JP7610207B2 - ベリリウム溶液の製造方法、ベリリウムの製造方法、水酸化ベリリウムの製造方法、酸化ベリリウムの製造方法、及び、ベリリウム酸化物の製造方法 - Google Patents

ベリリウム溶液の製造方法、ベリリウムの製造方法、水酸化ベリリウムの製造方法、酸化ベリリウムの製造方法、及び、ベリリウム酸化物の製造方法 Download PDF

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JP7610207B2
JP7610207B2 JP2021542982A JP2021542982A JP7610207B2 JP 7610207 B2 JP7610207 B2 JP 7610207B2 JP 2021542982 A JP2021542982 A JP 2021542982A JP 2021542982 A JP2021542982 A JP 2021542982A JP 7610207 B2 JP7610207 B2 JP 7610207B2
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beryllium
solution
producing
oxide
heating step
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勝 中道
宰煥 金
孔明 赤津
優 中野
智彦 川上
和男 米原
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NATIONAL INSTITUTES FOR QUANTUM AND RADIOLOGICALSCIENCE AND TECHNOLOGY
Kaken Co Ltd
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NATIONAL INSTITUTES FOR QUANTUM AND RADIOLOGICALSCIENCE AND TECHNOLOGY
Kaken Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F1/00—Methods of preparing compounds of the metals beryllium, magnesium, aluminium, calcium, strontium, barium, radium, thorium, or the rare earths, in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F3/00—Compounds of beryllium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F3/00—Compounds of beryllium
    • C01F3/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/382—Phosphine chalcogenides, e.g. compounds of the formula R3P=X with X = O, S, Se or Te
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
    • C22B3/3846—Phosphoric acid, e.g. (O)P(OH)3
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B35/00—Obtaining beryllium
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/02—Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2021542982A 2019-08-30 2020-08-27 ベリリウム溶液の製造方法、ベリリウムの製造方法、水酸化ベリリウムの製造方法、酸化ベリリウムの製造方法、及び、ベリリウム酸化物の製造方法 Active JP7610207B2 (ja)

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JP2019158616 2019-08-30
JP2019158616 2019-08-30
PCT/JP2020/032263 WO2021039875A1 (ja) 2019-08-30 2020-08-27 ベリリウム溶液の製造方法、ベリリウムの製造方法、水酸化ベリリウムの製造方法、酸化ベリリウムの製造方法、及び、ベリリウム酸化物

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CN112813288B (zh) * 2020-12-29 2022-08-12 东方电气集团科学技术研究院有限公司 一种以工业铍制备高纯铍的方法
CN113981491B (zh) * 2021-12-20 2023-04-25 郑州大学 一种低温熔盐电解制备金属铍的方法
CN115896492A (zh) * 2022-11-04 2023-04-04 核工业北京化工冶金研究院 一种铀铍浸出液中铀铍分离提取方法

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US20140314640A1 (en) 2012-04-18 2014-10-23 Habibulla Kusainovich OSPANOV Method for extraction of beryllium from the minerals of genthelvite group when processing the raw minerals (ores, concentrates)
CN105734309A (zh) 2016-03-17 2016-07-06 湘潭大学 一种从金绿宝石型铍矿石中提取铍的方法
CN105734282A (zh) 2016-03-15 2016-07-06 香花岭锡业有限责任公司 金绿宝石型铍矿石中铍的浸出方法
CN105907962A (zh) 2016-04-26 2016-08-31 新疆有色金属研究所 高纯含铍反萃液及其制备方法、氟铍酸铵、氟化铍和金属铍的制备方法
CN106521192A (zh) 2016-10-10 2017-03-22 南华大学 采用微波预处理从低品位羟硅铍石中浸出铍的方法

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US1511829A (en) 1921-10-01 1924-10-14 Sheldon J Dickinson Method of making metallic beryllium
US3057684A (en) * 1955-06-29 1962-10-09 Commissariat Energie Atomique Methods of obtaining sintered beryllium oxide
GB900698A (en) * 1959-08-12 1962-07-11 Atomic Energy Authority Uk Improvements in or relating to the production of beryllium metal
US3431073A (en) 1963-12-26 1969-03-04 Ngk Insulators Ltd Method of production of active beryllium oxide powders
IL31712A (en) 1968-03-06 1973-06-29 Anaconda Co Extraction of beryllium from ores
US3669649A (en) * 1970-01-30 1972-06-13 Dow Chemical Co Process for recovery of beryllium
US5091160A (en) 1990-11-05 1992-02-25 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Energy Use of microwave radiation to eliminate foam in ore leaching
JP2003073751A (ja) 2001-08-27 2003-03-12 Taiheiyo Cement Corp マイクロウェーブ酸分解法および超臨界流体抽出を用いた金属の高度濃縮方法
EA018643B1 (ru) 2004-02-23 2013-09-30 Цайтэн Чжан Раствор металлсодержащего хелатного полимера и его применение (варианты)
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CN105734309A (zh) 2016-03-17 2016-07-06 湘潭大学 一种从金绿宝石型铍矿石中提取铍的方法
CN105907962A (zh) 2016-04-26 2016-08-31 新疆有色金属研究所 高纯含铍反萃液及其制备方法、氟铍酸铵、氟化铍和金属铍的制备方法
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US12467115B2 (en) 2025-11-11
US20220298021A1 (en) 2022-09-22
WO2021039875A1 (ja) 2021-03-04
BR112022003267A2 (pt) 2022-05-17
JPWO2021039875A1 (https=) 2021-03-04
AU2020336502A1 (en) 2022-03-24

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