JPH0241537B2 - - Google Patents
Info
- Publication number
- JPH0241537B2 JPH0241537B2 JP56191874A JP19187481A JPH0241537B2 JP H0241537 B2 JPH0241537 B2 JP H0241537B2 JP 56191874 A JP56191874 A JP 56191874A JP 19187481 A JP19187481 A JP 19187481A JP H0241537 B2 JPH0241537 B2 JP H0241537B2
- Authority
- JP
- Japan
- Prior art keywords
- residue
- polymer
- dcp
- polyquaternary
- propanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- ROSDSFDQCJNGOL-UHFFFAOYSA-N protonated dimethyl amine Natural products CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 claims description 45
- 229920000642 polymer Polymers 0.000 claims description 33
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 12
- 125000005265 dialkylamine group Chemical group 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 6
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 5
- 150000001412 amines Chemical class 0.000 claims description 5
- 125000002147 dimethylamino group Chemical group [H]C([H])([H])N(*)C([H])([H])[H] 0.000 claims description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 238000007792 addition Methods 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 description 21
- 239000000701 coagulant Substances 0.000 description 14
- 239000007795 chemical reaction product Substances 0.000 description 12
- JGVZJRHAZOBPMW-UHFFFAOYSA-N 1,3-bis(dimethylamino)propan-2-ol Chemical compound CN(C)CC(O)CN(C)C JGVZJRHAZOBPMW-UHFFFAOYSA-N 0.000 description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N 2-propanol Substances CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 2
- 239000003471 mutagenic agent Substances 0.000 description 2
- 231100000707 mutagenic chemical Toxicity 0.000 description 2
- 230000003505 mutagenic effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- VEFLKXRACNJHOV-UHFFFAOYSA-N 1,3-dibromopropane Chemical compound BrCCCBr VEFLKXRACNJHOV-UHFFFAOYSA-N 0.000 description 1
- 229940051269 1,3-dichloro-2-propanol Drugs 0.000 description 1
- NCXUNZWLEYGQAH-UHFFFAOYSA-N 1-(dimethylamino)propan-2-ol Chemical compound CC(O)CN(C)C NCXUNZWLEYGQAH-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 125000004663 dialkyl amino group Chemical group 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- CTQYLOABGNIMLI-UHFFFAOYSA-N n,n,n',n'-tetramethylpropane-1,3-diamine Chemical compound CN(C)CCCN(C)C.CN(C)CCCN(C)C CTQYLOABGNIMLI-UHFFFAOYSA-N 0.000 description 1
- DMQSHEKGGUOYJS-UHFFFAOYSA-N n,n,n',n'-tetramethylpropane-1,3-diamine Chemical compound CN(C)CCCN(C)C DMQSHEKGGUOYJS-UHFFFAOYSA-N 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
- C08G73/0206—Polyalkylene(poly)amines
- C08G73/0213—Preparatory process
- C08G73/022—Preparatory process from polyamines and epihalohydrins
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
- C08G73/0206—Polyalkylene(poly)amines
- C08G73/0213—Preparatory process
- C08G73/0226—Quaternisation of polyalkylene(poly)amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Engineering & Computer Science (AREA)
- Hydrology & Water Resources (AREA)
- Life Sciences & Earth Sciences (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/213,300 US4319020A (en) | 1980-12-05 | 1980-12-05 | Polyquaternary flocculants |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS57121033A JPS57121033A (en) | 1982-07-28 |
| JPH0241537B2 true JPH0241537B2 (cg-RX-API-DMAC10.html) | 1990-09-18 |
Family
ID=22794539
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP56191874A Granted JPS57121033A (en) | 1980-12-05 | 1981-12-01 | Manufacture of polyquaternary polymer |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4319020A (cg-RX-API-DMAC10.html) |
| EP (1) | EP0053733B1 (cg-RX-API-DMAC10.html) |
| JP (1) | JPS57121033A (cg-RX-API-DMAC10.html) |
| AR (1) | AR225988A1 (cg-RX-API-DMAC10.html) |
| AU (1) | AU548049B2 (cg-RX-API-DMAC10.html) |
| BR (1) | BR8107798A (cg-RX-API-DMAC10.html) |
| CA (1) | CA1180848A (cg-RX-API-DMAC10.html) |
| DE (1) | DE3170640D1 (cg-RX-API-DMAC10.html) |
| ES (1) | ES507686A0 (cg-RX-API-DMAC10.html) |
| MX (1) | MX159331A (cg-RX-API-DMAC10.html) |
| PH (1) | PH18092A (cg-RX-API-DMAC10.html) |
| SG (1) | SG75386G (cg-RX-API-DMAC10.html) |
| ZA (1) | ZA818453B (cg-RX-API-DMAC10.html) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4569991A (en) * | 1982-01-26 | 1986-02-11 | Mitsubishi Monsanto Chemical Company | Production of thermoplastic resin |
| US4831116A (en) * | 1987-08-17 | 1989-05-16 | The Dow Chemical Company | Process for coagulating a grafted rubber compound |
| EP0581002A2 (en) * | 1992-07-30 | 1994-02-02 | Cytec Technology Corp. | Use of blends of mannich acrylamide polymers and quaternary polyamines for flocculating enzyme broth streams |
| US5639449A (en) * | 1994-08-17 | 1997-06-17 | Avlon Industries, Inc. | Hair strengthening composition and method |
| CN103347818B (zh) * | 2011-02-10 | 2015-09-02 | 运水高有限公司 | 用于水处理的杀生物剂组合物 |
| CN104822459A (zh) * | 2012-12-20 | 2015-08-05 | 阿克佐诺贝尔化学国际公司 | 在钾碱矿的泡沫浮选方法中作为抑制剂的聚季铵聚合物 |
| FR3125049B1 (fr) * | 2021-07-09 | 2024-04-26 | Snf Sa | Polymère cationique biosourcé à haute densité de charge |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3755159A (en) * | 1968-11-26 | 1973-08-28 | American Cyanamid Co | Flocculation by methylamine-epichlorohydrin polymer |
| USRE28807E (en) | 1972-02-04 | 1976-05-11 | American Cyanamid Company | Polyquaternary flocculants |
| USRE28808E (en) | 1972-02-04 | 1976-05-11 | American Cyanamid Company | Polyquaternary flocculants |
| US3954680A (en) * | 1974-05-06 | 1976-05-04 | Nalco Chemical Company | Stabilized electroconductive polymers |
| US4054542A (en) * | 1975-04-14 | 1977-10-18 | Buckman Laboratories, Inc. | Amine-epichlorohydrin polymeric compositions |
-
1980
- 1980-12-05 US US06/213,300 patent/US4319020A/en not_active Expired - Lifetime
-
1981
- 1981-10-14 CA CA000387837A patent/CA1180848A/en not_active Expired
- 1981-10-23 PH PH26382A patent/PH18092A/en unknown
- 1981-11-05 EP EP81109517A patent/EP0053733B1/en not_active Expired
- 1981-11-05 DE DE8181109517T patent/DE3170640D1/de not_active Expired
- 1981-11-26 MX MX190295A patent/MX159331A/es unknown
- 1981-11-30 BR BR8107798A patent/BR8107798A/pt not_active IP Right Cessation
- 1981-12-01 JP JP56191874A patent/JPS57121033A/ja active Granted
- 1981-12-03 ES ES507686A patent/ES507686A0/es active Granted
- 1981-12-03 AR AR287693A patent/AR225988A1/es active
- 1981-12-04 AU AU78271/81A patent/AU548049B2/en not_active Ceased
- 1981-12-04 ZA ZA818453A patent/ZA818453B/xx unknown
-
1986
- 1986-09-18 SG SG753/86A patent/SG75386G/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0053733B1 (en) | 1985-05-22 |
| AU7827181A (en) | 1982-06-10 |
| US4319020A (en) | 1982-03-09 |
| MX159331A (es) | 1989-05-17 |
| BR8107798A (pt) | 1982-08-31 |
| CA1180848A (en) | 1985-01-08 |
| PH18092A (en) | 1985-03-20 |
| EP0053733A1 (en) | 1982-06-16 |
| ES8207201A1 (es) | 1982-09-01 |
| AR225988A1 (es) | 1982-05-14 |
| DE3170640D1 (en) | 1985-06-27 |
| ZA818453B (en) | 1982-10-27 |
| AU548049B2 (en) | 1985-11-21 |
| SG75386G (en) | 1987-10-23 |
| JPS57121033A (en) | 1982-07-28 |
| ES507686A0 (es) | 1982-09-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA2721478C (en) | Functionalized cationic polyamines and their use to reduce the ndma formation during the treatment of aqueous systems, and applications in the water treatment industry, includingwastewater and drinking water treatment processes | |
| EP0469891B1 (en) | Process for the production of improved polyaminopolyamide epichlorohydrin resins | |
| JP3305695B2 (ja) | 低減されたハロゲン含量を持つポリアミノアミド‐エピクロロヒドリン樹脂 | |
| EP0641818A1 (en) | Resins with reduced epichlorohydrin hydrolysates | |
| JP2656952B2 (ja) | 望ましくないハロゲン含量が低いエポキシ樹脂の製造方法 | |
| JP4339419B2 (ja) | アルコキシル化オルガノシリコーン樹脂 | |
| KR20020058082A (ko) | 에피할로히드린 유래의 에폭시 수지로부터 가수분해가능한 할로겐화물을 함유하는 물질과 다른 고분자량물질을 제거하는 방법 | |
| CN1195731C (zh) | 纯化三乙醇胺的方法 | |
| EP0053733B1 (en) | Polyquaternary flocculants | |
| JP4104773B2 (ja) | 浄水用凝集剤の製造方法 | |
| US4325940A (en) | Anti-microbial, cosmetic and water-treating ionene polymeric compounds | |
| CA1270077A (en) | Process for reducing the content of trihalomethane compounds and precursors thereof in influent water | |
| US3975347A (en) | Linear dimethylamine-epichlorohydrin copolymer | |
| US3595921A (en) | Reducing the color content of polyethylene polyamines prepared by the reaction of ammonia with ethylene dichloride | |
| JPH0517463A (ja) | 高純度エポキシ樹脂の製造方法 | |
| US4209397A (en) | Flocculants for aqueous systems | |
| JP2004211028A (ja) | エポキシ樹脂の精製方法及び半導体封止用エポキシ樹脂組成物 | |
| KR20000062736A (ko) | 메틸메타크릴레이트의 제조방법 | |
| JP3009194B2 (ja) | エポキシ樹脂用硬化剤 | |
| JPH05213920A (ja) | グリシジル化合物の精製方法 | |
| KR100498173B1 (ko) | 에피클로로히드린의 사용량을 최소화한 폴리아민계고분자의 제조방법 | |
| KR100219261B1 (ko) | 폴리에틸렌폴리아민류 제조시 발생되는 폐수의 처리방법 | |
| JPS6038430A (ja) | ポリアミノ化合物の製造法 | |
| JPS61249590A (ja) | 金属捕集剤 | |
| JPH0338261B2 (cg-RX-API-DMAC10.html) |