JPH0553480B2 - - Google Patents
Info
- Publication number
- JPH0553480B2 JPH0553480B2 JP58223170A JP22317083A JPH0553480B2 JP H0553480 B2 JPH0553480 B2 JP H0553480B2 JP 58223170 A JP58223170 A JP 58223170A JP 22317083 A JP22317083 A JP 22317083A JP H0553480 B2 JPH0553480 B2 JP H0553480B2
- Authority
- JP
- Japan
- Prior art keywords
- crystallization
- tower
- crystals
- fructose
- crystal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000013078 crystal Substances 0.000 claims description 101
- 238000002425 crystallisation Methods 0.000 claims description 84
- 230000008025 crystallization Effects 0.000 claims description 82
- 239000005715 Fructose Substances 0.000 claims description 61
- 229930091371 Fructose Natural products 0.000 claims description 59
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 56
- 239000007788 liquid Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 26
- 235000000346 sugar Nutrition 0.000 claims description 26
- 238000001816 cooling Methods 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 8
- 239000000498 cooling water Substances 0.000 claims description 7
- 235000015001 Cucumis melo var inodorus Nutrition 0.000 claims description 6
- 240000002495 Cucumis melo var. inodorus Species 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 230000006378 damage Effects 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000243 solution Substances 0.000 description 26
- 238000003756 stirring Methods 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 5
- 239000003960 organic solvent Substances 0.000 description 5
- 238000006116 polymerization reaction Methods 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 235000019534 high fructose corn syrup Nutrition 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 235000008504 concentrate Nutrition 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000002231 fructose derivatives Chemical class 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 235000012907 honey Nutrition 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000004904 shortening Methods 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 239000011549 crystallization solution Substances 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000011033 desalting Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N fructose group Chemical group OCC(=O)[C@@H](O)[C@H](O)[C@H](O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 210000004885 white matter Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58223170A JPS60118200A (ja) | 1983-11-29 | 1983-11-29 | 無水結晶果糖の連続結晶化方法及び装置 |
| US06/669,039 US4666527A (en) | 1983-11-29 | 1984-11-06 | Continuous crystallization of fructose anhydride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58223170A JPS60118200A (ja) | 1983-11-29 | 1983-11-29 | 無水結晶果糖の連続結晶化方法及び装置 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60118200A JPS60118200A (ja) | 1985-06-25 |
| JPH0553480B2 true JPH0553480B2 (US20110009641A1-20110113-C00256.png) | 1993-08-10 |
Family
ID=16793894
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58223170A Granted JPS60118200A (ja) | 1983-11-29 | 1983-11-29 | 無水結晶果糖の連続結晶化方法及び装置 |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US4666527A (US20110009641A1-20110113-C00256.png) |
| JP (1) | JPS60118200A (US20110009641A1-20110113-C00256.png) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8506482D0 (en) * | 1985-03-13 | 1985-04-17 | Tate & Lyle Plc | Sugar process |
| FR2582016B1 (fr) * | 1985-05-15 | 1987-09-18 | Roquette Freres | Procede et installation de production de fructose cristallise anhydre |
| FR2582015B1 (fr) * | 1985-05-15 | 1987-09-18 | Roquette Freres | Procede et installation de preparation de dextrose cristallise anhydre |
| US5350456A (en) * | 1987-02-02 | 1994-09-27 | A. E. Staley Manufacturing Company | Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener |
| US5234503A (en) * | 1987-02-02 | 1993-08-10 | A.E. Saley Manufacturing Co. | Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener |
| US5656094A (en) * | 1987-02-02 | 1997-08-12 | A.E. Staley Manufacturing Company | Integrated process for producing crystalline fructose and a high-fructose, liquid phase sweetener |
| US5230742A (en) * | 1987-02-02 | 1993-07-27 | A. E. Staley Manufacturing Co. | Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener |
| FI77693C (fi) * | 1987-06-03 | 1989-04-10 | Suomen Sokeri Oy | Foerfarande foer kristallisering av fruktos. |
| US4895601A (en) * | 1988-12-12 | 1990-01-23 | Archer Daniels Midland Company | Aqueous-alcohol fructose crystallization |
| US5047088A (en) * | 1989-06-30 | 1991-09-10 | A. E. Staley Manufacturing Company | Method for crystallization of fructose |
| JP3168550B2 (ja) * | 1992-12-02 | 2001-05-21 | 株式会社林原生物化学研究所 | 脱水剤およびそれを用いる含水物の脱水方法並びにその方法で得られる脱水物品 |
| US6005100A (en) * | 1992-12-02 | 1999-12-21 | Kabushiki Kaisha Hayashibara Seitbutsu Kagaku Kenkyujo | Trehalose composition for prolonging product shelf life |
| US6663780B2 (en) | 1993-01-26 | 2003-12-16 | Danisco Finland Oy | Method for the fractionation of molasses |
| FI96225C (fi) | 1993-01-26 | 1996-05-27 | Cultor Oy | Menetelmä melassin fraktioimiseksi |
| US5795398A (en) | 1994-09-30 | 1998-08-18 | Cultor Ltd. | Fractionation method of sucrose-containing solutions |
| US6224776B1 (en) | 1996-05-24 | 2001-05-01 | Cultor Corporation | Method for fractionating a solution |
| JP3639858B2 (ja) * | 1997-09-12 | 2005-04-20 | 日本甜菜製糖株式会社 | ラフィノースの結晶を製造する方法及び装置 |
| FR2796310B1 (fr) * | 1999-07-01 | 2001-10-19 | Rhodia Chimie Sa | Procede et reacteur multifonctionnel de synthese et cristallisation |
| WO2001014037A1 (fr) * | 1999-08-25 | 2001-03-01 | Kansai Chemical Engineering Co., Ltd. | Appareil et procede de cristallisation |
| FI20010977A (fi) * | 2001-05-09 | 2002-11-10 | Danisco Sweeteners Oy | Kromatografinen erotusmenetelmä |
| KR100967093B1 (ko) | 2008-04-01 | 2010-07-01 | 주식회사 신동방씨피 | 고순도 무수결정과당의 제조방법 |
| JP5667666B2 (ja) | 2013-06-28 | 2015-02-12 | 三井製糖株式会社 | 糖結晶含有液を製造する方法 |
| US8999007B2 (en) | 2013-07-12 | 2015-04-07 | Ostara Nutrient Recovery Technologies Inc. | Method for fines control |
| CN106745615A (zh) * | 2017-01-11 | 2017-05-31 | 启迪桑德环境资源股份有限公司 | 冷却结晶器 |
| CN114191842A (zh) * | 2021-12-29 | 2022-03-18 | 江苏道明化学有限公司 | 一种过氧化二异丙苯结晶工艺 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE865102C (de) * | 1950-10-06 | 1953-01-29 | Albert Henkel Sen | Zuckermassen-Kocher mit Ruehrwerk fuer stetigen Durchlaufbetrieb |
| US3607392A (en) * | 1967-12-21 | 1971-09-21 | Boehringer Mannheim Gmbh | Process and apparatus for the recovery of crystalline fructose from methanolic solution |
| JPS5239901B2 (US20110009641A1-20110113-C00256.png) * | 1973-02-12 | 1977-10-07 | ||
| US4056364A (en) * | 1974-08-30 | 1977-11-01 | Amstar Corporation | Two stage continuous crystallization apparatus with controls |
-
1983
- 1983-11-29 JP JP58223170A patent/JPS60118200A/ja active Granted
-
1984
- 1984-11-06 US US06/669,039 patent/US4666527A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| US4666527A (en) | 1987-05-19 |
| JPS60118200A (ja) | 1985-06-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |