JPS58121770A - Preparation of extracted spice having improved taste and flavor - Google Patents

Preparation of extracted spice having improved taste and flavor

Info

Publication number
JPS58121770A
JPS58121770A JP56209716A JP20971681A JPS58121770A JP S58121770 A JPS58121770 A JP S58121770A JP 56209716 A JP56209716 A JP 56209716A JP 20971681 A JP20971681 A JP 20971681A JP S58121770 A JPS58121770 A JP S58121770A
Authority
JP
Japan
Prior art keywords
acetic acid
ethyl alcohol
spice
aqueous solution
flavor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP56209716A
Other languages
Japanese (ja)
Inventor
Kakuji Nishiyama
西山 覚次
Terumi Okuno
奥野 照美
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KITSUKOO SHOKUHIN KOGYO KK
Original Assignee
KITSUKOO SHOKUHIN KOGYO KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KITSUKOO SHOKUHIN KOGYO KK filed Critical KITSUKOO SHOKUHIN KOGYO KK
Priority to JP56209716A priority Critical patent/JPS58121770A/en
Publication of JPS58121770A publication Critical patent/JPS58121770A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To obtain an extracted spice having improved and strong taste and flavor, by extracting natural spice with a mixed aqueous solution of ethyl alcohol and acetic acid having specific concentrations. CONSTITUTION:Ethyl alcohol, acetic acid and water are mixed together to obtain a mixed aqueous solution having an ethyl alcohol content of 5-20% (V/V) and an acetic acid content of 5-15% (W/V). The objective extracted spice can be prepared by extracting a natural spice such as cinnamon, pepper, ginger, etc. with the above aqueous solution of a mixture of ethyl alcohol and acetic acid. Refined Japanese sake, low-class distilled spirits, whiskey, etc. can be used in place of ethyl alcohol, and rice vinegar, fruit vinegar, etc. can be used in place of acetic acid. The amount of the mixed aqueous solution used in the extraction is preferably 1-30pts.wt. per 1pt.wt. of the spice.

Description

【発明の詳細な説明】 本発明は、天然香辛料を特定濃度の、エチルアルコール
・酢酸混合水溶液で抽出し、風味の改良ための素材であ
るから、その香辛料の使用量を一定にして、その香辛法
度をより高いものにしようとする欲求が常に存在する。
Detailed Description of the Invention The present invention is a material for improving flavor by extracting natural spices with a mixed aqueous solution of ethyl alcohol and acetic acid at a specific concentration. There is always a desire to raise the law to a higher level.

本発明者らは、抽出香辛料について、その香辛料の使用
量を一定にして、その香辛法度を改良すべく、鋭意検討
を重ねた結果、天然香辛料を特定濃度の、エチルアルコ
ール・酢酸混合水溶液で抽出すると、該抽出香辛料の風
味が格段に増強されることを知り、との知見に基いて本
発明を完成した。
The inventors of the present invention have conducted intensive studies to improve the spice tolerance by keeping the amount of spices used constant.As a result, the inventors have found that natural spices are extracted with a mixed aqueous solution of ethyl alcohol and acetic acid at a specific concentration. Then, they found that the flavor of the extracted spice was significantly enhanced, and based on this knowledge, they completed the present invention.

即ち、本発明は天然香辛料を!−20%CV/V)のエ
チルアルコールおよびj−7j%(W/V)の酢酸を含
有する混合水溶液で抽出することを特徴とする風味の改
良された抽出香辛料の製造法である。
In other words, the present invention uses natural spices! -20% CV/V) of ethyl alcohol and j-7j% (W/V) of acetic acid.

以下、本発明の詳細な説明する。The present invention will be explained in detail below.

先ず本発明に用いる天然香辛料としては、クローブ、シ
ンナモン、ナツメッグ、オールスパイス、ローレル、セ
ロリシード、フェンネル、コリアンダー、タイム、セー
ジ等特に香味の強い芳香性香辛料、ペラパー、ジンジャ
−1唐辛子等辛味を特徴とする辛味性香辛料およびパプ
リカ、ターメリック等着色を目的とする着色性香辛料な
どが挙げられる。これらは天然原形品でもよいが、粉砕
したものが好ましい。またこれらは抽出香辛料の用途、
目的によシ、/種以上選択して使用するととができる。
First, the natural spices used in the present invention include aromatic spices with a particularly strong flavor such as cloves, cinnamon, nutmeg, allspice, bay leaf, celery seed, fennel, coriander, thyme, and sage, and pungent spices such as perapa and ginger chili pepper. Examples include pungent spices for coloring, and coloring spices for coloring, such as paprika and turmeric. These may be natural original products, but pulverized products are preferred. These are also used as extracted spices,
Depending on the purpose, you can select and use more than one species.

次に、これらの香辛料の抽出に用いる溶液は、jN2θ
% (V/V ’)のエチルアルコールドj〜15%(
W/V)の酢酸を含有する混合水溶液である。この特定
濃度の混合水溶液を用いることは極めて重要であって、
いずれか一方の水溶液だけでは、バランスのとれた、強
くかつ優れた香気の抽出は困難である。
Next, the solution used to extract these spices is jN2θ
% (V/V') of ethyl alcohol j ~ 15% (
This is a mixed aqueous solution containing acetic acid of W/V). It is extremely important to use a mixed aqueous solution with a specific concentration.
It is difficult to extract a balanced, strong, and excellent aroma using only one aqueous solution.

以下、これらについて実験例を挙げて説明する。These will be explained below using experimental examples.

実験例1 粉末天然香辛料(クローブ)を10v;5つA〜Cの3
区分に分け、Aの区分にはエチルアルコール9%(V/
V)−酢酸/7%(W/V)の混合水溶液を、Bの区分
にはエチルアルコール9チの単独水溶液を、そしてCの
区分には酢酸/θチの単独水溶液を、それぞれ200−
加え、密閉条件下において攪拌しながら3日間抽出し、
それぞれ3種類の抽出液を得た。
Experimental example 1 10v of powdered natural spice (cloves); 3 of 5 A to C
Divided into categories, category A contains 9% ethyl alcohol (V/
V) -A mixed aqueous solution of acetic acid/7% (W/V), a single aqueous solution of 9% ethyl alcohol in the B category, and a single aqueous solution of acetic acid/θ2 in the C category, each at 200%
and extracted for 3 days with stirring under sealed conditions.
Three types of extracts were obtained.

次に上記Aの抽出液について、2点比較法により夫々B
またはCの抽出液を対−堕で、20名のパネルによる官
能検査を実施したところ、下記第1表に記載の如き結果
が得られた。
Next, with respect to the above extract A, each of B
When the extract of C or C was subjected to a sensory test by a panel of 20 people, the results shown in Table 1 below were obtained.

第  /  表 以上の結果から、エチルアルコール(エタノール)・酢
酸の混合溶液を使用した区分Aは、エチルアルコール単
独溶液区分Bまたは酢酸単独溶液区分Cに比べて、香シ
が良くしかも強いことが明らかである。
From the results in Table 1 and above, it is clear that Category A, which uses a mixed solution of ethyl alcohol (ethanol) and acetic acid, has a better and stronger aroma than Category B, a solution containing ethyl alcohol alone, or Category C, a solution containing only acetic acid. It is.

即ち、本発明はエチルアルコールと酢酸を同時に用いる
ところに特徴があり、酢酸の代りに他の有機酸を用いて
も本発明の効果は得られない。例えば、香辛料の抽出を
、エチルアルコールと各種有機酸の一種からなる種々の
混合水溶液で抽出を行い、得られた抽出液の香、シの良
さ、強さについて官能試験を行ったところ、乳酸、クエ
ン酸、酒石酸、リンゴ酸などの有機酸に比べて、酢酸は
工を参考#=エチルアルコールの組合せにおいて、香辛
料の香気の抽出効果が格段に優れており、香シが優良で
しかも強い抽出液が得られた。
That is, the present invention is characterized in that ethyl alcohol and acetic acid are used simultaneously, and the effects of the present invention cannot be obtained even if other organic acids are used in place of acetic acid. For example, spices were extracted with various mixed aqueous solutions consisting of ethyl alcohol and various organic acids, and a sensory test was conducted to determine the aroma, pleasantness, and strength of the resulting extracts. Compared to organic acids such as citric acid, tartaric acid, and malic acid, acetic acid has a much better extracting effect on the aroma of spices when combined with ethyl alcohol, and is an extract with excellent aroma and strong aroma. was gotten.

また、混合水溶液のエチルアルコール濃度をj〜201
16(、V/v’)とすることも極めて重要であって、
その濃度が高過ぎると、得られる香辛料の抽出液はエチ
ルアルコール臭が強くなって、香辛料の香気とは異質の
香気を呈するようになシ、反対に低過ぎると香辛料の香
気成分の充分な抽出が出来ず、風味の貧弱な抽出液しか
得られない。また混合水溶液の酢酸濃度を5〜/j%(
W/V)とすることも極めて重要であって、その濃度が
高過ぎると、得られる香辛料の抽出液は酢酸臭が強くな
って、香辛料の香気とは異質の香気を呈するようになシ
、反対に低過ぎると風味の貧弱な抽出液しか得られない
In addition, the ethyl alcohol concentration of the mixed aqueous solution is j ~ 201
16 (, V/v') is also extremely important,
If the concentration is too high, the resulting spice extract will have a strong ethyl alcohol odor, giving it an aroma different from that of spices; However, only an extract with poor flavor can be obtained. In addition, the acetic acid concentration of the mixed aqueous solution was adjusted to 5~/j% (
W/V) is also extremely important; if the concentration is too high, the resulting spice extract will have a strong acetic acid odor, giving it an aroma different from that of spices. On the other hand, if it is too low, only an extract with poor flavor will be obtained.

即ち、エチルアルコールおよび酢酸の濃度が過不足の混
合水溶液を用いて香辛料を抽出しても本発明の如く、抽
出香辛料の風味を顕著に増強できない。
That is, even if spices are extracted using a mixed aqueous solution containing too much or too little concentration of ethyl alcohol and acetic acid, the flavor of the extracted spice cannot be significantly enhanced as in the present invention.

上記、香辛料の抽出に使用される、j−20%(V/V
 )のエチルアルコールおよび!〜/jチ(W/V )
の酢酸を含有する混合水溶液において、エチルアルコー
ルの代わシに、清酒、合成清酒、濁酒、白酒、味淋、焼
酎、ウィスキー、ブランデー、ラム、ジン等を上記アル
コール濃度範囲で使用することができ、また該混合水溶
液において、酢酸としては米酢、果実酢、穀物酢等の各
種醸造酢および合成酢酸水溶液を、上記酢酸濃度範囲で
使用することかで′きる。
J-20% (V/V
) of ethyl alcohol and! ~/jchi (W/V)
In the mixed aqueous solution containing acetic acid, in place of ethyl alcohol, refined sake, synthetic refined sake, turbid sake, baijiu, ajirin, shochu, whiskey, brandy, rum, gin, etc. can be used within the above alcohol concentration range, In the mixed aqueous solution, as the acetic acid, various brewed vinegars such as rice vinegar, fruit vinegar, and grain vinegar, and synthetic acetic acid aqueous solutions can be used within the acetic acid concentration range described above.

次に抽出に用いる混合水溶液は、香辛料に対し7〜30
倍(W/W ’)%に70〜20倍使用することが好ま
しい。使用量が多過ぎると香辛料の濃度が相対的に低く
なるので、あとで濃縮などの手段が必要となり、経済的
でなく、反対に少な過ぎると香辛料の香気の抽出を充分
に行うことができない。
Next, the mixed aqueous solution used for extraction has a ratio of 7 to 30% relative to the spice.
It is preferable to use 70 to 20 times (W/W')%. If the amount used is too large, the concentration of the spice will be relatively low, requiring means such as concentration afterwards, which is not economical, while if the amount is too small, the aroma of the spice cannot be extracted sufficiently.

次に抽出操作は密閉式タンク、開放式タンクのいずれで
行っても良いが、密閉式の方がアルコール、酢酸および
抽出香気の逸散を防止することができるので好ましい。
Next, the extraction operation may be performed in either a closed tank or an open tank, but a closed tank is preferable because it can prevent the alcohol, acetic acid, and extracted aroma from escaping.

抽出条件は、連続攪拌条件の場合/〜r日間、特に3〜
乙日間が好ましく、また時々攪拌する様な条件の場合で
はlθ〜≠θ日間、特に/j〜30日間が好ましい。即
ち香辛料の抽出操作を連続的攪拌条件下で行う場合、該
抽出液の経日的なフレーバー成分の増減をガスクロマト
グラフによる分析法で調べたところ、該抽出液は/−r
日間の範囲においてフレーバー成分の増加が見られ、特
に3〜6日間の範囲においては約3倍ものフレーバー成
分の増加が見られた。また香辛料の抽出操作を時々(例
えば2≠時間に7回の割合)攪拌する条件では該抽出液
は10−≠θ日日間おいてフレーバー成分の増加が見ら
れ、特に/j〜30日間においては著しいフレーバー成
分の増加が見られた。
Extraction conditions include continuous stirring for ~r days, especially for 3 ~
A period of 1 day is preferred, and in the case of occasional stirring, a period of lθ to ≠θ days, especially /j to 30 days is preferred. That is, when extracting spices under continuous stirring conditions, the increase and decrease of flavor components in the extract over time was investigated using gas chromatography analysis, and it was found that the extract was /-r.
An increase in flavor components was observed in the range of 3 to 6 days, and an increase of approximately 3 times in flavor components was observed especially in the range of 3 to 6 days. In addition, when the spice extraction operation is performed with occasional stirring (e.g., 7 times per 2≠hours), an increase in flavor components is observed in the extract after 10-≠θ days, and especially between /j and 30 days. A significant increase in flavor components was observed.

この際の抽出温度は20−50℃、特に20〜30℃が
好ましい。
The extraction temperature at this time is preferably 20-50°C, particularly 20-30°C.

このようにして、本発明によれば、風味が著しく増強さ
れた抽出香辛料を得ることができる。そして本発明方法
によって得られる抽出香辛料は、そのまま香辛味を有す
る調味料として用いても良いが、これに目的、用途に応
じてグルタミン酸ナトリウム、イノシン酸ナトリウム、
醤油等の調味料、魚介類エキス、肉エキス、その他を混
和して香辛調味料製品としてもよい。また、香辛料特有
の強い辛味、強く優れた香気を有しているので、ウスタ
ーソース、中濃ソース、トンカッソースな特に有効であ
る。
In this way, according to the present invention, extracted spices with significantly enhanced flavor can be obtained. The extracted spice obtained by the method of the present invention may be used as a seasoning having a spicy taste as it is, but depending on the purpose and use, it may be added to monosodium glutamate, sodium inosinate, etc.
It may also be mixed with seasonings such as soy sauce, seafood extract, meat extract, and others to produce a spice seasoning product. In addition, it has a strong spiciness and a strong aroma characteristic of spices, so it is particularly effective for Worcestershire sauce, Chuno sauce, and tonka sauce.

以下、実施例を示して、本発明をさらに詳細に説明する
Hereinafter, the present invention will be explained in further detail by showing examples.

実施例1 タイム101.セージ/θ2、フェンネル391クロー
ブ39.ペッパー/f1シンナモン30f1ナツメッグ
jf及び唐辛子7fをよく混合して調製した調合粉末天
然香辛料769を、エチルアルコールl0To (V/
V ”)および酢酸濃度として9% (W/V )とな
るように食酢(醸造酢)を混合した混合水溶液θ、/l
に加え、密閉条件下で連続攪拌して2j℃でj日間抽出
を行い、香辛料抽出液を得た。
Example 1 Time 101. Sage/θ2, Fennel 391 Clove 39. Pepper/f1 Cinnamon 30f1 Nutmeg jf and chili pepper 7f were mixed well to prepare blended powder natural spice 769, and ethyl alcohol l0To (V/
V'') and a mixed aqueous solution θ,/l of vinegar (brewed vinegar) mixed with acetic acid concentration of 9% (W/V).
In addition, extraction was performed for j days at 2j°C with continuous stirring under closed conditions to obtain a spice extract.

このようにして得られた抽出液は香辛味の著しく優れた
ものであった。
The extract obtained in this manner had an extremely excellent spiciness.

応用例/ タマネギroot1ニンジン!00?、)マドピユーレ
/、 2 tをコ四イドミルで砕き、約3tの水を加え
、均一に混和した後1I−j分間蒸煮し、布で濾過して
野菜母液を作成した。この野菜母液に食塩/、OKg、
糖蜜t!恥、醸造酢〔lのチ(W/V)’J1.2t、
砂糖1.7Kgを加え、水を加えて全量92tとし、加
熱溶解したのち、城女上記実施例/で得られた香辛料の
抽出液を加え、均一に攪拌し、密閉下で高温瞬間殺菌し
て、風味の格段に優れたウスターソース約1OLを得た
Application example/Onion root1 carrot! 00? , ) Madopyure/, 2 t was crushed in a cotetrioid mill, about 3 t of water was added, and after mixing uniformly, it was steamed for 1 I-j minutes and filtered through a cloth to prepare a vegetable mother liquor. Salt to this vegetable mother liquor/, OKg,
Molasses T! Shame, brewed vinegar [l no chi (W/V)'J1.2t,
Add 1.7 kg of sugar, add water to make a total volume of 92 tons, heat and dissolve, then add the spice extract obtained in the above example, stir evenly, and flash sterilize at high temperature under airtight conditions. Approximately 1 liter of Worcestershire sauce with a significantly superior flavor was obtained.

一方、比較の為、従来法に準じてウスターソースを製造
した。即ち上記の如−く調製した野菜母液に食塩tOK
9 ;糖蜜/、 j K9、醸造酢(10チ(W7v 
)’)I−71,砂糖/、 7 Kq、 上記実施例1
と同じ調合粉末天然香辛料7JS’、エチルアルコール
rOtdおよび水を加えて均一に攪拌し加熱溶解して対
照のウスターソース約/θtを得た。
On the other hand, for comparison, Worcestershire sauce was produced according to the conventional method. That is, add salt to the vegetable mother liquor prepared as above.
9; Molasses/, j K9, brewed vinegar (10 chi (W7v)
)') I-71, Sugar/, 7 Kq, Example 1 above
The same blended powdered natural spice 7JS', ethyl alcohol rOtd and water were added, stirred uniformly and dissolved by heating to obtain a control Worcestershire sauce approx./θt.

このようにして得られた2種類のウスターソースの味と
香りについて2≠名のパネルによυ官能検査を実施した
結果、第2表に記載の如き結果が得られた。尚、表中の
数字は良とした人数を示す。
A sensory test was conducted on the taste and aroma of the two types of Worcestershire sauce thus obtained by a panel of 2 people, and the results shown in Table 2 were obtained. The numbers in the table indicate the number of people who passed the test.

第  コ  表 (註)※+jチ有意差、※※:/%有意差この結果から
、本発明によれば風味の優れたウスターソースが得られ
ることが判る。
Table 3 (Note) *+j Significant difference, **: /% Significant difference From these results, it can be seen that according to the present invention, Worcestershire sauce with excellent flavor can be obtained.

実施例コ コシヨウ、タイム、セージ、セロリシード、ローレルお
よびクローブをよく混合して調製しるように食酢(醸造
酢)を混合水溶液コθθ−に加え、密閉下において連続
的に攪拌しながら、2、!t℃で3日間抽出を行い、濾
過処理して、香味の非常に増強された抽出香辛料を得た
Example Coconut, thyme, sage, celery seed, laurel and cloves were mixed well and table vinegar (brewed vinegar) was added to the mixed aqueous solution θθ-, and while continuously stirring under closed conditions, 2. ! Extraction was carried out for 3 days at t° C. and filtered to obtain extracted spices with highly enhanced flavor.

応用例コ タミン酸ナトリウム39を加え、均一に攪拌溶解し、サ
ラダオイル/20tttlを加え、均一に攪拌したのち
高温瞬間殺菌して、本発明のサラダドレッシングを作成
した。
Application Example Sodium cotamate 39 was added, stirred and dissolved uniformly, salad oil/20tttl was added, stirred uniformly and then sterilized at high temperature to create a salad dressing of the present invention.

一方比較のため、従来法に準じてサラダドレッシングを
調製した。即ち、酢酸濃度として5%(W/V)に々る
ように醸造酢を混合した酢酸水溶液200ttlに、上
記実施例コと同じ調合粉末天然香辛料/691工チルア
ルコール10m11食塩30f1グルタミン酸ナトリウ
ム!fおよびサラダオイル/2θmlを加え、均一に攪
拌し高温瞬間殺菌して対照のサラダドレッシングを調製
した。
On the other hand, for comparison, a salad dressing was prepared according to a conventional method. That is, to 200 ttl of acetic acid aqueous solution mixed with brewed vinegar so that the acetic acid concentration reaches 5% (W/V), the same powdered natural spices as in the above example / 10 ml of 691 industrial ethyl alcohol, 11 common salt, 30 f, 1 sodium glutamate! f and salad oil/2θml were added, stirred uniformly, and instant sterilized at high temperature to prepare a control salad dressing.

このようにして得られた。2種類のサラダドレッシング
につき、応用例/と同様に官能検査を実施したところ、
第3表に記載の如き結果が得られた。
Obtained in this way. When we conducted a sensory test on two types of salad dressings in the same way as in the application example,
The results shown in Table 3 were obtained.

この結果から、本発明によれば香味の優れたサラダドレ
ッシングが得られることが判る。
This result shows that according to the present invention, a salad dressing with excellent flavor can be obtained.

第   3   表 (註)※:jチ有意差Table 3 (Note) *: Significant difference

Claims (1)

【特許請求の範囲】[Claims] 天然香辛料を、j−20% (V/V)のエチルアルコ
ールおよびj〜/、!1%(W/V)の酢酸を含有する
混合水溶液で抽出することを特徴とする風味の改良され
た抽出香辛料の製造法。
Natural spices, j-20% (V/V) ethyl alcohol and j~/,! A method for producing an extracted spice with improved flavor, which comprises extracting with a mixed aqueous solution containing 1% (W/V) acetic acid.
JP56209716A 1981-12-28 1981-12-28 Preparation of extracted spice having improved taste and flavor Pending JPS58121770A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP56209716A JPS58121770A (en) 1981-12-28 1981-12-28 Preparation of extracted spice having improved taste and flavor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56209716A JPS58121770A (en) 1981-12-28 1981-12-28 Preparation of extracted spice having improved taste and flavor

Publications (1)

Publication Number Publication Date
JPS58121770A true JPS58121770A (en) 1983-07-20

Family

ID=16577456

Family Applications (1)

Application Number Title Priority Date Filing Date
JP56209716A Pending JPS58121770A (en) 1981-12-28 1981-12-28 Preparation of extracted spice having improved taste and flavor

Country Status (1)

Country Link
JP (1) JPS58121770A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06209745A (en) * 1991-12-24 1994-08-02 Tokyo Met Gov Soosu Kogyo Kyodo Kumiai Production of sauce
JPH07308170A (en) * 1994-05-18 1995-11-28 Shinguru Seru Shokuhin Kk Food improved in antimutagenic titer
KR100623003B1 (en) 2004-12-22 2006-09-14 전북대학교산학협력단 Manufacturing Method of Ginger Extract using Ultrasonication
JP2010162009A (en) * 2009-01-13 2010-07-29 Sato Shokuhin Kogyo Kk Hot-taste seasoning

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06209745A (en) * 1991-12-24 1994-08-02 Tokyo Met Gov Soosu Kogyo Kyodo Kumiai Production of sauce
JPH07308170A (en) * 1994-05-18 1995-11-28 Shinguru Seru Shokuhin Kk Food improved in antimutagenic titer
KR100623003B1 (en) 2004-12-22 2006-09-14 전북대학교산학협력단 Manufacturing Method of Ginger Extract using Ultrasonication
JP2010162009A (en) * 2009-01-13 2010-07-29 Sato Shokuhin Kogyo Kk Hot-taste seasoning

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