AU2020336502B2 - Method for producing beryllium solution, method for producing beryllium, method for producing beryllium hydroxide, method for producing beryllium oxide, and beryllium oxide - Google Patents

Method for producing beryllium solution, method for producing beryllium, method for producing beryllium hydroxide, method for producing beryllium oxide, and beryllium oxide

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Publication number
AU2020336502B2
AU2020336502B2 AU2020336502A AU2020336502A AU2020336502B2 AU 2020336502 B2 AU2020336502 B2 AU 2020336502B2 AU 2020336502 A AU2020336502 A AU 2020336502A AU 2020336502 A AU2020336502 A AU 2020336502A AU 2020336502 B2 AU2020336502 B2 AU 2020336502B2
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AU
Australia
Prior art keywords
beryllium
solution
heating step
producing
heating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
AU2020336502A
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English (en)
Other versions
AU2020336502A1 (en
Inventor
Yoshiaki AKATSU
Tomohiko Kawakami
Jaehwan Kim
Masaru Nakamichi
Suguru NAKANO
Kazuo Yonehara
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kaken Inc
National Institutes For Quantum Science and Technology
Original Assignee
KAKEN Inc
National Institutes For Quantum Science and Technology
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Publication of AU2020336502A1 publication Critical patent/AU2020336502A1/en
Application granted granted Critical
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F1/00—Methods of preparing compounds of the metals beryllium, magnesium, aluminium, calcium, strontium, barium, radium, thorium, or the rare earths, in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F3/00—Compounds of beryllium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F3/00—Compounds of beryllium
    • C01F3/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/382—Phosphine chalcogenides, e.g. compounds of the formula R3P=X with X = O, S, Se or Te
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
    • C22B3/3846—Phosphoric acid, e.g. (O)P(OH)3
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B35/00—Obtaining beryllium
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/02—Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
AU2020336502A 2019-08-30 2020-08-27 Method for producing beryllium solution, method for producing beryllium, method for producing beryllium hydroxide, method for producing beryllium oxide, and beryllium oxide Active AU2020336502B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2019158616 2019-08-30
JP2019-158616 2019-08-30
PCT/JP2020/032263 WO2021039875A1 (ja) 2019-08-30 2020-08-27 ベリリウム溶液の製造方法、ベリリウムの製造方法、水酸化ベリリウムの製造方法、酸化ベリリウムの製造方法、及び、ベリリウム酸化物

Publications (2)

Publication Number Publication Date
AU2020336502A1 AU2020336502A1 (en) 2022-03-24
AU2020336502B2 true AU2020336502B2 (en) 2026-02-05

Family

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AU2020336502A Active AU2020336502B2 (en) 2019-08-30 2020-08-27 Method for producing beryllium solution, method for producing beryllium, method for producing beryllium hydroxide, method for producing beryllium oxide, and beryllium oxide

Country Status (5)

Country Link
US (1) US12467115B2 (https=)
JP (1) JP7610207B2 (https=)
AU (1) AU2020336502B2 (https=)
BR (1) BR112022003267A2 (https=)
WO (1) WO2021039875A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112813288B (zh) * 2020-12-29 2022-08-12 东方电气集团科学技术研究院有限公司 一种以工业铍制备高纯铍的方法
CN113981491B (zh) * 2021-12-20 2023-04-25 郑州大学 一种低温熔盐电解制备金属铍的方法
CN115896492A (zh) * 2022-11-04 2023-04-04 核工业北京化工冶金研究院 一种铀铍浸出液中铀铍分离提取方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB900698A (en) * 1959-08-12 1962-07-11 Atomic Energy Authority Uk Improvements in or relating to the production of beryllium metal
US3057684A (en) * 1955-06-29 1962-10-09 Commissariat Energie Atomique Methods of obtaining sintered beryllium oxide
US3669649A (en) * 1970-01-30 1972-06-13 Dow Chemical Co Process for recovery of beryllium
US20140314640A1 (en) * 2012-04-18 2014-10-23 Habibulla Kusainovich OSPANOV Method for extraction of beryllium from the minerals of genthelvite group when processing the raw minerals (ores, concentrates)
CN105734282A (zh) * 2016-03-15 2016-07-06 香花岭锡业有限责任公司 金绿宝石型铍矿石中铍的浸出方法

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US2899276A (en) 1959-08-11 Process for preparing dense
US1511829A (en) 1921-10-01 1924-10-14 Sheldon J Dickinson Method of making metallic beryllium
US3431073A (en) 1963-12-26 1969-03-04 Ngk Insulators Ltd Method of production of active beryllium oxide powders
IL31712A (en) 1968-03-06 1973-06-29 Anaconda Co Extraction of beryllium from ores
US5091160A (en) 1990-11-05 1992-02-25 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Energy Use of microwave radiation to eliminate foam in ore leaching
JP2003073751A (ja) 2001-08-27 2003-03-12 Taiheiyo Cement Corp マイクロウェーブ酸分解法および超臨界流体抽出を用いた金属の高度濃縮方法
EA018643B1 (ru) 2004-02-23 2013-09-30 Цайтэн Чжан Раствор металлсодержащего хелатного полимера и его применение (варианты)
US8945931B2 (en) 2004-06-18 2015-02-03 Berylliant, Inc. Method and kits to detect beryllium by fluorescence
US8936770B2 (en) 2010-01-22 2015-01-20 Molycorp Minerals, Llc Hydrometallurgical process and method for recovering metals
JP2012088102A (ja) 2010-10-18 2012-05-10 Japan Atomic Energy Agency 使用済の金属ベリリウムからベリリウム資源を回収するための方法
CN103663506A (zh) 2013-12-06 2014-03-26 富蕴恒盛铍业有限责任公司 精制氢氧化铍的制备方法以及利用该精制氢氧化铍制备核纯级金属铍珠的方法
CN105734309B (zh) * 2016-03-17 2017-09-05 湘潭大学 一种从金绿宝石型铍矿石中提取铍的方法
CN105907962B (zh) * 2016-04-26 2018-09-07 新疆有色金属研究所 高纯含铍反萃液及其制备方法、氟铍酸铵、氟化铍和金属铍的制备方法
CN106521192B (zh) * 2016-10-10 2019-03-29 南华大学 采用微波预处理从低品位羟硅铍石中浸出铍的方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3057684A (en) * 1955-06-29 1962-10-09 Commissariat Energie Atomique Methods of obtaining sintered beryllium oxide
GB900698A (en) * 1959-08-12 1962-07-11 Atomic Energy Authority Uk Improvements in or relating to the production of beryllium metal
US3669649A (en) * 1970-01-30 1972-06-13 Dow Chemical Co Process for recovery of beryllium
US20140314640A1 (en) * 2012-04-18 2014-10-23 Habibulla Kusainovich OSPANOV Method for extraction of beryllium from the minerals of genthelvite group when processing the raw minerals (ores, concentrates)
CN105734282A (zh) * 2016-03-15 2016-07-06 香花岭锡业有限责任公司 金绿宝石型铍矿石中铍的浸出方法

Non-Patent Citations (1)

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Title
Zaki, et al. "Extraction equilibrium of beryllium and aluminum and recovery of beryllium from Egyptian beryl solution using CYANEX 921" Hydrometallurgy 80.4 (2005): 221-231 (Year: 2005) *

Also Published As

Publication number Publication date
US12467115B2 (en) 2025-11-11
US20220298021A1 (en) 2022-09-22
WO2021039875A1 (ja) 2021-03-04
BR112022003267A2 (pt) 2022-05-17
JPWO2021039875A1 (https=) 2021-03-04
AU2020336502A1 (en) 2022-03-24
JP7610207B2 (ja) 2025-01-08

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