JPH09300053A - Production of chromium alloy steel round cast billet - Google Patents

Production of chromium alloy steel round cast billet

Info

Publication number
JPH09300053A
JPH09300053A JP12140696A JP12140696A JPH09300053A JP H09300053 A JPH09300053 A JP H09300053A JP 12140696 A JP12140696 A JP 12140696A JP 12140696 A JP12140696 A JP 12140696A JP H09300053 A JPH09300053 A JP H09300053A
Authority
JP
Japan
Prior art keywords
slab
reduction
round billet
roll
round
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP12140696A
Other languages
Japanese (ja)
Other versions
JP3237518B2 (en
Inventor
Yutaka Tsuchida
裕 土田
Shinichi Nishioka
信一 西岡
Koichi Nomura
光一 野村
Hiroshi Maeda
浩史 前田
Michiou Nakagome
理欧 中込
Tatsuro Katsumura
龍郎 勝村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Engineering Corp
Original Assignee
NKK Corp
Nippon Kokan Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NKK Corp, Nippon Kokan Ltd filed Critical NKK Corp
Priority to JP12140696A priority Critical patent/JP3237518B2/en
Publication of JPH09300053A publication Critical patent/JPH09300053A/en
Application granted granted Critical
Publication of JP3237518B2 publication Critical patent/JP3237518B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

PROBLEM TO BE SOLVED: To produce a continuously round cast billet of a hardly workable alloy steel containing >0.5wt.% Cr improved in center porosity, component segregation at the core part and heat cracking by a conventional continuous casting equipment. SOLUTION: In the continuous casting process, light rolling reduction is applied to the part of the round cast billet 3 at the terminal stage of solidification by rolling reduction rolls 4a. Desirably. It is preferable that an electromagnetic stirring treatment is applied to molten steel 2 in a mold 1, and when the solid phase ratio fs in the core part of the cast billet satisfies 0.1<=fs<1, the rolling reduction is applied thereto in the range of 0.1-3% cross-sectional area reduction ratio in the C direction by the rolling reduction rolls having two or more stages. Further, in this process, it is more preferable that two or more sets of the rolling reduction rolls consisting of two pieces of V type caliver rolls in parallel to each other in the axial line and facing each other are arranged and the light rolling reduction is applied to the cast billet so that the rolling reductional direction of each rolling reduction roll is made different from each other. By this method, the Cr alloy steel round cast billet having sound internal quality can be provided with a simple continuous casting process.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、継目無鋼管用高C
r合金鋼など丸ビレット素材鋳片を連続鋳造にて製造す
る方法に関し、特に、内部品質が健全でセンターポロシ
ティや偏析などがなく、圧延した鋼管に内面疵がなく、
且つ、製管に当たって圧延不良を発生しない外面形状の
良好な丸鋳片を簡便に鋳造する方法に関するものであ
る。
TECHNICAL FIELD The present invention relates to a high C for seamless steel pipe.
Regarding a method for producing a round billet material slab such as r alloy steel by continuous casting, in particular, the internal quality is sound, there is no center porosity and segregation, and the rolled steel pipe has no internal flaws.
In addition, the present invention relates to a method for easily casting a round cast slab having a good outer surface shape that does not cause rolling defects in the pipe production.

【0002】[0002]

【従来技術】継目無鋼管は、一般に、連続鋳造で大断面
角形状のブルーム鋳片を鋳造し、加熱後、分塊圧延、ブ
ルーミングミルおよびビレッティングミル等で断面丸形
状のビレツト(丸ビレット)に熱間圧延した後に製管工
場へ搬送するか、または、連続鋳造機で丸ビレットを鋳
造した後、製管工場へ搬送し、そして、マンネスマン穿
孔もしくはプレス穿孔、または熱間押出し等により中空
素管を製造し、その後エロンゲータ、プラグミルまたは
マンドレルミル等の圧延機で延伸し、最終的にサイザー
およびストレッチレデューサ等により定径して製品とす
る。
2. Description of the Related Art Generally, a seamless steel pipe is produced by continuously casting a bloom slab with a large cross-section square shape, heating it, and then slabbing, blooming and billeting mills with a round cross-section billet (round billet). Hot rolled into a pipe mill or cast into a round billet with a continuous casting machine and then transported to a pipe mill, and then subjected to Mannesmann or press punching, or hot extrusion to produce hollow elements. The pipe is manufactured, then stretched by a rolling machine such as an elongator, a plug mill or a mandrel mill, and finally the diameter is adjusted by a sizer or a stretch reducer to obtain a product.

【0003】一般の低炭素鋼のように連続鋳造にて比較
的容易に鋳造することができ、しかも熱間加工性も良好
な鋳片は、継目無鋼管用の素材として鋳造ままで供給さ
れる。しかしながら、ステンレス鋼などのように、連続
鋳造では鋳片の軸心部に偏析やポロシティが発生し易
く、しかも熱間加工性に劣る鋳片は、大きな加工を加え
た後に供給されることが多い。熱間加工性に劣る鋳片の
場合にこのような工程を経る理由は、素材ビレットが先
ずマンネスマン穿孔という過酷な加工を受けるからであ
り、このような前工程を省略すると、軸心部のポロシテ
ィおよび偏析により管内面に疵が発生するからである。
従って、難加工性材料と呼ばれる鋳片は勿論のこと、炭
素量の多い鋳片およびCrが添加された鋳片について
も、穿孔前の加工が必要であるといわれている。
A slab, which can be cast relatively easily by continuous casting like general low carbon steel and has good hot workability, is supplied as it is as a raw material for a seamless steel pipe. . However, in continuous casting such as stainless steel, segregation and porosity are likely to occur in the axial center of the slab, and the slab with poor hot workability is often supplied after large processing. . The reason why such a step is performed in the case of a cast piece having poor hot workability is that the material billet is first subjected to severe processing such as Mannesmann drilling, and if such a preceding step is omitted, the porosity of the shaft center part is omitted. And segregation causes flaws on the inner surface of the pipe.
Therefore, it is said that not only the slab called a difficult-to-work material, but also the slab with a large amount of carbon and the slab to which Cr is added must be processed before drilling.

【0004】特に、鋳片の内部品質はその後の圧延過程
での製管成績に大きな影響を及ぼす。鋼中のCr含有量
が多くなると、連鋳鋳片の軸心部に偏析およびポロシテ
ィが発生し易く、それが原因で製管工程において継目無
管の内面にうろこ状の表面疵が発生するため、管内面を
手入れして疵を除去しなければならず、製造コストの上
昇を招くだけでなく、欠陥の程度によっては、製品とし
て使用できない。
In particular, the internal quality of the slab has a great influence on the pipe production performance in the subsequent rolling process. If the Cr content in the steel increases, segregation and porosity tend to occur in the axial center of the continuous cast slab, which causes scaly surface flaws on the inner surface of the seamless pipe in the pipe manufacturing process. However, the inner surface of the pipe must be cared for to remove the flaw, which not only increases the manufacturing cost but also cannot be used as a product depending on the degree of defects.

【0005】一般に、連鋳鋳片軸心部の鋳造欠陥は、鋳
片の最終凝固段階における凝固界面形状および凝固収縮
に起因しており、結晶による溶鋼流路の閉塞や溶鋼の粘
性が高い等のために、溶鋼の流動抵抗が大きくなって発
生する。即ち、デンドライト樹間の濃化溶鋼が優先的に
流動すると偏析となり、また溶鋼が鋳片軸心部に十分に
供給されない場合にはポロシティになるとされている。
Generally, the casting defect at the axial center of the continuous cast slab is caused by the solidification interface shape and solidification shrinkage in the final solidification stage of the slab, such as clogging of the molten steel flow path due to crystals and high viscosity of the molten steel. Because of this, the flow resistance of the molten steel becomes large and occurs. That is, it is said that when the concentrated molten steel between dendrite trees preferentially flows, it segregates, and when the molten steel is not sufficiently supplied to the core of the slab, it becomes porosity.

【0006】特にCrを含有する溶鋼では、Cr含有量
の増大につれて溶鋼の粘性が増大し、図7に示すように
Cr含有量が13wt. %前後で最大となる。そこで従来
は、仮に鋳片にポロシティが発生していても分塊圧延に
よりこれを圧着させ、しかる後にビレッティングミルで
丸形状のビレットに加工して、製管用素材として供給し
ていた。更に、この加工と加熱を繰り返す工程で生ずる
成分元素の拡散により、中心偏析も低減されていた。ま
た、鋳片品質の向上を図り製管時の欠陥発生を防止する
ために、連続鋳造機の鋳型に電磁撹拌装置を設置して鋳
型内の溶鋼を撹拌することにより、最終凝固部に十分な
等軸晶帯を形成させ、鋳片の中心偏析およびセンターポ
ロシティの生成を抑制している。
Particularly in the molten steel containing Cr, the viscosity of the molten steel increases as the Cr content increases, and the Cr content reaches a maximum around 13 wt.% As shown in FIG. Therefore, conventionally, even if porosity was generated in the slab, it was pressure-bonded by slabbing, then processed into a round billet with a billeting mill, and supplied as a material for pipe manufacturing. Furthermore, center segregation was also reduced by the diffusion of the constituent elements that occur in the process of repeating this processing and heating. Further, in order to improve the quality of the slab and prevent the occurrence of defects during pipe manufacturing, the electromagnetic stirrer is installed in the mold of the continuous casting machine to stir the molten steel in the mold to ensure that the final solidification part The equiaxed zone is formed to suppress the center segregation and center porosity of the slab.

【0007】また、鋳片の内部品質を向上させる手段と
しては、連続鋳造ラインにおいて鋳片に軽圧下を施す方
法がある。例えば、特開平6−63715号公報は、凝
固末期の鋳片をロールで圧下し、凝固末端領域(クレー
タエンド領域)の濃化溶鋼の流動を抑えることにより中
心偏析を防止する技術(以下、「先行技術1」という)
を開示している。しかしながら先行技術1では、鋳片の
軸心が固液共存状態にある相当長い区間にわたり、圧下
方向が一定になるように多数組の圧下ロールを配置して
いるが、特に重要な因子である圧下ロールの形状や必要
圧下量については開示していない。
As a means for improving the internal quality of the slab, there is a method of subjecting the slab to light reduction in a continuous casting line. For example, Japanese Patent Laid-Open No. 6-63715 discloses a technique for preventing center segregation by rolling down a slab in the final stage of solidification with a roll to suppress the flow of concentrated molten steel in the solidification end region (crater end region) (hereinafter, referred to as “ Prior art 1 ")
Is disclosed. However, in Prior Art 1, a large number of sets of reduction rolls are arranged so that the reduction direction is constant over a considerably long section in which the shaft center of the cast slab is in a solid-liquid coexisting state. It does not disclose the shape of the roll or the required amount of reduction.

【0008】「材料とプロセス」vol.7(1994)No.1.p.19
4 〜197 は、丸ブルーム鋳片を未凝固状態で2段で圧下
する方法を、ステンレス鋼SUS410に適用する技術(以
下、「先行技術2」という)について開示している。し
かしながら、先行技術2では、マクロ腐食試験結果にお
いて若干のポロシティの残存が認められる。また、得ら
れた鋳片の軸心密度は7.7であり、ポロシティの発生
していないときの密度7.8には及ばず、完全にはポロ
シティを圧着するに至っていない。
"Materials and Processes" vol.7 (1994) No.1.p.19
Nos. 4 to 197 disclose a technique (hereinafter, referred to as "prior art 2") of applying a method of rolling a round bloom slab in two stages in an unsolidified state to stainless steel SUS410. However, in Prior Art 2, some porosity remains in the macro corrosion test results. Moreover, the axial density of the obtained cast piece was 7.7, which did not reach the density 7.8 when porosity was not generated, and the porosity was not completely pressed.

【0009】「材料とプロセス」vol .7(1994)No.1.p.
179 〜182 は、C含有量0.4〜0.6wt. %の連鋳ブ
ルームの中心偏析を改善するために、凝固末期の鋳片を
金型に押し込み、連続的に大圧下をする鍛圧法(以下、
「先行技術3」という)を開示している。しかしながら
先行技術3では、1段で一気に、かつ未凝固液相を絞り
出すほど過剰に圧下することを特徴としているため、セ
ンターポロシティの消滅に対しては優れているが、鋳片
の軸心部は負偏析を呈している。
“Materials and Processes” vol. 7 (1994) No.1.p.
Nos. 179 to 182 are the forging method in which the slab in the final stage of solidification is pushed into the mold to continuously reduce the steel in order to improve the center segregation of the continuous casting bloom having a C content of 0.4 to 0.6 wt.%. (Less than,
"Prior Art 3") is disclosed. However, the prior art 3 is characterized in that the pressure is excessively reduced by squeezing the uncoagulated liquid phase in one step at a stretch, and therefore it is excellent in eliminating the center porosity, but the axial center portion of the slab is It exhibits negative segregation.

【0010】[0010]

【発明が解決しようとする課題】鋳片軸心部のポロシテ
ィや成分偏析を分塊圧延にて改善する工程を経る場合に
は、これに対するコストが加わる。また、上述した各先
行技術には、それぞれ下記の問題点がある。
When the process of improving the porosity and the component segregation of the core of the cast slab by the slabbing process, a cost is added. Further, each of the above-mentioned prior arts has the following problems.

【0011】先行技術1は、鋳片の中心偏析改善には効
果的であるが、軽圧下ロールを鋳造ラインの長い区間に
わたって同一圧下方向になるように設置しているため、
フラット形状のロールを使用した場合には、丸鋳片は変
形して楕円形状となってしまい、そのままの形状では製
管することができないという難点を有する。また、鋳片
に加える圧下量の大きさや圧下方向によっては、内部に
割れが発生する。
Prior art 1 is effective for improving the center segregation of the slab, but since the light reduction rolls are installed in the same reduction direction over a long section of the casting line,
When a flat roll is used, the round slab is deformed into an elliptical shape, and there is a problem in that it cannot be manufactured as it is. In addition, cracks may occur inside depending on the amount of reduction applied to the slab and the direction of reduction.

【0012】先行技術2は、軸心部の凝固組織の改善に
は効果的であるが、前述したように、センターポロシテ
ィの消滅には不十分である。また、先行技術3は、ポロ
シティの圧着には優れたプロセスであるが、鋳片の軸心
部に負偏析領域が形成されるので、成分の均一性が厳し
く問われ、管の内面腐食が問題となる継目無鋼管用素材
としては適用することができない。
The prior art 2 is effective in improving the solidification structure of the shaft center portion, but is insufficient for eliminating the center porosity as described above. Further, the prior art 3 is an excellent process for pressure bonding of porosity, but since a negative segregation region is formed in the axial center portion of the slab, the uniformity of the components is strictly demanded and the inner surface corrosion of the pipe is a problem. It cannot be applied as a material for seamless steel pipes.

【0013】従って、この発明の目的は、上述した問題
点を解決することにより、特に、内面疵や製管不良の発
生しない継目無管用素材として、鋳片軸心部の品質が優
れた丸ビレツト鋳片を、連続鋳造にて製造する方法を提
供することにある。
Therefore, an object of the present invention is to solve the above-mentioned problems, and in particular, as a material for a seamless pipe which does not cause inner surface flaws or defective pipe making, a round billet having an excellent core portion of a cast slab. It is to provide a method for producing a slab by continuous casting.

【0014】[0014]

【課題を解決するための手段】本発明者らは、上述の実
情に鑑み、安価で簡便な設備により、内質の健全な鋳片
を製造する技術の研究を重ね、次の方法を開発した。
SUMMARY OF THE INVENTION In view of the above-mentioned circumstances, the inventors of the present invention have conducted extensive research into a technique for producing a cast slab having a good internal quality with inexpensive and simple equipment, and have developed the following method. .

【0015】請求項1記載のクロム合金鋼丸ビレット鋳
片の製造方法は、Cr含有量が0.5wt.%を超えるCr
合金鋼を直径340mm以下の丸形状鋳型により連続鋳造
し、得られた丸ビレット鋳片の凝固末期の部分に圧下ロ
ールで軽圧下を加えることに特徴を有するものである。
In the method for producing a chromium alloy steel round billet slab according to claim 1, the Cr content is more than 0.5 wt.% Cr.
It is characterized in that alloy steel is continuously cast by a round mold having a diameter of 340 mm or less, and light reduction is applied by a reduction roll to the final solidification portion of the obtained round billet slab.

【0016】請求項2記載のクロム合金鋼丸ビレット鋳
片の製造方法は、請求項1記載の丸ビレット鋳片の製造
方法に更に、丸形状鋳型内において溶鋼に対して電磁撹
拌処理を行なうことを付加し、そして、上記圧下ロール
による丸ビレット鋳片の軽圧下を2段以上の圧下ロール
で行なうこととし、しかも丸ビレット鋳片の軸心固相率
fs が0.1≦fs <1を満たす時期に、C方向断面積
減少率が0.1〜3%の範囲内の圧下を加えることに特
徴を有するものである。
The method for producing a round billet slab of chromium alloy steel according to a second aspect is the method for producing a round billet slab according to the first aspect, further comprising performing electromagnetic stirring treatment on molten steel in a round mold. And the light reduction of the round billet slab by the reduction roll is performed by two or more reduction slabs, and the axial solid phase ratio fs of the round billet slab is 0.1 ≦ fs <1. It is characterized in that a reduction in the C-direction cross-sectional area reduction rate within the range of 0.1 to 3% is applied at the time of filling.

【0017】請求項3記載のクロム合金鋼丸ビレット鋳
片の製造方法は、請求項1または2記載の鋳片の製造方
法において、上記軽圧下方法として、軸線が互いに平行
で且つ丸ビレット鋳片を中間にして両側に対向する2個
のV型カリバーロールからなる圧下ロールを、丸ビレッ
ト鋳片の鋳造方向に沿って2基以上配置し、各圧下ロー
ルによる丸ビレット鋳片に対する各圧下方向が互いに異
なる方向に凝固末期の丸ビレット鋳片を圧下することに
特徴を有するものである。
A method for producing a round billet slab of chromium alloy steel according to a third aspect is the method for producing a slab according to the first or second aspect, wherein as the light reduction method, the axes are parallel to each other and the round billet slab is formed. Two or more reduction rolls made up of two V-type caliber rolls facing each other with the middle being the middle are arranged along the casting direction of the round billet slab, and the reduction directions of the round billet slabs by the respective reduction rolls are It is characterized by rolling down round billet slabs in the final stage of solidification in different directions.

【0018】[0018]

【発明の実施の形態】以下に、この発明の実施の形態に
ついて説明する。請求項1記載の発明の実施態様につい
て説明する。
Embodiments of the present invention will be described below. An embodiment of the invention described in claim 1 will be described.

【0019】図1は、請求項1記載の発明の一実施態様
を説明するための連続鋳造工程の縦断面概念図である。
1は丸形状鋳型、2は溶鋼、3は未凝固鋳片、3’は完
全凝固後の丸ビレット鋳片、4aは一段の圧下ロール、
5は鋳片凝固末期の固液共存相、6はガイドロール群、
そして7は引き抜きロールである。
FIG. 1 is a vertical cross-sectional conceptual view of a continuous casting process for explaining an embodiment of the invention described in claim 1.
1 is a round-shaped mold, 2 is molten steel, 3 is an unsolidified slab, 3'is a fully solidified round billet slab, 4a is a single-stage reduction roll,
5 is a solid-liquid coexisting phase at the final stage of solidification of the slab, 6 is a guide roll group,
And 7 is a drawing roll.

【0020】図1に示すように、転炉(図示せず)から
出鋼されたCr:0.5wt.%超えを含有する溶鋼2を、
直径340mm以下の丸形状鋳型1により連続鋳造し、得
られた未凝固丸ビレット鋳片3の凝固末期の部分に1段
の圧下ロール4aからなる圧下装置4で軽圧下を加える
ことにより鋳片の内質、特に鋳片軸心部のポロシティや
成分偏析が改善された丸ビレット鋳片3’を製造する。
As shown in FIG. 1, molten steel 2 containing Cr: 0.5 wt.% Or more, which was tapped from a converter (not shown),
Continuous casting using a round-shaped mold 1 having a diameter of 340 mm or less, and a light reduction is applied to a final solidification portion of the obtained unsolidified round billet slab 3 by a reduction device 4 consisting of a single stage of reduction roll 4a to form a slab. A round billet cast slab 3'in which the porosity of the core of the cast slab and especially the segregation of the components is improved is produced.

【0021】連続鋳造により直径340mm以下の丸ビ
レット鋳片3’を鋳造する場合には、鋳片軸心の最終凝
固部近傍では冷却速度が急激に大きくなり凝固が加速的
に進行し、Cr合金鋼ではCr含有量が増加すると溶鋼
の粘性が増大し、ポロシティが生成しやすくなる。本発
明者等の試験結果によれば、Cr含有量が0.5wt.%を
超えるとセンターポロシティが発生し易く、またCrの
偏析によりδフェライト相が生成する。更に熱応力によ
る放射状の割れを誘発する。そして、これらが原因とな
って継目無鋼管の内面疵発生頻度が高くなる。継目無鋼
管のかかる内面疵発生を防止するため、穿孔圧延工程に
先立つ所定の丸ビレット3’を連続鋳造する工程中、鋳
片軸心部に固液共存相5が存在する凝固末期の未凝固丸
ビレット鋳片3に、圧下ロール4aで軽圧下を付与する
ことにより中心偏析やセンターポロシティを消滅させ
る。軽圧下手段としてロールを用いるのは、簡便だから
である。上記製造方法により得られたクロム合金鋼丸ビ
レット鋳片は製管工場へ搬送され、所定の工程を経て継
目無鋼管に製造される。
When a round billet slab 3'having a diameter of 340 mm or less is cast by continuous casting, the cooling rate rapidly increases in the vicinity of the final solidification portion of the slab axis, solidification proceeds rapidly, and the Cr alloy In steel, when the Cr content increases, the viscosity of molten steel increases and porosity is likely to occur. According to the test results of the present inventors, when the Cr content exceeds 0.5 wt.%, Center porosity is likely to occur, and segregation of Cr produces a δ ferrite phase. Furthermore, it induces radial cracks due to thermal stress. Due to these factors, the frequency of occurrence of internal flaws in the seamless steel pipe increases. In order to prevent the occurrence of such internal flaws in the seamless steel pipe, during the process of continuously casting the predetermined round billet 3'prior to the piercing and rolling process, the solid-liquid coexisting phase 5 is present in the core of the cast slab, which is not solidified at the end of solidification. By applying a light reduction to the round billet slab 3 with a reduction roll 4a, center segregation and center porosity are eliminated. The reason why the roll is used as the light rolling means is simple. The chromium alloy steel round billet slab obtained by the above-mentioned manufacturing method is transported to a pipe manufacturing factory and manufactured into a seamless steel pipe through a predetermined process.

【0022】上述した本発明法を用いれば、従来法のよ
うに大断面の連鋳鋳片を製造し更に熱間圧延された丸ビ
レットではなく、小断面の丸ビレット連鋳鋳片を直接、
中空素管の素材として供給することができるので、製造
コストの低減にも寄与する。
By using the above-described method of the present invention, a continuous billet having a small cross section is directly produced instead of a round billet having a large cross section continuously cast and hot-rolled as in the conventional method.
Since it can be supplied as a material for the hollow shell, it also contributes to a reduction in manufacturing cost.

【0023】請求項2記載の発明の実施態様について説
明する。図2は、請求項2記載の発明の一実施態様を説
明するための連続鋳造工程の縦断面概念図である。4は
圧下装置であって2段の圧下ロール4b,4cからな
り、8は鋳型内電磁撹拌装置であり、そしてその他の記
号は図1と同じである。
An embodiment of the invention described in claim 2 will be described. FIG. 2 is a vertical sectional conceptual view of a continuous casting process for explaining an embodiment of the invention described in claim 2. Reference numeral 4 is a reduction device, which is composed of two-stage reduction rolls 4b and 4c, 8 is an in-mold electromagnetic stirring device, and other symbols are the same as those in FIG.

【0024】この実施態様例は、図2に示すように、請
求項1記載発明の上記実施態様例に対して更に鋳型内電
磁撹拌装置8を用いて連続鋳造中の溶鋼2を電磁撹拌す
ることを付加し、また、未凝固丸ビレット鋳片3の凝固
末期の部分に対する軽圧下方法として、鋳片の軸心固相
率fsが0.1≦fs<1の時期に2段の圧下ロール4
b,4cからなる圧下装置4で、C方向断面積減少率が
0.1〜3%の範囲内の圧下を加えることとするもので
ある。
In this embodiment, as shown in FIG. 2, the molten steel 2 being continuously cast is electromagnetically stirred by using an in-mold electromagnetic stirring device 8 in addition to the above embodiment of the invention of claim 1. In addition, as a light reduction method for the final solidification portion of the unsolidified round billet slab 3, a two-stage reduction roll 4 is used when the axial solid fraction fs of the slab is 0.1 ≦ fs <1.
The reduction device 4 composed of b and 4c applies reduction in the C-direction cross-sectional area reduction rate of 0.1 to 3%.

【0025】鋳型内溶鋼に電磁撹拌を付与することによ
り鋳片軸心部に等軸晶を生成させる作用を有し、その後
に行なう軽圧下によるV偏析の抑制およびセンターポロ
シティの消滅を一層効果的にする。
By imparting electromagnetic stirring to the molten steel in the mold, it has the effect of producing equiaxed crystals in the axial center of the slab, and is more effective in suppressing V segregation and eliminating center porosity due to subsequent light reduction. To

【0026】未凝固丸ビレット鋳片3の凝固末期の部分
に対する軽圧下条件中、鋳片の軸心固相率fsは、本発
明の適用にあたっては最も重要な要素である。V偏析が
発生し成長するに至るのは0.1≦fs≦0.5の時期
であり、この間に少なくとも1段目の軽圧下を加えるこ
とにより濃化溶鋼の流動を抑え、偏析チャンネルの形成
を防止することが望ましい。また、鋳片の軸心固相率f
sが0.5以下の時期にのみ圧下を付与した場合には、
一旦軽圧下をしてもその後の凝固収縮によりポロシティ
が形成されたり、熱応力による放射状割れが発生し易
い。
The axial solid fraction fs of the slab is the most important factor in the application of the present invention under the condition of light reduction to the final solidification portion of the unsolidified round billet slab 3. V segregation occurs and starts to grow at a time of 0.1 ≦ fs ≦ 0.5, and by applying at least the first stage of light reduction during this time, the flow of the concentrated molten steel is suppressed to form a segregation channel. It is desirable to prevent In addition, the axial solid fraction f of the slab
When the reduction is applied only when s is 0.5 or less,
Even after a slight reduction in pressure, porosity is likely to be formed due to subsequent solidification shrinkage, and radial cracks due to thermal stress are likely to occur.

【0027】一方、鋳片の軸心固相率fsが1未満、即
ち完全凝固せずに液相が存在する時期であれば、ポロシ
ティや割れの発生を抑制することができ、あるいは発生
した欠陥の圧着が可能である。従って、最終段の軽圧
下、但し本実施態様例では2段目軽圧下は鋳片の軸心固
相率fsが1未満の時期に行なえばよい。
On the other hand, if the axial solid fraction fs of the cast slab is less than 1, that is, when the liquid phase is present without complete solidification, porosity and cracking can be suppressed, or defects that have occurred. Crimping is possible. Therefore, the final stage of light reduction, but in the present embodiment, the second stage of light reduction may be performed at a time when the axial solid fraction fs of the cast slab is less than 1.

【0028】鋳片の軽圧下法については、上述した鋳片
の軸心固相率条件に加え、鋳片C方向断面積の減少率を
限定するにより、軸心部のV偏析の抑制、ポロシティの
形成抑制および圧着、並びに放射状割れの発生抑制およ
び圧着に対して効果を発揮する。鋳片C方向断面積減少
率が0.1%以下ではV偏析の発生を抑制することは可
能であるが、ポロシティや放射状割れを低減することは
できない。一方、C方向断面積減少率が3%を超える圧
下を加えると、ポロシティや熱応力割れを低減すること
はできるが、濃化溶鋼の絞り出しによる濃厚偏析が形成
されたり、圧下に伴なう変形に起因して鋳片内部に割れ
が発生し、製管時の管内面疵の発生原因となる。
Regarding the light reduction method of the cast slab, in addition to the above-mentioned solid phase ratio condition of the cast slab, the reduction rate of the cross-sectional area of the cast slab in the C direction is limited to suppress the V segregation of the shaft center portion and the porosity. It is effective in suppressing the formation and crimping, and suppressing the generation of radial cracks and crimping. When the reduction rate of the sectional area of the cast slab in the C direction is 0.1% or less, the occurrence of V segregation can be suppressed, but porosity and radial cracking cannot be reduced. On the other hand, porosity and thermal stress cracking can be reduced by applying a reduction whose cross-sectional area reduction rate in the C direction exceeds 3%, but thick segregation is formed due to squeezing of the concentrated molten steel, and deformation accompanying the reduction is also possible. This causes cracks inside the slab, which causes defects on the inner surface of the pipe during pipe manufacturing.

【0029】請求項3記載の発明の実施態様について説
明する。この実施態様例は、請求項1または2記載発明
の上記実施態様例において、鋳片凝固末期の部分を軽圧
下する場合に、圧下ロールとして軸線が互いに平行で且
つ鋳片を中間にして両側に向き合った2個のV型カリバ
ーロールを1組として少なくとも2組、この場合には2
組を鋳造方向に沿って2基配置し、即ち2段に配置し、
しかも上記圧下ロールによる鋳片の圧下方向を互いに異
なる方向、例えば、直角方向になるように配置し、鋳片
に対して所定の軽圧下を施すこととするものである。
An embodiment of the invention described in claim 3 will be described. In the embodiment example of the invention according to claim 1 or 2, when the part at the final stage of solidification of the slab is lightly reduced, this embodiment is a rolling roll whose axes are parallel to each other and the slab is in the middle. At least two sets of two facing V-type caliber rolls, in this case 2 sets
Two sets are arranged along the casting direction, that is, two sets are arranged,
Moreover, the slabs are arranged such that the slabs are pressed in different directions, for example, at right angles, and the slabs are subjected to a predetermined light reduction.

【0030】圧下ロールの形状としてV型カリバーロー
ルを採用し、しかも対向する2個のロールを1対とした
のは、ロールによる圧力を鋳片の軸心部に効率よく集中
させることにより鋳造欠陥の発生を確実に防止するため
である。また、各段の圧下ロールによる圧下方向を鋳片
C方向断面内の互いに異なる方向、例えば、2段に配置
された圧下ロールで互いに直角方向に圧下を加えること
としたのは、特定方向への偏った変形を防止し、鋳片の
外形を真円に近い形状とするためである。例えば、フラ
ットロールで平面的な圧下を一定方向に加えると、丸ビ
レット鋳片は楕円形状に変形し、製管時に芯振れを生じ
て管厚が偏肉したり、場合によっては圧延不可能とな
る。また、変形した丸ビレット鋳片をピーリング加工し
て真円化することもできるが、コストが上昇する。
A V-type caliber roll was adopted as the shape of the reduction roll, and two opposing rolls were made into a pair so that the pressure caused by the rolls was efficiently concentrated at the axial center of the cast slab, resulting in a casting defect. This is for surely preventing the occurrence of. Further, the reduction direction by the reduction rolls in each stage is different from each other in the slab C direction cross section, for example, the reduction rolls arranged in two stages apply reductions in the directions perpendicular to each other. This is because uneven deformation is prevented and the outer shape of the cast slab has a shape close to a perfect circle. For example, when flat rolling is applied in a certain direction with a flat roll, the round billet slab is deformed into an elliptical shape, causing core runout during pipe production, resulting in uneven thickness of the pipe, and in some cases it is impossible to roll. Become. Further, the deformed round billet slab can be peeled into a perfect circle, but the cost is increased.

【0031】上述した本発明方法により、従来よりも簡
便な方法で内質が健全な丸ビレット鋳片を得ることがで
き、これを素材として従来と全く変わらない製管法を用
いてより製造コストが低く、且つ製管上の問題が発生せ
ず、しかも管内面疵が発生しない高級継目無鋼管を製造
することが可能となる。
The above-described method of the present invention makes it possible to obtain a round billet slab having a good internal quality by a simpler method than the conventional method, and using this as a raw material, a pipe manufacturing method which is completely the same as the conventional method can be used to further reduce the manufacturing cost. It is possible to manufacture a high-grade seamless steel pipe which has a low pipe temperature, does not cause problems in pipe manufacturing, and has no inner surface defects.

【0032】[0032]

【実施例】次に、この発明を実施例により、更に詳細に
説明する。図2に示した鋳型内電磁撹拌装置8、および
2段の圧下ロール4b,4cからなる圧下装置4を有す
る半径11.5mの湾曲型ビレット用連続鋳造機によ
り、鋳片断面径170mmまたは330mmの丸形状鋳型に
Cr含有量が2.5wt.%または13.8wt.%の継目無鋼
管向けCr合金溶鋼を鋳造し、丸ビレット鋳片を製造し
た。凝固末期鋳片の軽圧下はフラットロールによる2段
圧下、または、カリバーロールによる1段圧下もしくは
2段圧下で行なった。次いで、鋳片を所定温度に加熱
し、マンネスマン穿孔機で圧延して中空粗管を製造し、
エロンゲータで延伸後、サイザーで定径して継目無鋼管
を製造した。
Next, the present invention will be described in more detail with reference to examples. With the electromagnetic stirrer in the mold 8 shown in FIG. 2 and the continuous casting machine for a curved billet having a radius of 11.5 m, which has the rolling down device 4 including the two-stage rolling down rolls 4b and 4c, the slab cross-section diameter of 170 mm or 330 mm is obtained. A round billet slab was produced by casting a molten Cr alloy steel for a seamless steel pipe having a Cr content of 2.5 wt.% Or 13.8 wt.% In a round mold. The light reduction of the final solidification slab was performed by two-stage reduction by a flat roll, or one-stage or two-stage reduction by a caliber roll. Then, the slab is heated to a predetermined temperature, rolled with a Mannesmann punch to produce a hollow rough tube,
After stretching with an elongator, the diameter was adjusted with a sizer to produce a seamless steel pipe.

【0033】図3〜5は、凝固末期の鋳片に軽圧下を付
与する圧下ロールの配置および構成を示す概略図であっ
て、V型カリバーロールからなる圧下ロールの鋳片に対
する配置を示し、図3は側面概略図、図4は図3のA−
A線断面図、そして図5は図3のB−B線断面図であ
る。これらの図に示すように、未凝固鋳片3に接するV
型カリバー部を角度θ=90°に切った2個のカリバー
ロール9a,9a’、および、9b,9b’を組み合わ
せて1組の圧下ロールとし、それぞれを1段目圧下ロー
ル4bおよび2段目圧下ロール4cとした。そして1段
目圧下ロール4bと2段目圧下ロール4cとのロール相
互間の傾斜角度を直角とした。
3 to 5 are schematic views showing the arrangement and configuration of a reduction roll for imparting a light reduction to the slab in the final stage of solidification, showing the arrangement of the reduction roll consisting of a V-type caliber roll with respect to the slab. 3 is a schematic side view, and FIG. 4 is A- of FIG.
A line sectional view, and FIG. 5 is a BB line sectional view of FIG. As shown in these figures, V contacting the unsolidified slab 3
Two caliber rolls 9a, 9a 'and 9b, 9b' in which the die caliber portion is cut at an angle of θ = 90 ° are combined to form one set of reduction rolls, which are the first-stage reduction roll 4b and the second-stage reduction roll, respectively. The reduction roll 4c was used. The inclination angle between the first-stage reduction roll 4b and the second-stage reduction roll 4c was set to a right angle.

【0034】表1および2に、本発明の範囲内の製造方
法である実施例1〜12、および、本発明の範囲外の製
造方法である比較例1〜3を示す。
Tables 1 and 2 show Examples 1 to 12 which are manufacturing methods within the scope of the present invention, and Comparative Examples 1 to 3 which are manufacturing methods outside the scope of the present invention.

【0035】[0035]

【表1】 [Table 1]

【0036】[0036]

【表2】 [Table 2]

【0037】鋳造された化学成分組成の溶鋼は、実施例
および比較例のいずれにおいても鋳片軸心の偏析および
ポロシティを形成し易く、しかも難加工性の鋼種であ
る。注湯温度は溶鋼の化学成分組成に応じた常法の温度
とし、設置した電磁撹拌装置にて鋳型内で溶鋼を撹拌
(但し、実施例12を除く)しつつ鋳造した。また、鋳
片の冷却水量も溶鋼の化学成分組成や鋳片サイズに応じ
た適正な量とした。
The cast molten steel having the chemical composition is a steel type which is liable to form segregation and porosity of the slab axis in each of the examples and comparative examples, and which is difficult to work. The pouring temperature was set to a temperature according to a conventional method depending on the chemical composition of the molten steel, and the molten steel was cast in the mold by an installed electromagnetic stirring device while stirring (excluding Example 12). The amount of cooling water for the slab was also an appropriate amount according to the chemical composition of the molten steel and the slab size.

【0038】凝固末期の未凝固鋳片3に対して軽圧下を
付与するための圧下ロール4b,4cの径は380mm
で、圧下方式は油圧式とした。各圧下ロール4b,4c
の設置位置は、鋳型内溶鋼2のメニスカスからそれぞれ
15.5mおよび17.5mの位置とし、溶鋼組成や鋳
片径等が鋳造No.間で異なっていても、鋳造速度を調整
することにより鋳片の軸心固相率fsを任意に選定する
ことができるようにした。
The diameter of the pressing rolls 4b and 4c for imparting a light reduction to the unsolidified slab 3 at the final stage of solidification is 380 mm.
Therefore, the rolling-down method was hydraulic. Each rolling roll 4b, 4c
The installation positions of the molten steel 2 in the mold are 15.5 m and 17.5 m from the meniscus of the molten steel 2, respectively. Even if they differ from each other, the axial solid fraction fs of the slab can be arbitrarily selected by adjusting the casting speed.

【0039】鋳造終了後、丸ビレット鋳片から所定の試
験片を採取し、鋳片軸心部のポロシティ、割れおよびV
偏析などの鋳片内質特性試験を行なった。次いで製管
後、継目無鋼管の内面疵発生状況を観察し、鋳片内質を
総合的に評価した。
After completion of casting, a predetermined test piece was sampled from the round billet slab, and porosity, cracks and V
A cast internal property test such as segregation was performed. Then, after the pipe was manufactured, the state of occurrence of internal flaws in the seamless steel pipe was observed, and the quality of the cast slab was comprehensively evaluated.

【0040】〔鋳片のセンターポロシティ試験〕鋳片の
軸心を通るL方向断面の長さ500mmの試片3枚につ
き、機械研削ままでの目視観察、および浸透探傷試験
(PT)を実施し、試片長さに対するポロシティ分布総
長さの比でセンターポロシティを評価した。ポロシティ
指数1は、ポロシティ性欠陥を検出できなかったもの
で、指数が小さいほど優れていることを表わす。
[Center porosity test of slab] Three specimens each having a length of 500 mm in a cross section passing through the axis of the slab and having a length of 500 mm were subjected to visual observation under mechanical grinding and a penetrant flaw detection test (PT). The center porosity was evaluated by the ratio of the total length of porosity distribution to the sample length. A porosity index of 1 indicates that a porosity defect could not be detected, and the smaller the index, the better.

【0041】〔鋳片割れ、およびV偏析顕出試験〕鋳片
のC方向断面試片1枚と、ポロシティ試験を実施後のL
方向断面の長さ500mmの試片3枚につき、塩酸マク
ロ腐食試験により割れおよびV偏析を顕出した。そし
て、目視にて欠陥の径および長さを測定し、径と長さの
積に基づき割れおよびV偏析を評価した。割れおよびV
偏析の指数1はいずれもこれらの欠陥発見できなかった
ことを意味し、指数が小さいほど優れていることを表わ
す。
[Breaking of slab and V segregation revealing test] One piece of a C-section cross section of the slab and L after carrying out the porosity test
Cracking and V segregation were revealed by a hydrochloric acid macro-corrosion test for three test pieces each having a cross section of 500 mm in length. Then, the diameter and the length of the defect were visually measured, and the crack and the V segregation were evaluated based on the product of the diameter and the length. Crack and V
A segregation index of 1 means that none of these defects could be found, and the smaller the index, the better.

【0042】〔管内面評価試験〕鋳造された丸ビレット
鋳片を1100〜1300℃の間の所定温度に加熱し、
マンネスマン穿孔機で圧延して中空素管を製造し、エロ
ンゲーターで延伸後、サイザーで定径して継目無鋼管を
製造した。そして、鋼管の内面疵の発生状況と程度を検
査し、管内面評価試験とした。素材となる鋳片の内質を
総合的に評価し得る指標でもあり、評点が小さいほど内
質が優れており、評点1は欠陥のないもの、評点2は欠
陥が極く軽微で合格のもの、評点3は欠陥は軽微だが手
入れを要するもの、そして評点4は大きな欠陥が発生し
た不合格のものを表わす。
[Inner surface evaluation test] The cast round billet slab is heated to a predetermined temperature between 1100 and 1300 ° C,
A hollow shell was manufactured by rolling with a Mannesmann piercing machine, stretched with an elongator, and then sized with a sizer to manufacture a seamless steel tube. Then, the occurrence state and degree of inner surface flaws of the steel pipe were inspected, and the inner surface of the pipe was evaluated. It is also an index that can comprehensively evaluate the internal quality of the slab used as the raw material, and the smaller the score, the better the internal quality, with a score of 1 having no defects, and a score of 2 having very few defects and passing. A score of 3 indicates that the defect is slight but requires maintenance, and a score of 4 indicates that the defect is large and is not accepted.

【0043】以上の試験結果を、表1および2に併記し
た。この試験結果から下記事項がわかる。 軽圧下を付与しなかった比較例1および3は、ポロシ
ティ指数、割れ指数およびV偏析指数の鋳片内質特性全
般にわたり劣っており、管内面評点においても劣ってい
る。
The above test results are also shown in Tables 1 and 2. The following items can be understood from the test results. Comparative Examples 1 and 3 to which light reduction was not applied are inferior in overall porosity index, cracking index, and V segregation index in-cast property, and inferior in pipe inner surface score.

【0044】鋳片の軸心部が完全凝固後に軽圧下をし
た比較例2は、圧下を付与した時期に液相が存在しなか
ったため、鋳片内質は殆んど改善されず、その結果とし
て管内面評点において劣っている。
In Comparative Example 2 in which the axial center portion of the cast slab was lightly reduced after complete solidification, since the liquid phase did not exist at the time of applying the reduction, the internal quality of the slab was hardly improved. As a result, it is inferior in the internal rating.

【0045】このように、比較例はいずれも鋳片内質評
点の少なくとも一つにおいて劣っている。これに対し
て、本発明法による実施例1〜12は、鋳片内質評点の
全てにおいて優れているか、またはその評点全般にわた
り比較的優れている。
As described above, all of the comparative examples are inferior in at least one of the cast slab internal quality scores. On the other hand, Examples 1 to 12 according to the method of the present invention are excellent in all of the slab internal quality scores, or relatively excellent in all the scores.

【0046】鋳型内で溶鋼の電磁撹拌を行わなかった
が、凝固末期において軽圧下を付与した実施例12、並
びに、鋳型内での溶鋼電磁撹拌および凝固末期における
軽圧下付与共に行なったがフラットロールで軽圧下した
実施例1は、凝固末期に軽圧下を付与しなかった比較例
1および3よりも、鋳片内質特性および管内面評点共に
若干改善されている。
Example 12 in which the molten steel was not electromagnetically stirred in the mold but light reduction was applied in the final stage of solidification, and the electromagnetic stirring of molten steel in the mold and light reduction in the final stage of solidification were also performed, but a flat roll was used. In Example 1, which was lightly reduced in Example 2, both the slab internal properties and the tube inner surface rating were slightly improved, as compared with Comparative Examples 1 and 3 in which light reduction was not applied at the final stage of solidification.

【0047】V型カリバーロールによりC方向断面積
減少率が0.1〜3%の範囲内の軽圧下を軸心固相率f
sが0.1≦fs <1を満たす時期に付与しても、1段
目圧下ロールまたは2段目圧下ロールだけによる1段軽
圧下を行なった実施例2または3は、鋳片内質特性の3
指数のいずれかにおいては改善されているが、管内面評
点においてはなおも改善の余地がある。
With the V-type caliber roll, the axial center solid phase fraction f is obtained by reducing the cross-sectional area in the C direction in the range of 0.1 to 3% at a light reduction.
Even if it is applied when s satisfies 0.1 ≦ fs <1, Example 2 or 3 in which the first-stage reduction roll or the second-stage reduction roll is used to perform the first-stage light reduction is the internal property of the slab. Of 3
Although there is an improvement in any of the indices, there is still room for improvement in the in-pipe score.

【0048】V型カリバーロールにより軸心固相率f
sが0.1≦fs <1を満たす時期に2段軽圧下を行な
ったが、2段目圧下時のfsが小さ目であった(fs=
0.44)実施例5、および、C方向断面減少率が大き
目であった(3.32%)実施例11は共に、鋳片内質
特性の3指数および管内面疵評点において改善の余地が
ある。
Axial solid fraction f by V-type caliber roll
Two-stage light reduction was performed when s satisfied 0.1 ≦ fs <1, but fs at the second-stage reduction was small (fs =
0.44) In both Example 5 and Example 11 in which the C-direction cross-section reduction rate was large (3.32%), there was room for improvement in the 3 index of cast piece internal quality characteristics and the pipe inner surface flaw rating. is there.

【0049】上述した実施例に対して、実施例4、
6、7、8、9および10はいずれも、V型カリバーロ
ールにより軸心固相率fsが0.1≦fs <1を満たす
時期に2段軽圧下を行ない、且つ1段目軽圧下を軸心固
相率fsが0.1≦fs≦0.5の時期に、2段目軽圧
下を0.5<fsの時期に行ない、しかもC方向断面積
減少率が0.1〜3%の範囲内にあった場合であり、鋳
片内質特性の3指数および管内面疵評点共に、一段と優
れている。
In contrast to the above embodiment, the fourth embodiment,
All of 6, 7, 8, 9 and 10 are subjected to the second stage light reduction at the time when the axial solid fraction fs satisfies 0.1 ≦ fs <1 by the V-type caliber roll, and the first stage light reduction is performed. When the axial solid fraction fs is 0.1 ≦ fs ≦ 0.5, the second stage light reduction is performed at 0.5 <fs, and the C-direction cross-sectional area reduction rate is 0.1 to 3%. It was in the range of, and both the 3 index of the slab internal property and the tube inner surface flaw rating were further excellent.

【0050】上述した結果に基づき、凝固末期の鋳片に
対して1段軽圧下または2段軽圧下を付与した場合の、
ポロシティ指数、割れ指数およびV偏析指数に及ぼす軽
圧下付与時の軸心固相率fsの影響の概念図を、図6に
示した。同図より、1段軽圧下の場合は軸心固相率fs
が、ポロシティ指数は0.5≦fs<1の時期に、割れ
指数は0.7≦fs<1の時期に、そしてV偏析指数は
0.1≦fs≦0.5の時期に軽圧下を付与する場合に
のみ改善効果が発揮されることがわかった。しかしなが
ら、この場合には、個々の指数について単独に改善効果
が現れているに過ぎない。これに対して、管内面の健全
性を満足する評点が得られる本発明の各請求項の範囲内
の条件、特に、請求項3の範囲内の条件によれば、鋳片
内質特性の3指数を同時に改善し得ることがわかる。
On the basis of the above-mentioned results, when one-stage light reduction or two-stage light reduction is applied to the slab in the final stage of solidification,
FIG. 6 is a conceptual diagram showing the effect of the axial solid fraction fs at the time of applying a light reduction on the porosity index, cracking index and V segregation index. From the figure, the axial solid fraction fs in the case of one-step light pressure
However, when the porosity index is 0.5 ≦ fs <1, the crack index is 0.7 ≦ fs <1, and the V segregation index is 0.1 ≦ fs ≦ 0.5. It was found that the improvement effect is exhibited only when it is added. However, in this case, the improvement effect is only manifested for each index. On the other hand, according to the conditions within the scope of each claim of the present invention, in particular, the conditions within the scope of claim 3 for obtaining a score satisfying the soundness of the inner surface of the pipe, the slab internal quality characteristic is 3 It can be seen that the index can be improved at the same time.

【0051】[0051]

【発明の効果】この発明は上述したように構成したの
で、従来よりも簡便なプロセスで内質の健全なCr合金
鋼の鋳片素材を提供することができ、内面疵のない難加
工性のCr合金鋼継目無管を製造することができる。即
ち、この発明により、難加工性のCr合金鋼、特に従来
困難とされていた高Cr合金鋼の無欠陥ビレットの連続
鋳造化を達成し、その結果、従来と変らない製管法を用
いても管内面疵がなく、付加価値の高い継目無鋼管を製
造することができ、且つ製造コストも低減し得るとい
う、工業上有用な効果がもたらされる。
EFFECTS OF THE INVENTION Since the present invention is configured as described above, it is possible to provide a slab material of Cr alloy steel having a good internal quality by a simpler process than conventional ones, and it is possible to obtain a hard workability without internal flaws. A Cr alloy steel seamless pipe can be manufactured. That is, the present invention achieves continuous casting of a defect-free billet of a difficult-to-work Cr alloy steel, particularly a high-Cr alloy steel, which has been considered difficult in the past, and as a result, uses a pipe manufacturing method that does not change from the conventional one. Also, there is an industrially useful effect that a seamless steel pipe with a high added value can be manufactured without any inner surface flaws and the manufacturing cost can be reduced.

【図面の簡単な説明】[Brief description of drawings]

【図1】この発明の一実施態様を説明するための連続鋳
造工程の縦断面概念図である。
FIG. 1 is a conceptual vertical cross-sectional view of a continuous casting process for explaining an embodiment of the present invention.

【図2】この発明の他の実施態様を説明するための連続
鋳造工程の縦断面概念図である。
FIG. 2 is a vertical sectional conceptual view of a continuous casting process for explaining another embodiment of the present invention.

【図3】この発明の一実施例におけるV型カリバーロー
ルからなる圧下ロールの鋳片に対する配置の要部を示す
側面概略図である。
FIG. 3 is a schematic side view showing a main part of the arrangement of a reduction roll made of a V-type caliber roll with respect to a cast piece in one embodiment of the present invention.

【図4】図3のA−A線断面図である。FIG. 4 is a sectional view taken along line AA of FIG. 3;

【図5】図3のB−B線断面図である。FIG. 5 is a sectional view taken along line BB of FIG. 3;

【図6】凝固末期の鋳片に対して1段軽圧下または2段
軽圧下を付与した場合の、鋳片内質特性の各指数に及ぼ
す軽圧下付与時の軸心固相率fsの影響の念図であ
る。
FIG. 6 shows the influence of the solid phase fraction fs of the axial center at the time of light reduction on each index of the internal properties of the slab when the first stage light reduction or the second stage light reduction is applied to the slab in the final stage of solidification. it is a conceptual diagram of.

【図7】鋼中Cr含有量と溶鋼の粘性との関係を示すグ
ラフである。
FIG. 7 is a graph showing the relationship between the Cr content in steel and the viscosity of molten steel.

【符号の説明】[Explanation of symbols]

1 丸形状鋳型 2 溶鋼 3 未凝固丸ビレット鋳片 3’ 丸ビレット鋳片 4 圧下装置 4a 圧下ロール 4b 1段目圧下ロール 4c 2段目圧下ロール 5 固液共存相 6 ガイドロール群 7 引き抜きロール 8 鋳型内電磁撹拌装置 9a,9a’,9b,9b’ V型カリバーロール 1 Round shape mold 2 Molten steel 3 Unsolidified round billet slab 3'Round billet slab 4 Rolling down device 4a Rolling down roll 4b 1st stage rolling down roll 4c 2nd stage rolling down roll 5 Solid-liquid coexisting phase 6 Guide roll group 7 Drawing roll 8 In-mold electromagnetic stirrer 9a, 9a ', 9b, 9b' V-type caliber roll

───────────────────────────────────────────────────── フロントページの続き (72)発明者 前田 浩史 東京都千代田区丸の内一丁目1番2号 日 本鋼管株式会社内 (72)発明者 中込 理欧 東京都千代田区丸の内一丁目1番2号 日 本鋼管株式会社内 (72)発明者 勝村 龍郎 東京都千代田区丸の内一丁目1番2号 日 本鋼管株式会社内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Hiroshi Maeda 1-1-2 Marunouchi, Chiyoda-ku, Tokyo Nihon Kokan Co., Ltd. (72) Riyo Nakagome 1-2-1 Marunouchi, Chiyoda-ku, Tokyo Nippon Steel Tube Co., Ltd. (72) Inventor Tatsuro Katsumura 1-2-2 Marunouchi, Chiyoda-ku, Tokyo Nihon Steel Tube Co., Ltd.

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 Cr含有量が0.5wt.%を超えるCr合
金鋼を直径340mm以下の丸形状鋳型により連続鋳造
し、得られた丸ビレット鋳片の凝固末期の部分に圧下ロ
ールで軽圧下を加えることを特徴とする、クロム合金鋼
丸ビレット鋳片の製造方法。
1. A Cr alloy steel having a Cr content of more than 0.5 wt.% Is continuously cast by a round mold having a diameter of 340 mm or less, and the round billet slab obtained is lightly rolled by a rolling roll at the end of solidification. A method for manufacturing a chromium alloy steel round billet slab, which comprises adding
【請求項2】 請求項1記載の丸ビレット鋳片の製造方
法に更に、前記丸形状鋳型内における溶鋼の電磁撹拌処
理を付加し、そして、前記圧下ロールによる前記軽圧下
として、2段以上の圧下ロールで前記丸ビレット鋳片の
軸心固相率fs が0.1≦fs <1を満たす時期に、C
方向断面積減少率が0.1〜3%の範囲内の圧下を加え
ることを特徴とする請求項1記載のクロム合金鋼丸ビレ
ット鋳片の製造方法。
2. The method for manufacturing a round billet slab according to claim 1, further comprising electromagnetic stirring treatment of molten steel in the round mold, and the light reduction by the reduction roll is performed in two or more stages. When the axial solid fraction fs of the round billet slab satisfies 0.1 ≦ fs <1 with the pressing roll, C
The method for producing a chrome alloy steel round billet slab according to claim 1, wherein the reduction in the direction cross-sectional area reduction rate is within the range of 0.1 to 3%.
【請求項3】 前記軽圧下は、軸線が互いに平行で且つ
前記丸ビレット鋳片を中間にして両側に対向する2個の
V型カリバーロールからなる圧下ロールを、前記丸ビレ
ット鋳片の鋳造方向に沿って2基以上配置し、前記各圧
下ロールによる前記丸ビレット鋳片に対する各圧下方向
が互いに異なる方向に前記凝固末期の前記丸ビレット鋳
片を圧下することを特徴とする、請求項1または2記載
のクロム合金鋼丸ビレット鋳片の製造方法。
3. In the light reduction, a reduction roll composed of two V-shaped caliber rolls whose axes are parallel to each other and face each other with the round billet slab in the middle is used in the casting direction of the round billet slab. 2 or more are arranged along each, and the respective round billet slabs for the round billet slabs by the respective drafting rolls are rolled down in different directions from each other, and the round billet slabs at the final stage of solidification are rolled down. 2. The method for producing a round billet slab of chromium alloy steel according to 2.
JP12140696A 1996-05-16 1996-05-16 Manufacturing method of chrome alloy steel round billet slab Expired - Lifetime JP3237518B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP12140696A JP3237518B2 (en) 1996-05-16 1996-05-16 Manufacturing method of chrome alloy steel round billet slab

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP12140696A JP3237518B2 (en) 1996-05-16 1996-05-16 Manufacturing method of chrome alloy steel round billet slab

Publications (2)

Publication Number Publication Date
JPH09300053A true JPH09300053A (en) 1997-11-25
JP3237518B2 JP3237518B2 (en) 2001-12-10

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Country Status (1)

Country Link
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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09300006A (en) * 1996-05-15 1997-11-25 Nkk Corp Manufacture of seamless steel tube difficult to be worked
JP2000153349A (en) * 1998-11-17 2000-06-06 Sumitomo Metal Ind Ltd Production of round cast billet for seamless steel pipe
JP2001232446A (en) * 1999-12-14 2001-08-28 Nkk Corp CONTINUOUS CASTING METHOD FOR HIGH Cr STEEL WITH SMALL CROSS SECTION
JP2002103002A (en) * 2000-09-25 2002-04-09 Sumitomo Metal Ind Ltd Method for producing cast billet and seamless steel tube
JP2002361372A (en) * 2001-06-07 2002-12-17 Sumitomo Metal Ind Ltd CASTING METHOD FOR HIGH Cr-CONTAINING STEEL
EP1291099A2 (en) * 2001-09-08 2003-03-12 SMS Demag AG Verfahren und Vorrichtung zur Optimierung der Qualität von Gussträngen mit runden oder annähernd runden Querschnitten
JP2010052043A (en) * 2008-07-31 2010-03-11 Jfe Steel Corp Continuous casting method and equipment for round slab
JP2010052042A (en) * 2008-07-30 2010-03-11 Jfe Steel Corp Continuous casting method for round slab for seamless steel pipe
JP2012152781A (en) * 2011-01-26 2012-08-16 Jfe Steel Corp Facility for round slab continuous casting for making seamless steel pipe
JP2014226675A (en) * 2013-05-20 2014-12-08 新日鐵住金株式会社 CONTINUOUS CASTING METHOD OF HIGH Cr STEEL
CN107116192A (en) * 2017-06-27 2017-09-01 中冶京诚工程技术有限公司 Continuous casting billet pressing equipment
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Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09300006A (en) * 1996-05-15 1997-11-25 Nkk Corp Manufacture of seamless steel tube difficult to be worked
JP2000153349A (en) * 1998-11-17 2000-06-06 Sumitomo Metal Ind Ltd Production of round cast billet for seamless steel pipe
JP2001232446A (en) * 1999-12-14 2001-08-28 Nkk Corp CONTINUOUS CASTING METHOD FOR HIGH Cr STEEL WITH SMALL CROSS SECTION
JP2002103002A (en) * 2000-09-25 2002-04-09 Sumitomo Metal Ind Ltd Method for producing cast billet and seamless steel tube
JP2002361372A (en) * 2001-06-07 2002-12-17 Sumitomo Metal Ind Ltd CASTING METHOD FOR HIGH Cr-CONTAINING STEEL
EP1291099A2 (en) * 2001-09-08 2003-03-12 SMS Demag AG Verfahren und Vorrichtung zur Optimierung der Qualität von Gussträngen mit runden oder annähernd runden Querschnitten
EP1291099A3 (en) * 2001-09-08 2003-12-10 SMS Demag AG Method and device for optimizing the quality of continuously cast ingots, having a circular or quasi circular cross-section
JP2010052042A (en) * 2008-07-30 2010-03-11 Jfe Steel Corp Continuous casting method for round slab for seamless steel pipe
JP2010052043A (en) * 2008-07-31 2010-03-11 Jfe Steel Corp Continuous casting method and equipment for round slab
JP2012152781A (en) * 2011-01-26 2012-08-16 Jfe Steel Corp Facility for round slab continuous casting for making seamless steel pipe
JP2014226675A (en) * 2013-05-20 2014-12-08 新日鐵住金株式会社 CONTINUOUS CASTING METHOD OF HIGH Cr STEEL
IT201600102472A1 (en) * 2016-10-12 2018-04-12 Danieli Off Mecc SOFT REDUCTION DEVICE FOR METAL PRODUCTS OF ROUND SECTION
WO2018069854A1 (en) * 2016-10-12 2018-04-19 Danieli & C. Officine Meccaniche S.P.A. A device for the soft reduction of round-section metal products
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US10744559B2 (en) 2016-10-12 2020-08-18 Daniel & C. Officine Meccaniche S.P.A. Device for the soft reduction of round-section metal products
CN109952166B (en) * 2016-10-12 2021-12-07 丹尼尔和科菲森梅克尼齐有限公司 Device for soft reduction of metal products with circular section
CN107116192A (en) * 2017-06-27 2017-09-01 中冶京诚工程技术有限公司 Continuous casting billet pressing equipment

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