的に、すなわちつなぎ目地構造に積み上
げ、その間の目地の部分を目地材で埋めて、所定長の筒
状管を形成してもよいし、円筒状もしくは角筒状に鋳込
み成形した筒状の電鋳レンガを一列に積み重ねて、その
間の目地の部分を目地材で埋め、所定長の筒状管を形成
してもよい。
Therefore, the shapes of the vacuum degassing tank 14, the riser pipe 16 and the descender pipe 18 are not particularly limited as long as they are at least cylindrical. For example, the cross-sectional shape may be not only circular but also rectangular. . Vacuum degassing tank 14, using electroformed refractories,
The method of constructing the riser pipe 16 and the downcomer pipe 18 is not particularly limited. For example, small rectangular parallelepiped electroformed bricks are alternately stacked three-dimensionally, that is, in a jointed joint structure, and the joint portion therebetween is jointed with jointing material. Filling, a tubular tube of a predetermined length may be formed, or cylindrical electroformed bricks cast and formed into a cylindrical shape or a square tubular shape are stacked in a row, and the joint portion therebetween is filled with a joint material, A cylindrical tube having a predetermined length may be formed.

【0021】特に、減圧脱泡槽14の側面は、図3に示
されるように、下側の側面を構成する電鋳レンガ30を
上方に迫り出させるように構成した迫構造とすれば、左
右から力が加わることにより、目地のずれを防止し、強
固に目地を締めることができるので好ましい。特に、後
述する固定手段40および付勢手段46を設ける際に極
めて有効である。
In particular, as shown in FIG. 3, the side surface of the vacuum degassing tank 14 has a pressing structure in which the electroformed brick 30 constituting the lower side surface is protruded upward. Applying a force from above is preferable because displacement of joints can be prevented and joints can be firmly tightened. In particular, it is very effective when the fixing means 40 and the urging means 46 described later are provided.

【0022】なお、電鋳耐火物を用いる場合であって
も、上昇管16の下端であって、上流案内ダクト20内
の溶融ガラスGに浸漬させる部分や、下降管18の下端
であって後述するケーシング52内の溶融ガラスGに浸
漬させる部分については、特に溶融ガラスGと大気との
界面が存在することから、この界面近傍においては反応
性に富み、特に電鋳耐火物では界面部分や目地部分の劣
化が進行しやすい。従って、上昇管16の下端部および
下降管18の下端部は、白金または白金合金で作製する
のが好ましい。
Even when an electroformed refractory is used, the lower end of the rising pipe 16 which is immersed in the molten glass G in the upstream guide duct 20 or the lower end of the descending pipe 18 will be described later. The portion of the casing 52 to be immersed in the molten glass G is particularly rich in the vicinity of the interface between the molten glass G and the atmosphere because of the presence of the interface between the molten glass G and the atmosphere. Deterioration of the part is easy to progress. Therefore, the lower end of the riser 16 and the lower end of the downcomer 18 are preferably made of platinum or a platinum alloy.

【0023】電鋳耐火物としては、耐火原料を電気溶融
した後、所定形状に鋳込み成形したものであれば特に限
定されず、従来公知の各種の電鋳耐火物を使用すればよ
い。中でも、耐蝕性が高く、素地からの発泡も少ない点
で、アルミナ系電鋳耐火物、ジルコニア系電鋳耐火物、
AZS(Al2 3 −ZrO2 −SiO2 )系電鋳耐火
物等が好適に例示され、具体的には、マースナイト(M
B−G)、ZB−X950、ジルコナイト(ZB)(い
ずれも旭硝子(株)製)等が挙げられる。
The electroformed refractory is not particularly limited as long as the refractory raw material is electromelted and then cast into a predetermined shape, and various conventionally known electroformed refractories may be used. Among them, in terms of high corrosion resistance and little foaming from the substrate, alumina-based electroformed refractories, zirconia-based electroformed refractories,
AZS (Al 2 O 3 —ZrO 2 —SiO 2 ) based electroformed refractories are preferably exemplified, and specifically, masonite (M
BG), ZB-X950, and zirconite (ZB) (all manufactured by Asahi Glass Co., Ltd.).

【0024】そして、減圧脱泡槽14の周囲には減圧脱
泡槽14を被覆する断熱用の耐火レンガ32(以下、断
熱レンガ32とする)が配設され、上昇管16および下
降管18の周囲にもそれぞれを被覆する断熱レンガ32
が配設される。断熱レンガ32としては、公知の種々の
レンガを使用すればよく、特に限定されない。このよう
に配設された断熱レンガ32は、その外側が減圧ハウジ
ング12に覆われることにより減圧ハウジング12内に
収容される。なお、減圧ハウジング12の外壁面の温度
は、断熱レンガ32によってできるだけ減圧ハウジング
12に伝達される熱を遮断して、できるだけ低温、例え
ば100℃程にするのが好ましい。
A refractory brick 32 for heat insulation (hereinafter referred to as a heat insulating brick 32) for covering the vacuum degassing tank 14 is provided around the vacuum degassing tank 14. Insulated bricks 32 that cover each area
Is arranged. Various known bricks may be used as the heat insulating bricks 32, and there is no particular limitation. The heat insulating brick 32 arranged in this manner is accommodated in the decompression housing 12 by covering the outside thereof with the decompression housing 12. Note that the temperature of the outer wall surface of the decompression housing 12 is preferably set to be as low as possible, for example, about 100 ° C., by blocking the heat transmitted to the decompression housing 12 by the heat insulating bricks 32 as much as possible.

【0025】また、減圧脱泡槽14、上昇管16および
下降管18の周囲には、必要に応じて、断熱レンガ32
とともに、加熱ヒータを設けて加熱可能な構成としても
よいし、冷却水を通過可能にして冷却可能な構成として
もよい。
Further, around the vacuum degassing tank 14, the riser pipe 16 and the descender pipe 18, if necessary, a heat insulating brick 32
In addition, a configuration may be adopted in which a heater can be provided to enable heating, or a configuration in which cooling water is allowed to pass and cooling is possible.

【0026】このように、図示例の減圧脱泡装置は、減
圧脱泡槽14、上昇管16および下降管18が、少なく
とも溶融ガラスGと直接接触する主要部分が電鋳耐火物
で形成されるものである。従って、前述したように、延
性に富む白金合金製の場合のように減圧脱泡槽にフラン
ジを設けることにより伸縮可能な構成とすることができ
ないため、熱膨張をいかにして逃がすかが問題となる。
また、熱膨張を十分に逃がすことができないと、装置内
に歪みが生じてしまい、最悪の場合には、破損に至るな
ど、装置の安全性を損なうおそれがあるという問題があ
る。さらに、減圧脱泡槽等を構成する耐火物が一旦熱膨
張し、その後収縮する場合には、目地が開き、溶融ガラ
スが漏れ出すおそれがあるという問題もある。
As described above, in the vacuum degassing apparatus of the illustrated example, at least the main parts of the vacuum degassing tank 14, the riser pipe 16 and the downcomer pipe 18 which are in direct contact with the molten glass G are formed of the electroformed refractory. Things. Therefore, as described above, since it is not possible to provide a structure capable of expanding and contracting by providing a flange in a vacuum degassing tank as in the case of a platinum alloy having high ductility, how to escape thermal expansion is a problem. Become.
In addition, if the thermal expansion cannot be sufficiently released, distortion occurs in the device, and in the worst case, there is a problem that the safety of the device may be impaired, such as damage. Furthermore, when the refractory constituting the vacuum degassing tank or the like once thermally expands and then contracts, there is a problem that joints are opened and molten glass may leak.

【0027】そこで、本発明は、減圧ハウジングの本体
部12aを、上昇管収容部12bと下降管収容部12c
の間の少なくとも1か所で分割して、この分割された各
構成部分(以下、分割片とする)を気密かつ伸縮可能に
連結する緩衝部材36を設けたことにより、上記問題を
解決したものである。すなわち、減圧脱泡槽14、例え
ば、減圧脱泡装置14を構成する電鋳耐火物、およびそ
の周囲を覆う断熱レンガ32の熱膨張を、減圧ハウジン
グ12に設けられた緩衝部材36によって吸収すること
により、減圧ハウジング12自体、およびこのハウジン
グ12内に収容される減圧脱泡槽14の熱膨張に起因す
る歪みや劣化を防止し、装置の安全性を向上させること
ができる。
In the present invention, the main body 12a of the decompression housing is divided into an ascending tube accommodating portion 12b and a descending tube accommodating portion 12c.
The above-mentioned problem has been solved by providing a buffer member 36 which is divided at least at one point between the two and the divided components (hereinafter, referred to as divided pieces) are connected in an airtight and stretchable manner. It is. That is, the buffer member 36 provided in the decompression housing 12 absorbs the thermal expansion of the vacuum degassing tank 14, for example, the electroformed refractory constituting the vacuum degassing device 14 and the insulating brick 32 covering the periphery thereof. Accordingly, it is possible to prevent distortion and deterioration due to thermal expansion of the decompression housing 12 itself and the decompression and deaeration tank 14 housed in the housing 12, thereby improving the safety of the apparatus.

【0028】具体的には、図1に示されるように、減圧
ハウジングの本体部12aには、緩衝部材36が2か所
に設けられる。緩衝部材36は、減圧脱泡槽14やその
周囲を覆う断熱レンガ32の熱膨張を吸収して、減圧ハ
ウジング12の歪みや劣化を防止するためのものであ
り、減圧ハウジングの本体部12aであって、上昇管収
容部12bと下降管収容部12cの間で切断されて分割
された各分割片の間を、気密かつ伸縮可能に連結するこ
とにより設けられる。緩衝部材36としては、減圧ハウ
ジング12としての機能を損なわない程度の強度および
気密性を有し、かつ伸縮可能な部材であれば特に限定さ
れず、従来公知の種々の部材が使用可能であるが、金属
製の筒状ベローズとするのが、強度、気密性および伸縮
性の点から好ましく、例えばステンレス製の筒状ベロー
ズが好適に例示される。
More specifically, as shown in FIG. 1, two buffer members 36 are provided in the main body 12a of the decompression housing. The buffer member 36 is for absorbing thermal expansion of the vacuum degassing tank 14 and the heat insulating bricks 32 surrounding the same to prevent distortion and deterioration of the vacuum housing 12, and is a main body 12a of the vacuum housing. In this manner, each of the divided pieces cut and divided between the riser tube accommodating portion 12b and the descending tube accommodating portion 12c is provided in an airtight and stretchable manner. The cushioning member 36 is not particularly limited as long as it has strength and airtightness that does not impair the function of the decompression housing 12 and can expand and contract, and various conventionally known members can be used. It is preferable to use a metal cylindrical bellows in view of strength, airtightness and elasticity, and a stainless steel bellows is preferably exemplified.

【0029】設けられる緩衝部材36の数は、特に限定
されるものではなく、少なくとも1か所以上であれば何
か所であってもよいが、図示例のように2か所設ける構
成とすれば、減圧ハウジングの本体部12aは、上昇管
16側の分割片13a、中央の分割片13bおよび下降
管18側の分割片13cという、3つの分割片に分割さ
れるので、後述する可動支持手段60を中央の分割片1
3bにも設けることができ、減圧脱泡装置全体を少なく
とも3点でバランス良く支持することができるので好ま
しい。なお、あるいは可動支持手段60を左右の分割片
13a,13cに設けて中央の分割片13bを固定する
ようにしてもよい。
The number of cushioning members 36 provided is not particularly limited, and may be any number as long as it is at least one or more. For example, the main body 12a of the decompression housing is divided into three divided pieces: a divided piece 13a on the riser pipe 16 side, a central divided piece 13b, and a divided piece 13c on the descending pipe 18 side. 60 is the center split piece 1
3b, which is preferable because the entire vacuum degassing apparatus can be supported in a balanced manner at at least three points. Alternatively, the movable support means 60 may be provided on the left and right divided pieces 13a and 13c to fix the central divided piece 13b.

【0030】また、減圧脱泡槽14には、図1に示され
るように、固定手段40および付勢手段46が設けられ
るのが好ましい。固定手段40は、減圧脱泡槽14の長
手方向の一方の側端(図示例では上昇管16側の端部1
4a)を所定位置に固定するためのものであり、その材
質、構造は特に限定されず、種々の固定手段が使用可能
である。例えば、図示例のように、減圧脱泡槽14の端
面と接合する板材42と、この板材42に連結して設け
られ、他端が図示しない槽窯荷重受け鋼材等に固定され
る棒材44とから構成すればよい。棒材44は減圧ハウ
ジング12を貫通する部分でシーリングされている。な
お、板材42および棒材44は、ステンレス製とするの
が強度および耐蝕性の点から好ましく、棒材44の本数
は、特に限定されないが、複数本(例えば2本)とする
のが減圧脱泡槽14の端面全体を固定できる点で好まし
い。
Further, as shown in FIG. 1, the vacuum degassing tank 14 is preferably provided with fixing means 40 and urging means 46. The fixing means 40 is connected to one end of the vacuum degassing tank 14 in the longitudinal direction (the end 1 on the riser pipe 16 side in the illustrated example).
4a) is to be fixed at a predetermined position, and its material and structure are not particularly limited, and various fixing means can be used. For example, as shown in the drawing, a plate member 42 joined to the end surface of the vacuum degassing tank 14 and a rod member 44 provided to be connected to the plate member 42 and having the other end fixed to a tank kiln load receiving steel material (not shown) or the like. What is necessary is just to comprise from. The bar 44 is sealed at a portion penetrating the decompression housing 12. The plate member 42 and the bar member 44 are preferably made of stainless steel in view of strength and corrosion resistance. The number of the bar members 44 is not particularly limited. This is preferable in that the entire end face of the foam tank 14 can be fixed.

【0031】付勢手段46は、減圧脱泡槽14の他端、
すなわち固定手段40が設けられない側(図示例では下
降管18側の端部14b)を、固定手段40に向かって
付勢することにより、減圧脱泡槽14の形状を一定圧力
で保持しつつ、目地を強固に締めるためのものであり、
その材質、構造は特に限定されず、種々の付勢手段が使
用可能である。例えば、図示例のように、減圧脱泡槽1
4の端面14bと接合する板材48と、この板材48に
隣接して設けられる付勢部材50と、この付勢部材50
に連結して設けられ、一端が図示しない槽窯荷重受け鋼
材等に固定される棒材52とから構成すればよい。棒材
52は減圧ハウジング12を貫通する部分でシーリング
されている。なお、板材48および棒材52は、固定手
段40と同様、ステンレス製とするのが好ましく、付勢
部材50および棒材52の数は、特に限定されないが、
複数本(例えば2本)ずつ設けられるのが減圧脱泡槽1
4の端面全体を付勢できる点で好ましい。なお、付勢部
材50としては、皿ばね、板ばね等の公知の種々のばね
を用いることができるが、複数枚を組み合わせて任意の
圧縮力を付加しやすいこと等から、皿ばねを用いるのが
好ましい。
The urging means 46 includes the other end of the vacuum degassing tank 14,
In other words, the side where the fixing means 40 is not provided (the end 14b on the side of the downcomer pipe 18 in the illustrated example) is urged toward the fixing means 40 so that the shape of the vacuum degassing tank 14 is maintained at a constant pressure. , To tighten the joints firmly,
The material and structure are not particularly limited, and various urging means can be used. For example, as shown in the illustrated example, the vacuum degassing tank 1
4, a pressing member 50 provided adjacent to the plate member 48, and a pressing member 50
And a bar 52 fixed at one end to a tank furnace load receiving steel (not shown) or the like. The bar 52 is sealed at a portion penetrating the decompression housing 12. The plate member 48 and the bar members 52 are preferably made of stainless steel, similarly to the fixing means 40. The numbers of the urging members 50 and the bar members 52 are not particularly limited,
The vacuum degassing tank 1 is provided in a plurality (for example, two).
4 is preferable in that the entire end face can be biased. As the urging member 50, various known springs such as a disc spring and a leaf spring can be used. However, a disc spring is used because it is easy to apply an arbitrary compressive force by combining a plurality of springs. Is preferred.

【0032】このように、固定手段40および付勢手段
46を減圧脱泡槽14の両端に設けることにより、耐火
物の熱膨張や収縮(冷却時)が生じても、目地を強固に
締めることができ、目地からの溶融ガラスの漏れを有効
に防止できる。さらには、減圧脱泡槽14の形状を保持
しつつ、減圧脱泡槽14の熱膨張を一方向、すなわち付
勢手段50の付勢方向(減圧脱泡槽14の長手方向)に
逃がすこともできるので、熱膨張に起因して装置内に歪
みが生じるのをより効果的に防止し、装置の安全性を高
める効果も得られる。なお、このような固定手段40お
よび付勢手段46は、図示例とは逆に、すなわち、固定
手段40を下降管18側に設け、付勢手段46を上昇管
16側に設ける構成としてもよい。
As described above, by providing the fixing means 40 and the urging means 46 at both ends of the vacuum degassing tank 14, even if thermal expansion or contraction (at the time of cooling) of the refractory occurs, the joint is firmly tightened. And leakage of the molten glass from the joint can be effectively prevented. Further, while maintaining the shape of the vacuum degassing tank 14, the thermal expansion of the vacuum degassing tank 14 may be released in one direction, that is, the urging direction of the urging means 50 (the longitudinal direction of the vacuum degassing tank 14). Therefore, it is possible to more effectively prevent the occurrence of distortion in the device due to thermal expansion, and to obtain an effect of improving the safety of the device. The fixing means 40 and the urging means 46 may be configured in a manner opposite to the illustrated example, that is, the fixing means 40 is provided on the downcomer pipe 18 side and the urging means 46 is provided on the ascending pipe 16 side. .

【0033】ところで、図示例のような減圧脱泡装置
は、最下端部分は溶融ガラスに埋没するため支点になら
ず、また溶融ガラスに浸漬しない範囲で、下端に近い部
分のハウジングを支持すると、重心が支点より上になっ
て安定を欠き装置の設置が困難となることから、支持手
段により減圧ハウジング12の本体部12a自体を持ち
上げて支持するように構成されるのが一般的である。こ
こで、本発明の減圧脱泡装置10においては、このよう
な支持手段として、図1に示すように、固定された支持
手段54と可動支持手段60とを組み合わせて構成する
のが好ましい。すなわち、上昇管16側の分割片の13
aにはその下端を支持する固定支持手段54が、中央部
および下降管18側の分割片13b,13cにはそれぞ
れ下端を支持する可動支持手段60,60が設けられ
る。
By the way, in the vacuum degassing apparatus as shown in the figure, the lowermost portion is buried in the molten glass, so that it does not become a fulcrum. Since the center of gravity is higher than the fulcrum and the installation of the device is difficult due to lack of stability, it is general that the main body 12a of the decompression housing 12 is lifted and supported by the support means. Here, in the vacuum degassing apparatus 10 of the present invention, as shown in FIG. 1, it is preferable that such a supporting means is constituted by combining a fixed supporting means 54 and a movable supporting means 60. That is, 13 of the divided pieces on the riser 16 side.
A is provided with fixed support means 54 for supporting the lower end thereof, and movable support means 60, 60 for supporting the lower end thereof at the central portion and the divided pieces 13b, 13c on the side of the downcomer 18 respectively.

【0034】固定支持手段54は、減圧脱泡装置10を
減圧ハウジング12ごと所定の高さに支持するためのも
のであり、固定手段40が設けられた分割片(図示例で
は上昇管16側の分割片13a)の下端に設けられる。
固定支持手段54としては、昇降可能な支持手段を用い
るのが、装置の高さを変更することにより減圧条件等を
適宜調整することができる点で好ましく、例えば、図示
例のように、ジャッキ等の昇降装置56と、この昇降装
置56上に設けられるスペーサ58とから構成すればよ
い。
The fixed supporting means 54 is for supporting the vacuum degassing apparatus 10 together with the vacuum housing 12 at a predetermined height, and is provided with a divided piece provided with the fixing means 40 (in the illustrated example, on the side of the rising pipe 16). It is provided at the lower end of the segment 13a).
As the fixed support means 54, it is preferable to use a support means which can be moved up and down in that the pressure reduction condition and the like can be appropriately adjusted by changing the height of the apparatus. For example, as shown in the illustrated example, a jack or the like is used. And a spacer 58 provided on the lifting device 56.

【0035】可動支持手段60は、固定支持手段54に
よって支持される分割片以外の分割片(図示例では中央
の分割片13b、および下降管18側の分割片13c)
の下端に設けられ、減圧ハウジング12を所定の高さに
支持するとともに、減圧脱泡槽14の長手方向に移動可
能に構成される支持手段であり、例えば、ジャッキ等の
昇降装置62と、この昇降装置62の上に回転可能に設
けられるコロ64とから構成すればよい。また、コロ6
4は各分割片に対して複数個設けてもよいし、コロ64
の代わりに、レール上の車輪、あるいはレールに替わる
棒鋼に通したボールベアリング等を用いてもよい。
The movable support means 60 is a divided piece other than the divided piece supported by the fixed support means 54 (in the illustrated example, the central divided piece 13b and the divided piece 13c on the downcomer pipe 18 side).
Is provided at the lower end of the vacuum decompression housing 12 at a predetermined height, and is configured to be movable in the longitudinal direction of the vacuum degassing tank 14. For example, a lifting device 62 such as a jack, What is necessary is just to comprise the roller 64 rotatably provided on the raising / lowering apparatus 62. Roller 6
4 may be provided for each divided piece.
In place of the above, a wheel on a rail or a ball bearing passing through a steel bar instead of the rail may be used.

【0036】このように、減圧ハウジング12の一分割
片(図示例では上昇管16側の分割片13a)が固定支
持手段56により固定的に支持され、かつ、減圧ハウジ
ング12の他の分割片(図示例では中央の分割片13
b、および下降管18側の分割片13c)が可動支持手
段60により減圧脱泡槽14の長尺方向に移動可能に支
持されることで、減圧ハウジング12自体の熱膨張を逃
がすとともに、減圧ハウジング12内部、特に減圧脱泡
槽14の熱膨張に起因する緩衝部材36の伸縮をスムー
ズに行わせることもでき、減圧ハウジング12の歪みを
より効果的に除去し、装置の安全性をより一層高めるこ
とができる。
As described above, one divided piece (the divided piece 13a on the riser tube 16 side in the illustrated example) of the decompression housing 12 is fixedly supported by the fixed support means 56, and the other divided piece (the In the illustrated example, the center divided piece 13
b, and the divided piece 13c) on the side of the downcomer pipe 18 are supported by the movable supporting means 60 so as to be movable in the longitudinal direction of the decompression degassing tank 14, so that the thermal expansion of the decompression housing 12 itself is released and the decompression housing is released. The expansion and contraction of the buffer member 36 caused by the thermal expansion of the inside 12, particularly the vacuum degassing tank 14, can be performed smoothly, and the distortion of the vacuum housing 12 can be more effectively removed, and the safety of the apparatus can be further enhanced. be able to.

【0037】なお、下降管18と減圧脱泡層14とが接
合する部分(以下、接合部66とする)は、互いに半球
面状に形成するのが好ましい。具体的には、図2に示さ
れるように、下降管18の上端面を凸面状に形成し、こ
の上端と接する減圧脱泡槽14側の接合部を、上記凸面
と嵌合可能な凹面状に形成するのが好ましい。こうする
ことにより、減圧脱泡槽14がその長手方向に熱膨張し
て、上昇管16と下降管18の芯間距離に変動が生じた
場合であっても、下降管18を減圧脱泡槽14の熱膨張
に応じてスムーズに追随させることができるので、接合
部66における応力の集中を緩和し、減圧脱泡槽14の
熱膨張や収縮に起因する接合部66の劣化や破損を防止
するとともに、接合部66近傍における目地の開きを防
止し、溶融ガラスの漏れを防止することもできる。ま
た、下降管18および減圧脱泡槽14のいずれを凹面状
(あるいは凸面状)に構成してもよく、従って、下降管
18の上端を凹面状に形成し、減圧脱泡部14側の接合
部66を凸面状に形成してもよい。さらに、このような
接合部は、下降管18に限らず上昇管16に適用しても
よいが、付勢手段46が設けられる側の管との接合部に
適用するのが熱膨張や収縮を一方向に効率的に逃がすこ
とができる点で好ましい。
The portion where the downcomer 18 and the vacuum degassing layer 14 are joined (hereinafter, referred to as a joining portion 66) is preferably formed in a hemispherical shape. Specifically, as shown in FIG. 2, the upper end surface of the downcomer pipe 18 is formed in a convex shape, and the joint on the reduced pressure degassing tank 14 side in contact with the upper end is formed into a concave shape that can be fitted with the convex surface. It is preferable to form it. In this way, even if the vacuum degassing tank 14 thermally expands in its longitudinal direction and the distance between the cores of the riser 16 and the downcomer 18 fluctuates, the downcomer 18 is removed from the vacuum degasser. Since it is possible to smoothly follow the thermal expansion of the joint 14, the concentration of stress in the joint 66 is reduced, and the deterioration and breakage of the joint 66 due to the thermal expansion and contraction of the vacuum degassing tank 14 are prevented. At the same time, it is possible to prevent the joint from being opened in the vicinity of the joint portion 66 and to prevent the molten glass from leaking. Either the downcomer 18 or the vacuum degassing tank 14 may be formed in a concave shape (or a convex shape). Therefore, the upper end of the downcomer 18 is formed in a concave shape, and the joining at the vacuum degassing section 14 side is performed. The portion 66 may be formed in a convex shape. Further, such a joint may be applied not only to the downcomer pipe 18 but also to the ascending pipe 16, but applying to the joint with the pipe on the side where the urging means 46 is provided reduces thermal expansion and contraction. This is preferable in that it can be efficiently released in one direction.

【0038】このような本発明の減圧脱泡装置10で溶
融ガラスGを脱泡処理して次の処理炉に連続的に供給す
るプロセス例を以下に示す。まず、図示しない真空ポン
プで減圧ハウジング12内および減圧脱泡槽14内を真
空吸引状態に維持する。この状態で、溶解槽20で溶融
されたガラスGは案内ダクト20を通って上昇管16を
介して上昇して減圧脱泡槽14内に導かれ、溶融ガラス
Gは減圧脱泡槽14内で減圧条件下において脱泡処理さ
れる。そして、脱泡処理された溶融ガラスGは下降管1
8を介してキャナル24に導かれる。
An example of a process for defoaming the molten glass G by the vacuum degassing apparatus 10 of the present invention and continuously supplying the same to the next processing furnace will be described below. First, the inside of the vacuum housing 12 and the vacuum degassing tank 14 are maintained in a vacuum suction state by a vacuum pump (not shown). In this state, the glass G melted in the melting tank 20 rises through the guide duct 20 through the riser pipe 16 and is guided into the vacuum degassing tank 14, and the molten glass G is brought into the vacuum degassing tank 14. Defoaming is performed under reduced pressure. Then, the defoamed molten glass G is supplied to the downcomer 1
8 to the canal 24.

【0039】なお、図示例の減圧脱泡装置は、減圧脱泡
槽14、上昇管16および下降管18が、少なくとも前
記溶融ガラスと直接接触する主要部分が電鋳耐火物で形
成されるものであるが、本発明は、これに限定されず、
白金合金製のものにも適用可能である。また、本発明
は、図2に示すサイフォン方式減圧脱泡装置のみなら
ず、特開平5−262530号公報、特開平7−291
633号公報に示す水平式減圧脱泡装置にも適用しても
よいのはもちろんである。
In the vacuum degassing apparatus shown in the drawing, the vacuum degassing tank 14, the riser pipe 16 and the downcomer pipe 18 are formed at least in a main part which is in direct contact with the molten glass by an electroformed refractory. However, the present invention is not limited to this,
It is also applicable to those made of platinum alloy. The present invention is not limited to the siphon-type vacuum degassing apparatus shown in FIG. 2, but is also disclosed in JP-A-5-262530 and JP-A-7-291.
As a matter of course, the present invention may be applied to a horizontal vacuum degassing apparatus described in JP-A-633.

【0040】以上、本発明の溶融ガラスの減圧脱泡装置
について詳細に説明したが、本発明は上記実施例に限定
されず、本発明の要旨を逸脱しない範囲において、各種
の改良および変更を行ってもよいのはもちろんである。
Although the vacuum degassing apparatus for molten glass according to the present invention has been described in detail above, the present invention is not limited to the above-described embodiment, and various improvements and modifications can be made without departing from the gist of the present invention. Of course, you may.

【0041】[0041]

【発明の効果】以上、詳細に説明したように、本発明に
よれば、連続的に供給される溶融ガラスから気泡を除去
する、溶融ガラスの減圧脱泡装置において、高温の溶融
ガラスに対して十分な耐久性を有し、安全性に優れた、
溶融ガラスの減圧脱泡装置を提供することができる。
As described in detail above, according to the present invention, in a vacuum degassing apparatus for molten glass for removing bubbles from a continuously supplied molten glass, a high-temperature molten glass can be used. With sufficient durability and excellent safety,
A vacuum degassing apparatus for molten glass can be provided.

【図面の簡単な説明】[Brief description of the drawings]

【図1】 本発明の減圧脱泡装置の一例を示す概略断面
図である。
FIG. 1 is a schematic sectional view showing an example of a vacuum degassing apparatus of the present invention.

【図2】 図1に示される減圧脱泡装置における、下降
管と減圧脱泡装置との接合部を示す概略断面図である。
FIG. 2 is a schematic cross-sectional view showing a joint between a downcomer pipe and a vacuum degassing apparatus in the vacuum degassing apparatus shown in FIG.

【図3】 図1に示される減圧脱泡装置における、減圧
脱泡槽の側面を示す模式図である。
FIG. 3 is a schematic view showing a side surface of a vacuum degassing tank in the vacuum degassing apparatus shown in FIG.

【図4】 従来における減圧脱泡装置の一例を示す概略
断面図である。
FIG. 4 is a schematic sectional view showing an example of a conventional vacuum degassing apparatus.

【符号の説明】[Explanation of symbols]

10 (溶融ガラスの)減圧脱泡装置 12 減圧ハウジング 14 減圧脱泡槽 16 上昇管 18 下降管 20 溶解槽 22 上流案内ダクト 24 キャナル 32 断熱レンガ 36 緩衝部材 40 固定手段 42,48 板材 44,52 棒材 46 付勢手段 50 付勢部材 54 固定支持手段 56,62 昇降装置 58 スペーサ 60 可動支持手段 64 コロ 66 接合部 DESCRIPTION OF SYMBOLS 10 Decompression degassing apparatus (of molten glass) 12 Decompression housing 14 Decompression housing 16 Ascending pipe 18 Downcoming pipe 20 Melting tank 22 Upstream guide duct 24 Canal 32 Insulating brick 36 Buffer member 40 Fixing means 42,48 Plate 44,52 Rod Material 46 urging means 50 urging member 54 fixed support means 56, 62 elevating device 58 spacer 60 movable support means 64 roller 66 joint

フロントページの続き (72)発明者 今牧 捷治 神奈川県横浜市鶴見区末広町1丁目1番地 旭硝子株式会社京浜工場内Continued on the front page (72) Inventor Shoji Imamaki 1-1, Suehirocho, Tsurumi-ku, Yokohama-shi, Kanagawa Prefecture Inside the Keihin Plant of Asahi Glass Co., Ltd.

Claims (5)

【特許請求の範囲】[Claims] 【請求項1】溶融ガラスの減圧脱泡を行う筒状の減圧脱
泡槽と、 この減圧脱泡槽に連通して設けられ、前記減圧脱泡前の
溶融ガラスを前記減圧脱泡槽に導入する導入手段と、 前記減圧脱泡槽に連通して設けられ、前記減圧脱泡後の
溶融ガラスを前記減圧脱泡槽から導出する導出手段と、 前記減圧脱泡槽を収容する本体部、前記導入手段の一部
を収容する導入手段収容部、および前記導出手段の一部
を収容する導出手段収容部から構成され、真空吸引され
る減圧ハウジングとを具備し、 前記減圧ハウジングは、その本体部が前記導入手段収容
部と前記導出手段収容部の間の少なくとも1か所で分割
され、この分割された各分割片を気密かつ伸縮可能に連
結する緩衝部材を有することを特徴とする溶融ガラスの
減圧脱泡装置。
1. A vacuum degassing tank having a cylindrical shape for performing degassing of molten glass under reduced pressure, and provided in communication with the vacuum degassing tank. The molten glass before the degassing is introduced into the vacuum degassing tank. Introducing means for providing, a deriving means provided in communication with the vacuum degassing tank, and a deriving means for deriving the molten glass after the vacuum degassing from the vacuum degassing tank; An introduction means accommodating part accommodating a part of the introduction means, and a decompression means accommodation part accommodating a part of the derivation means, which is provided with a decompression housing which is suctioned under vacuum; Is divided at at least one place between the introduction means accommodating section and the deriving means accommodating section, and has a buffer member for connecting each of the divided pieces in an airtight and stretchable manner. Vacuum deaerator.
【請求項2】前記減圧脱泡槽の長手方向の一方の側端に
設けられ、前記減圧脱泡槽を固定する固定手段と、 前記減圧脱泡槽の長手方向の他方の側端に設けられ、前
記減圧脱泡槽を前記固定手段に向かって付勢する付勢手
段とを有する請求項1に記載の溶融ガラスの減圧脱泡装
置。
2. A fixing means provided at one longitudinal end of the vacuum degassing tank for fixing the vacuum degassing tank, and a fixing means provided at the other longitudinal end of the vacuum degassing tank. 2. A vacuum degassing apparatus for molten glass according to claim 1, further comprising: urging means for urging said vacuum degassing tank toward said fixing means.
【請求項3】前記減圧ハウジングの本体部を構成する前
記分割片のうち、前記固定手段が設けられた分割片を、
前記減圧ハウジングが所定の高さとなるように支持する
支持手段と、 他の分割片を、前記減圧脱泡槽の長手方向に移動可能
に、かつ、前記減圧ハウジングが前記所定高さとなるよ
うに支持する可動支持手段とを有する請求項1または2
に記載の溶融ガラスの減圧脱泡装置。
3. A divided piece provided with the fixing means among the divided pieces constituting the main body of the decompression housing,
A supporting means for supporting the decompression housing at a predetermined height; and another divided piece movably in the longitudinal direction of the decompression tank, and supporting the decompression housing at the predetermined height. 3. A movable supporting means comprising:
2. A vacuum degassing apparatus for molten glass according to item 1.
【請求項4】前記導入手段は、前記減圧脱泡前の溶融ガ
ラスを前記減圧脱泡槽に上昇させて導入する上昇管であ
り、前記導出手段は、前記減圧脱泡後の溶融ガラスを前
記減圧脱泡槽から下降させて導出する下降管であり、 さらに、前記上昇管および前記下降管の少なくともいず
れか一方の上端面が半球面状に形成され、前記減圧脱泡
槽における前記半球面と接する部分が、前記半球面と嵌
合可能な半球面状に形成された請求項1〜3のいずれか
1項に記載の溶融ガラスの減圧脱泡装置。
4. The introduction means is an ascending pipe that raises and introduces the molten glass before the decompression degassing into the decompression degassing tank, and the derivation means removes the molten glass after the decompression degassing from the molten glass. It is a downcomer pipe that descends from the vacuum degassing tank and is drawn out, and further, the upper end surface of at least one of the riser pipe and the downcomer pipe is formed in a hemispherical shape, and the hemispherical surface in the vacuum degassing vessel. The vacuum degassing apparatus for molten glass according to any one of claims 1 to 3, wherein a contacting portion is formed in a hemispherical shape capable of fitting with the hemispherical surface.
【請求項5】前記導入手段、前記減圧脱泡槽および前記
導出手段は、少なくとも前記溶融ガラスと直接接触する
主要部分が電鋳耐火物で形成された請求項1〜4のいず
れか1項に記載の溶融ガラスの減圧脱泡装置。
5. The apparatus according to claim 1, wherein said introducing means, said vacuum degassing tank and said deriving means have at least a main part which is in direct contact with said molten glass formed of an electroformed refractory. A vacuum degassing apparatus for molten glass as described in the above.
JP29809897A 1997-10-30 1997-10-30 Reduced pressure deforming apparatus for molten glass Pending JPH11130444A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP29809897A JPH11130444A (en) 1997-10-30 1997-10-30 Reduced pressure deforming apparatus for molten glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP29809897A JPH11130444A (en) 1997-10-30 1997-10-30 Reduced pressure deforming apparatus for molten glass

Publications (1)

Publication Number Publication Date
JPH11130444A true JPH11130444A (en) 1999-05-18

Family

ID=17855141

Family Applications (1)

Application Number Title Priority Date Filing Date
JP29809897A Pending JPH11130444A (en) 1997-10-30 1997-10-30 Reduced pressure deforming apparatus for molten glass

Country Status (1)

Country Link
JP (1) JPH11130444A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0963955A1 (en) * 1998-06-10 1999-12-15 Asahi Glass Company Ltd. Apparatus for refining molten glass under reduced pressure
US6948338B2 (en) 2001-09-14 2005-09-27 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
US7007514B2 (en) 2001-09-28 2006-03-07 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
JP2006298657A (en) * 2005-04-15 2006-11-02 Asahi Glass Co Ltd Vacuum defoaming apparatus of molten glass and method for making molten glass clear by using the same
JP2006327830A (en) * 2005-04-28 2006-12-07 Asahi Glass Co Ltd Glass manufacturing apparatus, its component and method for conducting ohmic heating of the component
CN115893812A (en) * 2022-10-31 2023-04-04 陕西彩虹工业智能科技有限公司 Auxiliary installation device and installation method for butt welding position material of glass channel

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0963955A1 (en) * 1998-06-10 1999-12-15 Asahi Glass Company Ltd. Apparatus for refining molten glass under reduced pressure
US6321572B1 (en) 1998-06-10 2001-11-27 Asahi Glass Company, Ltd. Vacuum degassing apparatus for molten glass
KR100613638B1 (en) * 1998-06-10 2006-08-21 아사히 가라스 가부시키가이샤 Vacuum degassing apparatus for molten glass
US6948338B2 (en) 2001-09-14 2005-09-27 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
US7007514B2 (en) 2001-09-28 2006-03-07 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
US7650764B2 (en) 2001-09-28 2010-01-26 Asahi Glass Company, Limited Vacuum degassing apparatus for molten glass
JP2006298657A (en) * 2005-04-15 2006-11-02 Asahi Glass Co Ltd Vacuum defoaming apparatus of molten glass and method for making molten glass clear by using the same
JP2006327830A (en) * 2005-04-28 2006-12-07 Asahi Glass Co Ltd Glass manufacturing apparatus, its component and method for conducting ohmic heating of the component
JP4561468B2 (en) * 2005-04-28 2010-10-13 旭硝子株式会社 GLASS MANUFACTURING APPARATUS AND ITS COMPONENTS, METHOD FOR ELECTRIC HEATING THE COMPONENTS, AND GLASS MANUFACTURING METHOD
CN115893812A (en) * 2022-10-31 2023-04-04 陕西彩虹工业智能科技有限公司 Auxiliary installation device and installation method for butt welding position material of glass channel

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