JPH0235733B2 - - Google Patents
Info
- Publication number
- JPH0235733B2 JPH0235733B2 JP58028262A JP2826283A JPH0235733B2 JP H0235733 B2 JPH0235733 B2 JP H0235733B2 JP 58028262 A JP58028262 A JP 58028262A JP 2826283 A JP2826283 A JP 2826283A JP H0235733 B2 JPH0235733 B2 JP H0235733B2
- Authority
- JP
- Japan
- Prior art keywords
- phenolate
- reaction
- phenol
- water
- potassium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 18
- 229940031826 phenolate Drugs 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 11
- 229910052783 alkali metal Inorganic materials 0.000 claims description 8
- -1 alkali metal phenolate Chemical class 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 5
- 239000003209 petroleum derivative Substances 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-M phenolate Chemical compound [O-]C1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-M 0.000 description 11
- 238000000034 method Methods 0.000 description 10
- ZGJADVGJIVEEGF-UHFFFAOYSA-M potassium;phenoxide Chemical compound [K+].[O-]C1=CC=CC=C1 ZGJADVGJIVEEGF-UHFFFAOYSA-M 0.000 description 8
- 230000018044 dehydration Effects 0.000 description 7
- 238000006297 dehydration reaction Methods 0.000 description 7
- 239000003350 kerosene Substances 0.000 description 7
- 230000021523 carboxylation Effects 0.000 description 6
- 238000006473 carboxylation reaction Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 230000004927 fusion Effects 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 150000004707 phenolate Chemical class 0.000 description 2
- NESLWCLHZZISNB-UHFFFAOYSA-M sodium phenolate Chemical compound [Na+].[O-]C1=CC=CC=C1 NESLWCLHZZISNB-UHFFFAOYSA-M 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000007065 Kolbe-Schmitt synthesis reaction Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2826283A JPS59155334A (ja) | 1983-02-21 | 1983-02-21 | アルカリ金属フエノラ−トの製造法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2826283A JPS59155334A (ja) | 1983-02-21 | 1983-02-21 | アルカリ金属フエノラ−トの製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS59155334A JPS59155334A (ja) | 1984-09-04 |
JPH0235733B2 true JPH0235733B2 (fr) | 1990-08-13 |
Family
ID=12243654
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2826283A Granted JPS59155334A (ja) | 1983-02-21 | 1983-02-21 | アルカリ金属フエノラ−トの製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS59155334A (fr) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5025054B2 (ja) * | 2001-08-23 | 2012-09-12 | 上野製薬株式会社 | パラヒドロキシ安息香酸の製造方法 |
JP5164119B2 (ja) * | 2009-02-19 | 2013-03-13 | 田岡化学工業株式会社 | 2−(2,4−ジ−tert−アミルフェノキシ)脂肪酸クロリドの製造方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4915253A (fr) * | 1972-06-01 | 1974-02-09 |
-
1983
- 1983-02-21 JP JP2826283A patent/JPS59155334A/ja active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4915253A (fr) * | 1972-06-01 | 1974-02-09 |
Also Published As
Publication number | Publication date |
---|---|
JPS59155334A (ja) | 1984-09-04 |
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