JPH03297361A - Preparation of seasoning raw material having good preservability - Google Patents
Preparation of seasoning raw material having good preservabilityInfo
- Publication number
- JPH03297361A JPH03297361A JP2100806A JP10080690A JPH03297361A JP H03297361 A JPH03297361 A JP H03297361A JP 2100806 A JP2100806 A JP 2100806A JP 10080690 A JP10080690 A JP 10080690A JP H03297361 A JPH03297361 A JP H03297361A
- Authority
- JP
- Japan
- Prior art keywords
- flavor
- dried
- bonito
- acid
- bonite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000011194 food seasoning agent Nutrition 0.000 title claims abstract description 14
- 239000002994 raw material Substances 0.000 title abstract description 5
- 239000000796 flavoring agent Substances 0.000 claims abstract description 32
- 235000019634 flavors Nutrition 0.000 claims abstract description 31
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 18
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 9
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 9
- AUHDWARTFSKSAC-HEIFUQTGSA-N (2S,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)-2-(6-oxo-1H-purin-9-yl)oxolane-2-carboxylic acid Chemical compound [C@]1([C@H](O)[C@H](O)[C@@H](CO)O1)(N1C=NC=2C(O)=NC=NC12)C(=O)O AUHDWARTFSKSAC-HEIFUQTGSA-N 0.000 claims abstract description 8
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims abstract description 8
- GRSZFWQUAKGDAV-UHFFFAOYSA-N Inosinic acid Natural products OC1C(O)C(COP(O)(O)=O)OC1N1C(NC=NC2=O)=C2N=C1 GRSZFWQUAKGDAV-UHFFFAOYSA-N 0.000 claims abstract description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 8
- 235000013922 glutamic acid Nutrition 0.000 claims abstract description 8
- 239000004220 glutamic acid Substances 0.000 claims abstract description 8
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000013902 inosinic acid Nutrition 0.000 claims abstract description 8
- 239000004245 inosinic acid Substances 0.000 claims abstract description 8
- 229940028843 inosinic acid Drugs 0.000 claims abstract description 8
- 239000004310 lactic acid Substances 0.000 claims abstract description 7
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 7
- 239000011780 sodium chloride Substances 0.000 claims abstract description 4
- 241000269851 Sarda sarda Species 0.000 claims description 36
- 239000000463 material Substances 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 4
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 claims description 4
- 235000014304 histidine Nutrition 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 235000002639 sodium chloride Nutrition 0.000 claims description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims 2
- 235000011164 potassium chloride Nutrition 0.000 claims 2
- 239000001103 potassium chloride Substances 0.000 claims 2
- 229960004424 carbon dioxide Drugs 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- DDRJAANPRJIHGJ-UHFFFAOYSA-N creatinine Chemical compound CN1CC(=O)NC1=N DDRJAANPRJIHGJ-UHFFFAOYSA-N 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000004278 EU approved seasoning Substances 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 235000014347 soups Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000012937 correction Methods 0.000 description 2
- 229940109239 creatinine Drugs 0.000 description 2
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- AANLCWYVVNBGEE-IDIVVRGQSA-L Disodium inosinate Chemical compound [Na+].[Na+].O[C@@H]1[C@H](O)[C@@H](COP([O-])([O-])=O)O[C@H]1N1C(NC=NC2=O)=C2N=C1 AANLCWYVVNBGEE-IDIVVRGQSA-L 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
- 235000013890 disodium inosinate Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 229940074391 gallic acid Drugs 0.000 description 1
- 235000004515 gallic acid Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Abstract
Description
【発明の詳細な説明】
〔産業上の利用分野〕
本発明は保存性の良好な鰹節風味調味料素材の製造法に
関する。DETAILED DESCRIPTION OF THE INVENTION [Industrial Field of Application] The present invention relates to a method for producing a dried bonito flavor seasoning material with good storage stability.
〔従来の技術]
従来鰹節風味調味料には、風味原料として鰹節又は鰹節
の熱水抽出物が用いられているが、微生物汚染されやす
い、風味の保存安定性が悪いなどという問題点がある。[Prior Art] Traditionally, dried bonito flakes or hot water extracts of dried bonito flakes have been used as flavor ingredients in dried bonito flavor seasonings, but there are problems such as easy microbial contamination and poor flavor storage stability.
又風味原料を用いないでグルタミン酸ナトリウム、イノ
シン酸ナトリウム等と溶剤抽出等により調製された鰹節
フレーバーを併用した場合、原料に鰹節又は鰹節の熱水
抽出物を用いたものに比べ保存性は向上するものの、呈
味的には鰹節の持つこく味がなく、風味も天然の鰹節だ
しに比べ品質的に劣るという欠点がある。In addition, when monosodium glutamate, sodium inosinate, etc. are used in combination with bonito flavor prepared by solvent extraction, etc. without using flavor raw materials, the preservability is improved compared to when bonito flakes or a hot water extract of bonito flakes are used as raw materials. However, it has the disadvantage that it lacks the rich flavor that bonito flakes have, and the quality of the flavor is inferior to that of natural bonito flakes.
一方、従来の鰹節風味調味料素材の保存性改善方法とし
ては、風味調味料素材をCOz又はN2置換で包装した
り、没食子酸やトコフェロールなどの抗酸化剤を添加す
るという方法も考えられるが、いずれもいまだ満足すべ
き結果は得られていない。On the other hand, as a method for improving the shelf life of conventional bonito flavor seasoning materials, it is possible to package the flavor seasoning materials with COz or N2 substitution, or to add antioxidants such as gallic acid and tocopherol. In either case, satisfactory results have not yet been obtained.
本発明は、上記の如き風味調味料の問題点を解決し、保
存安定性、品質共に良好な鰹節風味調味料素材を得るこ
とを目的とする。The purpose of the present invention is to solve the above problems of flavor seasonings and to obtain a dried bonito flavor seasoning material with good storage stability and quality.
3問題点を解決するための手段〕
本発明者らは、上記問題点の解決につき鋭意検討を重ね
た結果、イノシン酸、ヒスチジン、グルタミン酸、乳酸
、NaCE、Kiをある配合比で配合し、水に溶かした
後、必要に応じ酸又はアルカリでpHを調整したものに
、液体又は超臨界炭酸ガス抽出により調製した鰹節フレ
ーバーを適当な比率で配合することにより、鰹節様の呈
味と香り、風味を持ち、しかも天然の鰹節だしよりもは
るかに保存性の良い調味料素材が得られることを見出だ
し、本発明を完成したものである。Means for Solving the 3 Problems] As a result of intensive studies to solve the above problems, the present inventors have formulated inosinic acid, histidine, glutamic acid, lactic acid, NaCE, and Ki in a certain ratio, After dissolving the bonito flakes in the liquid and adjusting the pH with acid or alkali as necessary, the bonito flakes flavor prepared by liquid or supercritical carbon dioxide gas extraction are blended in an appropriate ratio to create a bonito flakes-like taste, aroma, and flavor. The present invention was completed based on the discovery that it is possible to obtain a seasoning material that has a long shelf life and has a much better shelf life than natural bonito flakes.
本発明を更に詳しく説明する。The present invention will be explained in more detail.
呈味溶液はイノシン酸、ヒスチジン、グルタミン酸、乳
酸、NaC1,、KCI!を重量比率でイノシン酸量を
100としたとき、ヒスチジンを10−300、グルタ
ミン酸を0.1−100、乳酸を50−2000、Na
CEを10−1000.KCj2を10−1000の比
率で配合し、適量の水に溶解させた後、酸(HCffi
やIl:1PO4)又はアルカリ(NaOHやKOH等
)でpHを好ましくは5.7−6.7に調整する。Taste solutions include inosinic acid, histidine, glutamic acid, lactic acid, NaCl, KCI! When the amount of inosinic acid is 100 in weight ratio, histidine is 10-300, glutamic acid is 0.1-100, lactic acid is 50-2000, Na
CE 10-1000. After blending KCj2 at a ratio of 10-1000 and dissolving it in an appropriate amount of water, acid (HCffi
or Il:1PO4) or an alkali (such as NaOH or KOH) to preferably adjust the pH to 5.7-6.7.
又クレアチニン等のペプチドを1−300加えて、こく
味をさろに増強することも可能である。又別途、鰹節フ
レーバーは鰹節または節製造時の副産物から液体又は超
臨界状態の二酸化炭素によって抽出し、抽出物を調製す
る。抽出条件は、液体又は超臨界状態の二酸化炭素を用
いて常法に従って行えばよく、例えば超臨界炭酸ガス抽
出では温度31.1°C以上かつ圧カフ 5.2 kg
/c−以上の条件下で抽出する。又この際、エタノール
、水等の抽出助剤を用いると抽出効率はさろに向上する
。次に先の呈味溶液と抽出フレーバーを配合することに
より、鰹節様の呈味と香り、風味を持ち、しかも天然の
鰹節だしよりもはるかに保存性の良い調味料素材を得る
ことができるものである。It is also possible to add 1-300% of a peptide such as creatinine to further enhance the body taste. Separately, the bonito flakes flavor is prepared by extracting the bonito flakes or a by-product during the production of the bonito flakes using liquid or supercritical carbon dioxide. Extraction conditions may be carried out according to conventional methods using liquid or supercritical carbon dioxide. For example, in supercritical carbon dioxide extraction, temperature is 31.1°C or higher and pressure cuff is 5.2 kg.
Extract under conditions of /c- or higher. Moreover, at this time, if an extraction aid such as ethanol or water is used, the extraction efficiency will be further improved. Next, by blending the above-mentioned flavoring solution and extracted flavor, it is possible to obtain a seasoning material that has the taste, aroma, and flavor of bonito flakes, and has a much better shelf life than natural bonito flakes. It is.
以下、実験例、実施例によって本発明を更に詳細に説明
するが、本発明の利用範囲はこれらによって躍定される
ものではない。Hereinafter, the present invention will be explained in more detail using experimental examples and examples, but the scope of use of the present invention is not determined by these.
(実験例1)
鰹節をハンマークラシャー粉砕機で粉砕して得た粉砕物
2kgにエタノール600gと水600gを噴霧し、液
体の二酸化炭素(25°C160気圧)で2時間抽出し
た。抽出物約700gを得、これは良好な鰹節風味を有
した。(Experimental Example 1) 600 g of ethanol and 600 g of water were sprayed onto 2 kg of a crushed product obtained by crushing dried bonito flakes using a hammer crusher crusher, and the mixture was extracted with liquid carbon dioxide (25°C, 160 atm) for 2 hours. Approximately 700 g of extract was obtained, which had a good katsuobushi flavor.
(実験例2)
イノシン酸15.7■、グルタミン酸0.725■、ヒ
スチジン62.25■、クレアチニン35.95■、乳
酸106.7mg、NaC127,,6g 、 KCI
41.05■、Cf−2,17■を水に溶解させ、1
00−に定容した。この溶液のpHは5.8であり、鰹
節様の呈味をもつものであった。(Experimental Example 2) Inosinic acid 15.7■, glutamic acid 0.725■, histidine 62.25■, creatinine 35.95■, lactic acid 106.7mg, NaC 127,6g, KCI
41.05■, Cf-2,17■ was dissolved in water, 1
The volume was adjusted to 00-. The pH of this solution was 5.8, and it had a taste similar to dried bonito flakes.
(実験例3)
鰹節を鰹節削り機で削り、沸騰水1000戚にこれを2
0g加えて1分間後濾布で濾過し、鰹節一番だしを得た
。(Experiment Example 3) Shave bonito flakes with a bonito shaving machine and add 1,000 ounces of this to boiling water.
After adding 0g of the mixture for 1 minute, it was filtered with a filter cloth to obtain dried bonito flakes.
(実施例1)
実施例2で得られた呈味溶液に実験例1で得た鰹節フレ
ーバを0.1%加えることにより、鰹節様の味、香りを
持つ溶液を得た。実験例1で得た天然の鰹節だしは24
°Cで3力月すると油焼は風味、異風味が生成したのに
対し、得られた溶液は10力月経過後も良好な風味を有
していた。したがって、得られた溶液は鰹節だしより著
しく保存性が良好なものであることがわかる。(Example 1) By adding 0.1% of the dried bonito flavor obtained in Experimental Example 1 to the flavored solution obtained in Example 2, a solution having a taste and aroma similar to dried bonito flakes was obtained. The natural bonito stock obtained in Experimental Example 1 is 24
When heated at °C for 3 months, the oil-grilled mixture developed a flavor and off-flavor, whereas the resulting solution had a good flavor even after 10 months. Therefore, it can be seen that the obtained solution has a significantly better shelf life than bonito flakes.
(実施例2) 実施例1で得た溶液を用いたすまし汁(NaCi!。(Example 2) A refreshing soup (NaCi!) using the solution obtained in Example 1.
0、8%、醤油0.3%)(■)と実験例3で得た天然
の鰹節だしを用いたすまし汁(■)の官能を比較した。The sensory sensations of the soup stock (■) using the natural bonito flakes obtained in Experimental Example 3 were compared.
方法は、二点比較法で、訓練されたパネル20名を用い
て鰹節様の呈味の好ましさ、鰹節様の香り、風味の好ま
しさ、総合的味、風味の好ましさを比較した。The method was a two-point comparison method, using a trained panel of 20 people to compare the favorability of bonito-like taste, bonito-like aroma, flavor favorability, overall taste, and flavor favorability. did.
平成2年
2日
平成2年特許願第100806号
官能検査の結果は上記の通りで、当該溶液は鰹節だし汁
とほぼ同等の嗜好性を持つことがわかる。Patent Application No. 100806 dated 2nd year of 1990 The results of the sensory test are as described above, and it can be seen that the solution has almost the same palatability as bonito flakes soup stock.
〔発明の効果]
本発明によれば、呈味物質と液体炭酸ガスあるいは超臨
界炭酸ガス抽出による鰹節フレーバーを特定の配合比率
で配合することにより、保存性が良く品質の良い鰹節風
味調味料素材が得られ、これを使うことで風味調味料の
保存性、品質を改善することができる。[Effects of the Invention] According to the present invention, by blending a taste substance and a bonito flavor produced by liquid carbon dioxide gas or supercritical carbon dioxide gas extraction in a specific blending ratio, a high quality bonito flavor seasoning material with good storage stability can be obtained. can be obtained, and by using this, the storage stability and quality of flavor seasonings can be improved.
4、補正指令の日付 自発 5、補正により増加する請求項の数 6、補正の対象 明細書の特許請求の範囲 7、補正の内容 別紙の通り補正する。4. Date of amendment order Voluntary 5. Number of claims increased by amendment 6. Subject of correction Scope of claims in the specification 7. Contents of correction Correct as shown in the attached sheet.
なしnone
Claims (1)
、NaCl、及びKClを含む溶液に、液体又は超臨界
炭酸ガス抽出により調製した鰹節フレーバーを配合する
ことを特徴とする鰹節様の呈味と香り、風味を持ち、し
かも天然の鰹節だしよりも保存性が良好な調味料素材の
製造法。 2、呈味成分としてイノシン酸、ヒスチジン、グルタミ
ン酸、乳酸、NaCl、KClを、重量比で、イノシン
酸量を100とし、ヒスチジンを10−300、グルタ
ミン酸を0.1−100、乳酸を50−2000、Na
Clを10−1000、KClを10−1000の比率
で配合することを特徴とする請求項1記載の調味料素材
の製造法。[Claims] 1. A bonito flakes-like taste characterized by blending a bonito flavor prepared by liquid or supercritical carbon dioxide gas extraction into a solution containing at least inosinic acid, histidine, glutamic acid, NaCl, and KCl. A method for producing a seasoning material that has a strong aroma and flavor, and has a better shelf life than natural bonito flakes. 2. As taste components, inosinic acid, histidine, glutamic acid, lactic acid, NaCl, KCl, in weight ratio, inosinic acid amount is 100, histidine is 10-300, glutamic acid is 0.1-100, and lactic acid is 50-2000. , Na
2. The method for producing a seasoning material according to claim 1, characterized in that Cl is blended in a ratio of 10 to 1000 and KCl is blended in a ratio of 10 to 1000.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2100806A JP2893839B2 (en) | 1990-04-17 | 1990-04-17 | Manufacturing method of seasoning material with good shelf life |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2100806A JP2893839B2 (en) | 1990-04-17 | 1990-04-17 | Manufacturing method of seasoning material with good shelf life |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH03297361A true JPH03297361A (en) | 1991-12-27 |
JP2893839B2 JP2893839B2 (en) | 1999-05-24 |
Family
ID=14283624
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2100806A Expired - Lifetime JP2893839B2 (en) | 1990-04-17 | 1990-04-17 | Manufacturing method of seasoning material with good shelf life |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2893839B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006137706A (en) * | 2004-11-12 | 2006-06-01 | Ajinomoto Co Inc | Anti-fatigue composition |
JP2012143168A (en) * | 2011-01-07 | 2012-08-02 | Ajinomoto Co Inc | Method for manufacturing flavor raw material |
-
1990
- 1990-04-17 JP JP2100806A patent/JP2893839B2/en not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006137706A (en) * | 2004-11-12 | 2006-06-01 | Ajinomoto Co Inc | Anti-fatigue composition |
JP2012143168A (en) * | 2011-01-07 | 2012-08-02 | Ajinomoto Co Inc | Method for manufacturing flavor raw material |
Also Published As
Publication number | Publication date |
---|---|
JP2893839B2 (en) | 1999-05-24 |
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