JPH03141113A - クロルシランの不均化法 - Google Patents
クロルシランの不均化法Info
- Publication number
- JPH03141113A JPH03141113A JP2201579A JP20157990A JPH03141113A JP H03141113 A JPH03141113 A JP H03141113A JP 2201579 A JP2201579 A JP 2201579A JP 20157990 A JP20157990 A JP 20157990A JP H03141113 A JPH03141113 A JP H03141113A
- Authority
- JP
- Japan
- Prior art keywords
- formulas
- tables
- chemical formulas
- mathematical
- mathematical formulas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 239000005046 Chlorosilane Substances 0.000 title claims abstract description 14
- 238000007323 disproportionation reaction Methods 0.000 title abstract description 11
- 239000003054 catalyst Substances 0.000 claims abstract description 19
- 239000007791 liquid phase Substances 0.000 claims abstract description 8
- 239000012071 phase Substances 0.000 claims abstract description 8
- 125000000524 functional group Chemical group 0.000 claims abstract description 7
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 7
- 125000002947 alkylene group Chemical group 0.000 claims abstract 7
- 239000003431 cross linking reagent Substances 0.000 claims abstract 5
- 229920001296 polysiloxane Polymers 0.000 claims abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims abstract 2
- 239000000126 substance Substances 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 150000001412 amines Chemical class 0.000 claims description 4
- 150000001450 anions Chemical class 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 4
- 125000002993 cycloalkylene group Chemical group 0.000 claims 3
- 239000002245 particle Substances 0.000 claims 3
- 239000011148 porous material Substances 0.000 claims 3
- 239000012798 spherical particle Substances 0.000 claims 3
- 150000003868 ammonium compounds Chemical class 0.000 claims 2
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims 2
- 125000000753 cycloalkyl group Chemical group 0.000 claims 2
- 230000000704 physical effect Effects 0.000 claims 2
- 239000000843 powder Substances 0.000 claims 2
- 239000004971 Cross linker Substances 0.000 claims 1
- 125000000008 (C1-C10) alkyl group Chemical group 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 238000000465 moulding Methods 0.000 abstract 1
- MROCJMGDEKINLD-UHFFFAOYSA-N dichlorosilane Chemical compound Cl[SiH2]Cl MROCJMGDEKINLD-UHFFFAOYSA-N 0.000 description 7
- 150000002500 ions Chemical class 0.000 description 5
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 5
- 239000005052 trichlorosilane Substances 0.000 description 4
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical group [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000004793 Polystyrene Substances 0.000 description 2
- 239000002638 heterogeneous catalyst Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229920000620 organic polymer Polymers 0.000 description 2
- 229920002223 polystyrene Polymers 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- ICSWLKDKQBNKAY-UHFFFAOYSA-N 1,1,3,3,5,5-hexamethyl-1,3,5-trisilinane Chemical compound C[Si]1(C)C[Si](C)(C)C[Si](C)(C)C1 ICSWLKDKQBNKAY-UHFFFAOYSA-N 0.000 description 1
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 125000006615 aromatic heterocyclic group Chemical group 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 229920001429 chelating resin Polymers 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 229920006037 cross link polymer Polymers 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 125000002147 dimethylamino group Chemical group [H]C([H])([H])N(*)C([H])([H])[H] 0.000 description 1
- 150000002009 diols Chemical class 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000006459 hydrosilylation reaction Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 125000000250 methylamino group Chemical group [H]N(*)C([H])([H])[H] 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N phosphonic acid group Chemical group P(O)(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000005049 silicon tetrachloride Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/107—Halogenated silanes
- C01B33/10773—Halogenated silanes obtained by disproportionation and molecular rearrangement of halogenated silanes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
- C01B33/043—Monosilane
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Polymers (AREA)
- Catalysts (AREA)
- Silicon Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3925357.0 | 1989-07-31 | ||
| DE3925357A DE3925357C1 (enExample) | 1989-07-31 | 1989-07-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH03141113A true JPH03141113A (ja) | 1991-06-17 |
Family
ID=6386238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2201579A Pending JPH03141113A (ja) | 1989-07-31 | 1990-07-31 | クロルシランの不均化法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5094831A (enExample) |
| EP (1) | EP0411471B1 (enExample) |
| JP (1) | JPH03141113A (enExample) |
| AT (1) | ATE84280T1 (enExample) |
| CA (1) | CA2022222C (enExample) |
| DE (2) | DE3925357C1 (enExample) |
| DK (1) | DK0411471T3 (enExample) |
| ES (1) | ES2053029T3 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012532828A (ja) * | 2009-07-15 | 2012-12-20 | エボニック デグサ ゲーエムベーハー | ハロゲンシランを不均化するため及び異種金属を除去するための方法及びアミノ官能性樹脂の使用 |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3800564C1 (enExample) * | 1988-01-12 | 1989-03-16 | Degussa Ag, 6000 Frankfurt, De | |
| DE4035033C1 (enExample) * | 1990-11-03 | 1992-04-02 | Degussa Ag, 6000 Frankfurt, De | |
| DE4035032C1 (enExample) * | 1990-11-03 | 1992-04-30 | Degussa Ag, 6000 Frankfurt, De | |
| DE4110705C1 (enExample) * | 1991-04-03 | 1992-10-22 | Degussa Ag, 6000 Frankfurt, De | |
| DE4130643A1 (de) * | 1991-09-14 | 1993-03-18 | Degussa | Verfahren zur reinigung von alkoxysilanen |
| DE4142129C1 (enExample) * | 1991-12-20 | 1993-07-01 | Degussa Ag, 6000 Frankfurt, De | |
| DE4223539C1 (de) * | 1992-07-17 | 1993-11-25 | Degussa | Geformte Sulfonatgruppen-haltige Organopolysiloxane, Verfahren zu ihrer Herstellung und Verwendung |
| US5466767A (en) * | 1992-08-06 | 1995-11-14 | Degussa Aktiengesellschaft | Shaped organosiloxane polycondensates, process for their preparation and use |
| DE4240730A1 (de) * | 1992-12-03 | 1994-06-09 | Wacker Chemie Gmbh | Verfahren zur Herstellung von Dimethylchlorsilan |
| DE4409140A1 (de) * | 1994-03-17 | 1995-09-21 | Degussa | Wäßrige Lösungen von Organopolysiloxan-Ammoniumverbindungen, ihre Herstellung und Verwendung |
| DE102004045245B4 (de) * | 2004-09-17 | 2007-11-15 | Degussa Gmbh | Vorrichtung und Verfahren zur Herstellung von Silanen |
| DE102005046105B3 (de) * | 2005-09-27 | 2007-04-26 | Degussa Gmbh | Verfahren zur Herstellung von Monosilan |
| US20070173597A1 (en) * | 2006-01-20 | 2007-07-26 | Williams David A | Sealant composition containing inorganic-organic nanocomposite filler |
| US7687121B2 (en) * | 2006-01-20 | 2010-03-30 | Momentive Performance Materials Inc. | Insulated glass unit with sealant composition having reduced permeability to gas |
| US7531613B2 (en) * | 2006-01-20 | 2009-05-12 | Momentive Performance Materials Inc. | Inorganic-organic nanocomposite |
| DE102007059170A1 (de) | 2007-12-06 | 2009-06-10 | Evonik Degussa Gmbh | Katalysator und Verfahren zur Dismutierung von Wasserstoff enthaltenden Halogensilanen |
| DE102010043649A1 (de) | 2010-11-09 | 2012-05-10 | Evonik Degussa Gmbh | Verfahren zur Spaltung höherer Silane |
| DE102010043648A1 (de) | 2010-11-09 | 2012-05-10 | Evonik Degussa Gmbh | Verfahren zur selektiven Spaltung höherer Silane |
| DE102011004058A1 (de) | 2011-02-14 | 2012-08-16 | Evonik Degussa Gmbh | Monochlorsilan, Verfahren und Vorrichtung zu dessen Herstellung |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2732282A (en) * | 1956-01-24 | Cjhssihclj | ||
| BE523301A (enExample) * | 1952-10-29 | 1953-10-31 | ||
| US2834648A (en) * | 1953-03-25 | 1958-05-13 | Union Carbide Corp | Disproportionation of chlorosilanes employing amine-type catalysts |
| DE1251762B (de) * | 1965-03-19 | 1967-10-12 | Rhone Poulenc SA, Paris | Verfahren zur Dismutation von Chlorhydrogen silanen |
| BE784818A (fr) * | 1971-06-14 | 1972-12-13 | Westinghouse Electric Corp | Etalonnage du profil de deplacement de la position d'un entrainement par moteur |
| US3968199A (en) * | 1974-02-25 | 1976-07-06 | Union Carbide Corporation | Process for making silane |
| US4676967A (en) * | 1978-08-23 | 1987-06-30 | Union Carbide Corporation | High purity silane and silicon production |
| CA1162028A (en) * | 1979-08-01 | 1984-02-14 | Larry M. Coleman | Ultrahigh purity silane and silicon production |
| CA1184017A (en) * | 1980-08-28 | 1985-03-19 | Larry M. Coleman | Ultrahigh purity silane and silicon production with recycle of silane products |
| DE3131954C2 (de) * | 1981-08-13 | 1984-10-31 | Degussa Ag, 6000 Frankfurt | Metallkomplexe von polymeren, gegebenenfalls vernetzten Organosiloxanaminen, Verfahren zu ihrer Herstellung und Verwendung |
| JPS6042216A (ja) * | 1983-08-10 | 1985-03-06 | Osaka Titanium Seizo Kk | トリクロロシラン・ジクロロシラン・モノクロロシランの不均斉化方法 |
| FR2552434B1 (fr) * | 1983-09-28 | 1985-10-25 | Rhone Poulenc Spec Chim | Procede de fabrication de silane a partir de methyldichlorosilane et de chlorosilanes |
| DE3404702A1 (de) * | 1984-02-10 | 1985-09-05 | Degussa Ag, 6000 Frankfurt | Platin- und/oder palladium-haltige organopolysiloxan-ammoniumverbindungen, verfahren zu ihrer herstellung und verwendung |
| US4610858A (en) * | 1984-04-06 | 1986-09-09 | Denki Kagaku Kogyo Kabushiki Kaisha | Chlorosilane disproportionation catalyst and method for producing a silane compound by means of the catalyst |
| US4613491A (en) * | 1984-05-17 | 1986-09-23 | Korea Advanced Institute Of Science And Technology | Redistribution catalyst and methods for its preparation and use to convert chlorosilicon hydrides to silane |
| DE3711444A1 (de) * | 1987-04-04 | 1988-10-13 | Huels Troisdorf | Verfahren und vorrichtung zur herstellung von dichlorsilan |
| DE3712098A1 (de) * | 1987-04-10 | 1988-10-20 | Wacker Chemie Gmbh | Verfahren zur herstellung von disproportionierungsprodukten von dichlormethylsilan in gegenwart eines katalysators |
| DE3800563C1 (enExample) * | 1988-01-12 | 1989-03-16 | Degussa Ag, 6000 Frankfurt, De |
-
1989
- 1989-07-31 DE DE3925357A patent/DE3925357C1/de not_active Expired - Lifetime
-
1990
- 1990-07-26 AT AT90114312T patent/ATE84280T1/de not_active IP Right Cessation
- 1990-07-26 DE DE9090114312T patent/DE59000718D1/de not_active Expired - Fee Related
- 1990-07-26 ES ES90114312T patent/ES2053029T3/es not_active Expired - Lifetime
- 1990-07-26 EP EP90114312A patent/EP0411471B1/de not_active Expired - Lifetime
- 1990-07-26 DK DK90114312.3T patent/DK0411471T3/da active
- 1990-07-30 US US07/558,868 patent/US5094831A/en not_active Expired - Fee Related
- 1990-07-30 CA CA002022222A patent/CA2022222C/en not_active Expired - Fee Related
- 1990-07-31 JP JP2201579A patent/JPH03141113A/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012532828A (ja) * | 2009-07-15 | 2012-12-20 | エボニック デグサ ゲーエムベーハー | ハロゲンシランを不均化するため及び異種金属を除去するための方法及びアミノ官能性樹脂の使用 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE59000718D1 (de) | 1993-02-18 |
| EP0411471B1 (de) | 1993-01-07 |
| US5094831A (en) | 1992-03-10 |
| DE3925357C1 (enExample) | 1991-04-25 |
| CA2022222C (en) | 1996-06-18 |
| ATE84280T1 (de) | 1993-01-15 |
| ES2053029T3 (es) | 1994-07-16 |
| DK0411471T3 (da) | 1993-05-10 |
| EP0411471A1 (de) | 1991-02-06 |
| CA2022222A1 (en) | 1991-02-01 |
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