JPH0559045B2 - - Google Patents
Info
- Publication number
- JPH0559045B2 JPH0559045B2 JP58029171A JP2917183A JPH0559045B2 JP H0559045 B2 JPH0559045 B2 JP H0559045B2 JP 58029171 A JP58029171 A JP 58029171A JP 2917183 A JP2917183 A JP 2917183A JP H0559045 B2 JPH0559045 B2 JP H0559045B2
- Authority
- JP
- Japan
- Prior art keywords
- zeolite
- aqueous mixture
- type
- weight
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 44
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 34
- 239000010457 zeolite Substances 0.000 claims description 27
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 23
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 23
- 229910021536 Zeolite Inorganic materials 0.000 claims description 22
- 239000005335 volcanic glass Substances 0.000 claims description 21
- 239000004115 Sodium Silicate Substances 0.000 claims description 18
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 18
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 18
- 239000013078 crystal Substances 0.000 claims description 17
- 239000000377 silicon dioxide Substances 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 229910001868 water Inorganic materials 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 239000002245 particle Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 7
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 6
- 229910001388 sodium aluminate Inorganic materials 0.000 claims description 6
- 238000002425 crystallisation Methods 0.000 claims description 5
- 230000008025 crystallization Effects 0.000 claims description 5
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 4
- 229910052681 coesite Inorganic materials 0.000 claims description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims description 4
- 235000012239 silicon dioxide Nutrition 0.000 claims description 4
- 229910052682 stishovite Inorganic materials 0.000 claims description 4
- 229910052905 tridymite Inorganic materials 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 2
- 229910004806 Na2 SiO3.9H2 O Inorganic materials 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 54
- 229910052742 iron Inorganic materials 0.000 description 26
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 description 16
- 235000011121 sodium hydroxide Nutrition 0.000 description 13
- 238000000034 method Methods 0.000 description 12
- 239000002994 raw material Substances 0.000 description 12
- 239000000243 solution Substances 0.000 description 11
- 229910004298 SiO 2 Inorganic materials 0.000 description 10
- 239000003599 detergent Substances 0.000 description 10
- 239000011734 sodium Substances 0.000 description 9
- 238000005342 ion exchange Methods 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 7
- 238000010828 elution Methods 0.000 description 6
- 235000019353 potassium silicate Nutrition 0.000 description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 241000975357 Salangichthys microdon Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 238000011085 pressure filtration Methods 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000625836 Ochrolechia Species 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical class O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2917183A JPS59156911A (ja) | 1983-02-22 | 1983-02-22 | 火山ガラスを主原料とするａ型ゼオライトの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2917183A JPS59156911A (ja) | 1983-02-22 | 1983-02-22 | 火山ガラスを主原料とするａ型ゼオライトの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59156911A JPS59156911A (ja) | 1984-09-06 |
| JPH0559045B2 true JPH0559045B2 (ko) | 1993-08-30 |
Family
ID=12268790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2917183A Granted JPS59156911A (ja) | 1983-02-22 | 1983-02-22 | 火山ガラスを主原料とするａ型ゼオライトの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59156911A (ko) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4015850A1 (de) * | 1990-05-17 | 1991-11-21 | Henkel Kgaa | Verfahren zur herstellung von zeolithen aus getempertem sand |
| US6299854B1 (en) * | 1998-06-12 | 2001-10-09 | Teruo Henmi | Method of producing artificial zeolite |
| JP5225340B2 (ja) * | 2010-08-23 | 2013-07-03 | 日本建設技術株式会社 | ゼオライトの製造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5263200A (en) * | 1975-11-20 | 1977-05-25 | Sanki Eng Co Ltd | Process for preparing zeolite employing sillus as raw material |
-
1983
- 1983-02-22 JP JP2917183A patent/JPS59156911A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5263200A (en) * | 1975-11-20 | 1977-05-25 | Sanki Eng Co Ltd | Process for preparing zeolite employing sillus as raw material |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS59156911A (ja) | 1984-09-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3310373A (en) | Method for producing crystalline aluminosilicates | |
| EP0609270B1 (en) | Process for preparing uniform mfi-type zeolite crystals | |
| JP3417944B2 (ja) | ナノメーターサイズのモレキュラーシーブ結晶または凝集物及びそれらの製造方法 | |
| JPH05503065A (ja) | 結晶二珪酸ナトリウムの熱水製造方法 | |
| CA1213872A (en) | Process for preparation of zeolites | |
| DK167866B1 (da) | Fremgangsmaade til fremstilling af zeolitter | |
| JP7190577B2 (ja) | ゼオライトおよびその製造方法 | |
| JPH02221115A (ja) | ゼオライト及びその製造方法 | |
| PL117556B1 (en) | Continuous process for zeolite a manufactre | |
| US4376106A (en) | Process for producing Y-type zeolite | |
| US3343913A (en) | Table iv | |
| JPH08508003A (ja) | 微細な粒子状のゼオライト型アルカリ金属アルミニウムシリケートの製造方法 | |
| CA1132962A (en) | Preparing zeolite naa | |
| JPH0497908A (ja) | ゼオライトの製造方法 | |
| DK167869B1 (da) | Fremgangsmaade til fremstilling af zeolit af faujasittypen | |
| US3898319A (en) | Process for preparing zeolite Y | |
| JPS6346007B2 (ko) | ||
| HU181898B (en) | Semicontinuous industrial process for producing zeolite a | |
| JPH0559045B2 (ko) | ||
| GB1560223A (en) | Synethesis of favjasite | |
| US2958579A (en) | Process for manufacture of molecular sieve adsorbents | |
| JPS6261531B2 (ko) | ||
| JPS598617A (ja) | アルミノ珪酸塩 | |
| JP3678790B2 (ja) | フォージャサイト型ゼオライトの製造方法 | |
| SU998342A1 (ru) | Способ получени синтетического цеолита типа @ |