JPH03208897A - ＴｉＣウィスカーの製造法 - Google Patents
ＴｉＣウィスカーの製造法Info
- Publication number
- JPH03208897A JPH03208897A JP311090A JP311090A JPH03208897A JP H03208897 A JPH03208897 A JP H03208897A JP 311090 A JP311090 A JP 311090A JP 311090 A JP311090 A JP 311090A JP H03208897 A JPH03208897 A JP H03208897A
- Authority
- JP
- Japan
- Prior art keywords
- whiskers
- tic
- reaction
- hydrogen
- titanium tetrachloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 238000006243 chemical reaction Methods 0.000 claims abstract description 36
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims abstract description 19
- 229910052723 transition metal Inorganic materials 0.000 claims abstract description 6
- 150000003624 transition metals Chemical class 0.000 claims abstract description 6
- 239000001257 hydrogen Substances 0.000 claims description 20
- 229910052739 hydrogen Inorganic materials 0.000 claims description 20
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 16
- 239000007789 gas Substances 0.000 claims description 11
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000010574 gas phase reaction Methods 0.000 claims description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract description 45
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 15
- 239000010936 titanium Substances 0.000 abstract description 15
- 229910052799 carbon Inorganic materials 0.000 abstract description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052719 titanium Inorganic materials 0.000 abstract description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 3
- 239000001301 oxygen Substances 0.000 abstract description 3
- 229910052760 oxygen Inorganic materials 0.000 abstract description 3
- 239000008246 gaseous mixture Substances 0.000 abstract 3
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- 229910003074 TiCl4 Inorganic materials 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 239000012808 vapor phase Substances 0.000 abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 14
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000002994 raw material Substances 0.000 description 8
- 238000002441 X-ray diffraction Methods 0.000 description 7
- 229910002804 graphite Inorganic materials 0.000 description 7
- 239000010439 graphite Substances 0.000 description 7
- 229910052759 nickel Inorganic materials 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 230000002194 synthesizing effect Effects 0.000 description 3
- -1 Au as a catalyst Chemical class 0.000 description 2
- 229920002430 Fibre-reinforced plastic Polymers 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000011151 fibre-reinforced plastic Substances 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 2
- 229910000510 noble metal Inorganic materials 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000012779 reinforcing material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical compound [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 1
- 229910001981 cobalt nitrate Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011226 reinforced ceramic Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP311090A JPH03208897A (ja) | 1990-01-10 | 1990-01-10 | ＴｉＣウィスカーの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP311090A JPH03208897A (ja) | 1990-01-10 | 1990-01-10 | ＴｉＣウィスカーの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH03208897A true JPH03208897A (ja) | 1991-09-12 |
| JPH0583518B2 JPH0583518B2 (enrdf_load_stackoverflow) | 1993-11-26 |
Family
ID=11548213
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP311090A Granted JPH03208897A (ja) | 1990-01-10 | 1990-01-10 | ＴｉＣウィスカーの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH03208897A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5336291A (en) * | 1992-07-02 | 1994-08-09 | Toyota Jidosha Kabushiki Kaisha | Method of production of a metallic composite material incorporating metal carbide particles dispersed therein |
| US5441697A (en) * | 1992-08-06 | 1995-08-15 | Toyota Jidosha Kabushiki Kaisha | Method of producing TiC whiskers and metallic composites reinforced by TiC whiskers |
-
1990
- 1990-01-10 JP JP311090A patent/JPH03208897A/ja active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5336291A (en) * | 1992-07-02 | 1994-08-09 | Toyota Jidosha Kabushiki Kaisha | Method of production of a metallic composite material incorporating metal carbide particles dispersed therein |
| US5441697A (en) * | 1992-08-06 | 1995-08-15 | Toyota Jidosha Kabushiki Kaisha | Method of producing TiC whiskers and metallic composites reinforced by TiC whiskers |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0583518B2 (enrdf_load_stackoverflow) | 1993-11-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Boehm | Carbon from carbon monoxide disproportionation on nickel and iron catalysts: Morphological studies and possible growth mechanisms | |
| US4756791A (en) | Chemical vapor deposition process for producing metal carbide or nitride whiskers | |
| US4988564A (en) | Metal carbide, nitride, or carbonitride whiskers coated with metal carbides, nitrides, carbonitrides, or oxides | |
| US20060051281A1 (en) | Metal carbides and process for producing same | |
| EP0174622B1 (en) | A process for preparing fine fibers | |
| US4552740A (en) | Process for producing amorphous and crystalline silicon nitride | |
| JPH03208897A (ja) | ＴｉＣウィスカーの製造法 | |
| US7371359B2 (en) | Non-aqueous borate routes to boron nitride | |
| US4810530A (en) | Method of coating metal carbide nitride, and carbonitride whiskers with metal carbides, nitrides, carbonitrides, or oxides | |
| JPH03208898A (ja) | ＴｉＣウィスカーの製造方法 | |
| US5160574A (en) | Process for production of small diameter titanium carbide whiskers | |
| JPH09169522A (ja) | チタンの炭化物、窒化物および炭窒化物ホィスカーの製造方法 | |
| JPS6278217A (ja) | 気相法炭素繊維の製造法 | |
| JPS644999B2 (enrdf_load_stackoverflow) | ||
| JPH02233511A (ja) | ダイヤモンドの製造方法 | |
| JPS645000B2 (enrdf_load_stackoverflow) | ||
| JPH0648891A (ja) | ダイヤモンドの製造方法 | |
| JPS59164606A (ja) | ダイヤモンド合成法 | |
| JPS634069A (ja) | 熱分解黒鉛の製造方法 | |
| JPH0234599A (ja) | コイル状窒化珪素ウイスカーの製造方法 | |
| Bhat et al. | An examination of the growth models for TiC whiskers made by CVD | |
| JPS5945636B2 (ja) | 炭化ケイ素ウイスカ−の製造方法 | |
| JPS5874598A (ja) | 繊維状窒化珪素の製造方法 | |
| JPS62202809A (ja) | 熱分解黒鉛の製造方法 | |
| JPH0637284B2 (ja) | 窒化クロムの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |