JP7498716B2 - ポリ(ファルネセン)を含むバイオベースの増粘組成物 - Google Patents
ポリ(ファルネセン)を含むバイオベースの増粘組成物 Download PDFInfo
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- JP7498716B2 JP7498716B2 JP2021538223A JP2021538223A JP7498716B2 JP 7498716 B2 JP7498716 B2 JP 7498716B2 JP 2021538223 A JP2021538223 A JP 2021538223A JP 2021538223 A JP2021538223 A JP 2021538223A JP 7498716 B2 JP7498716 B2 JP 7498716B2
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/062—Oil-in-water emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Cosmetics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Description
これらの目的は、新規な増粘組成物により達成される。
-生物起源由来の少なくとも1種の油と、
-10,000g/mol~120,000g/molの範囲の数平均モル質量を有する少なくとも1種のポリ(ファルネセン)ポリマーと、を含む増粘組成物に関する。
-炭化水素油の総重量に対して、95重量%~100重量%および優先的には98重量%~100重量%の範囲の含有量のイソパラフィン、および/または
-95%以上、好ましくは98%以上、優先的には100%の含有量の生物起源の炭素、および/または
-炭化水素油の総重量に対して、10以下、好ましくは5重量%以下、優先的には2重量%以下の含有量のノルマルパラフィン;および/または
-炭化水素油の総重量に対して、1重量%以下、好ましくは0.5重量%以下、優先的には100重量ppm以下の含有量のナフテン系化合物;および/または
-炭化水素油の総重量に対して、500重量ppm以下、好ましくは300重量ppm以下、優先的には100重量ppm以下、より優先的には50重量ppm以下、有利には20重量ppm以下の含有量の芳香族化合物、を含む。
-10重量%~90重量%、好ましくは20重量%~80重量%、より好ましくは30重量%~70重量%、さらにより好ましくは40重量%~60重量%の生物起源源由来の油(複数可)と、
-10重量%~90重量%、好ましくは20重量%~80重量%、より好ましくは30重量%~70重量%、さらにより好ましくは40重量%~60重量%のポリ(ファルネセン)ポリマー(複数可)と、を含む。
本発明は、皮膚、爪または皮膚付属器(唇、毛髪および頭皮を含む)への局所塗布を意図した増粘組成物に関し、
当該増粘組成物は、該増粘組成物の総重量に対して、
-10重量%~90重量%の生物起源由来の少なくとも1種の油と、
-10重量%~90重量%の、10,000g/mol~120,000g/mol、好ましくは10,000g/mol~95000g/molの範囲の数平均モル質量を有する少なくとも1種のポリ(ファルネセン)ポリマーと、を含む。
-生物起源由来の炭化水素油;
-酸、エステルまたはアミド形態、好ましくは酸またはエステル形態のC6~C24脂肪酸の中から選択される植物油または動物油;
-およびそれらの混合物。
-炭化水素油の総重量に対して、15個の炭素原子を有するイソパラフィンおよび16個の炭素原子を有するイソパラフィンを合計で80重量%~98重量%の範囲の量で、または
-炭化水素油の総重量に対して、16個の炭素原子を有するイソパラフィン、17個の炭素原子を有するイソパラフィン、および18個の炭素原子を有するイソパラフィンを合計で80重量%~98重量%の範囲の量で、または
-炭化水素油の総重量に対して、17個の炭素原子を有するイソパラフィン、および18個の炭素原子を有するイソパラフィンを合計で80重量%~98重量%の範囲の量で含む。
-標準ASTM D86に従って230℃~340℃、好ましくは235℃~330℃、より優先的には240℃~325℃の範囲の沸点、および/または
-標準OECD306に従って測定される、少なくとも60%、好ましくは少なくとも70%、優先的には少なくとも75%、更に優先的には少なくとも80%の28日目の生分解性、および/または
-標準EN ISO2719に従って110℃以上の引火点、を有する。
-圧力:50bar~160bar、好ましくは80bar~150bar、より好ましくは90bar~120bar;
-温度:80℃~180℃、好ましくは120℃~160℃、より好ましくは150℃~160℃;
液体時空間速度(LHSV):0.2hr-1~5hr-1、好ましくは0.4hr-1~3hr-1、より好ましくは0.5hr-1~0.8hr-1;
-水素化処理(水素処理)速度:上記の条件に適合し、処理対象の供給原料の最大200Nm3/トンに及ぶことができる。
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の生物起源由来の油(複数可)と、
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の、10,000g/mol~120,000g/molの範囲の数平均モル質量を有するポリ(ファルネセン)ポリマー(複数可)と、
を含む。
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の上に定義される炭化水素油(複数可)と、
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の、10,000g/mol~120,000g/molの範囲の数平均モル質量を有するポリ(ファルネセン)ポリマーと、
を含む。
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の生物起源由来の油と、
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の、40,000g/mol~90,000g/molの範囲の数平均モル質量を有するポリ(ファルネセン)ポリマーと、
を含む。
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の上に先に定義される炭化水素油(複数可)と、
-10重量%~90重量%、好ましくは20重量%~80重量%、優先的には30重量%~70重量%、より優先的には40重量%~60重量%の、40,000g/mol~90,000g/molの範囲の数平均モル質量を有するポリ(ファルネセン)ポリマーと、
を含む。
-適切な場合には、増粘組成物のものとは異なる植物油、植物バター、エーテルおよび脂肪アルコール、油性エステル、アルカンおよびシリコーン油、好ましくは油性エステルから選択される少なくとも1種の脂肪物質、
および/または
-上述の添加剤の中から、好ましくはアニオン性発泡界面活性剤(ラウリルエーテル硫酸ナトリウム、アルキルリン酸ナトリウム、トリデシルエーテル硫酸ナトリウム等)、両性界面活性剤(例えば、アルキルベタイン、ココアンホ二酢酸二ナトリウム)またはHLBが10超の非イオン性界面活性剤(例えば、POE/PPG/POE、アルキルポリグルコシド、ポリグリセリル-3ヒドロキシラウリルエーテル)から選択される少なくとも1種の添加剤と、を含む化粧品組成物に関する。
-引火点:EN ISO2719
-15℃での密度:EN ISO1185
-40℃での粘度:EN ISO3104
-アニリン点:EN ISO2977
-沸点:ASTM D86
-生分解性:OECD306法
-20℃における屈折率:ASTM D1218
-蒸気圧:当業者に周知の方法に従って計算される。
-植物油:20℃で0.91の密度を有し、
植物油の総重量に対して
〇58.0重量%~64.0重量%のガドレイン酸(C20:1)
〇10.0重量%~14.0重量%のエルカ酸(C22:1 d13)
〇3.0重量%~6.0重量%のドコセン酸(C22:1 d 5)
〇15.0重量%~21.0重量%のドコサジエン酸(C22:2)を含むメドウフォーム油。
-植物ワックス:ホホバ油。
-油性エステル:イソノニルイソノナノエート(INCI名による)、市販品。
-シリコーンオイル:シクロペンタシロキサン(INCI名による)、市販品。
-スクアラン(INCI名による)。
-10%:5gの試験対象の脂肪物質添加。
-25%:先に得られた混合物において10gの試験対象の脂肪物質添加
((5+10)/(45+5+10)=0.25)。
-50%:先に得られた混合物において30gの試験対象の脂肪物質添加。
-75%:先に得られた混合物において90gの試験対象の脂肪物質添加。
-90%:先に得られた混合物において270gの試験対象の脂肪物質添加。
-ガラスピペットを使用することによる、評価対象の製品の液滴の皮膚(前腕の下側)への堆積。
-指を使用することによる製品の塗布:皮膚上の外観(光沢)、塗布時の触感(感覚)、および塗布後の最終的な感触の評価。
-成分を秤量し、均質相が得られるまで成分を撹拌および75℃での加熱下に置くことによる相Aの調製。
-相Bの調製:
〇相Bの水を秤量する。
〇撹拌せずに、Carbopol Ultrez21に振りかけ、撹拌せずに10分間水和させたままにする。
〇撹拌下に置き、75℃で加熱する。加熱中、激しく撹拌しながら、Rhodicare-tのプレミックスをグリセリンに注ぐ。
〇75℃で加熱し続けながら、均質相が得られるまで撹拌下で維持する。
-75℃で、激しく撹拌しながら、相Aを相Bに注ぐことによってエマルジョンを調製する。
-撹拌速度を維持しながら冷却を開始する。72℃で、9500rpmに設定したturrax(登録商標)分散機を用いて30秒間均質化し、中程度の撹拌下で冷却を継続する。
-50℃で、撹拌しながら、相Cの成分を連続的に導入し、中程度の撹拌下で冷却を継続する。
-30℃にて、撹拌しながら、相Dの構成成分を連続的に導入する。
-pHを測定し、必要に応じて調整する:5.00<pH<6.00。
-ガラスピペットを使用することによる、評価対象の製品の液滴の皮膚(前腕の下側)への堆積、および液滴の広がりの分析。
-指を使用することによる製品の塗布:皮膚上の広がりおよび外観(光沢)の評価。
試験した増粘組成物を以下の表8に示す。パーセンテージは、増粘組成物の総重量に対する重量パーセントである。
-4 にじみがない場合、
-3 ごくわずかなにじみがある場合、
-2 わずかににじんでいる場合、
-1 中程度のにじみがある場合、
-0 著しくにじんでいる場合。
-前腕の16cm2を測定する2つの領域(処理対象領域および対照領域)の範囲を定める;
-15%濃度の合成皮脂のアルコール希釈物50μLの所定の領域への塗布;
-処理対象領域にわたる2mg/cm2の投与量での組成物実施例9.3の塗布;
-所定の領域上への50μLの1.2%炭素粒子の水-アルコール懸濁液の堆積;
-ビデオダーモスコープC-Cubeを用いた画像(T0)の取得;
-湿らせた綿棒またはディスクを使用し、次いで風乾させることによる2つの領域の標準化された拭き取り;
-ビデオダーモスコープC-Cubeを用いた画像(T1)の取得。
Claims (21)
- 皮膚、唇または皮膚付属器への局所塗布を意図した増粘組成物であって、
-生物起源由来の少なくとも1種の油と、
-10,000~120,000g/molの範囲の数平均モル質量を有する少なくとも1種のポリ(ファルネセン)ポリマーと、を含み、前記ポリ(ファルネセン)ポリマーが部分的または完全に水素化されている、および/またはヒドロキシル基で官能化されている、増粘組成物。 - 前記生物起源由来の油が、炭化水素油、酸、エステルまたはアミドの形態の植物油または動物油、およびそれらの混合物の中から選択される、請求項1に記載の増粘組成物。
- 前記生物起源由来の油が炭化水素油である、請求項1または2に記載の増粘組成物。
- 前記炭化水素油が、炭化水素油の総重量に対して、90重量%~100重量%の範囲の含有量のイソパラフィン、0重量%~10重量%の範囲の含有量のノルマルパラフィンを含む、請求項3に記載の増粘組成物。
- 前記炭化水素油が、14個~18個の炭素原子を含む非環状イソパラフィンの中から選択される、請求項3または4に記載の増粘組成物。
- 前記炭化水素油が、以下:
-前記炭化水素油の総重量に対して、95重量%~100重量%若しくは98重量%~100重量%の範囲の含有量のイソパラフィン;および/または
-90%以上、若しくは95%以上、若しくは98%以上、若しくは100%の含有量の生物起源由来の炭素、および/または
-前記炭化水素油の総重量に対して、10重量%以下、若しくは5重量%以下、若しくは2重量%以下の含有量のノルマルパラフィン;および/または
-前記炭化水素油の総重量に対して、1重量%以下、若しくは0.5重量%以下、若しくは100重量ppm以下の含有量のナフテン系化合物;および/または
-前記炭化水素油の総重量に対して、500重量ppm以下、若しくは300重量ppm以下、若しくは100重量ppm以下、若しくは50重量ppm以下、若しくは20重量ppm以下の含有量の芳香族化合物、
を含む、請求項3~5のいずれか一項に記載の増粘組成物。 - 前記炭化水素油が、温度80℃~180℃、および気圧50bar~160barにおいて、脱酸素化および/または異性化された生物起源の供給原料の接触水素化の方法によって得られる、請求項3~6のいずれか一項に記載の増粘組成物。
- 前記ポリ(ファルネセン)ポリマーが、20,000~90,000g/mol、または30,000~85,000g/mol、または40,000~80,000g/mol、または50,000~80,000g/molの範囲の数平均モル質量を有する、請求項1~7のいずれか一項に記載の増粘組成物。
- 前記増粘組成物の総重量に対して、
-10重量%~90重量%、または20重量%~80重量%、または30重量%~70重量%、または40重量%~60重量%の生物起源由来の油(複数可)と、
-10重量%~90重量%、または20重量%~80重量%、または30重量%~70重量%、または40重量%~60重量%のポリ(ファルネセン)ポリマー(複数可)と、を含む、請求項1~8のいずれか一項に記載の増粘組成物。 - 化粧品組成物における、増粘剤、感覚剤、膜形成剤、テクスチャ剤、耐水性向上剤、保湿/水和剤、コンディショナー、または粘性油としての、請求項1~9のいずれか一項に記載の増粘組成物の使用。
- 前記化粧品組成物がさらに、少なくとも1種の脂肪物質を含む、請求項10に記載の使用。
- 請求項1~9のいずれか一項に記載の少なくとも1つの増粘組成物を含む、皮膚、唇または皮膚付属器に局所化粧品を塗布するための化粧品組成物。
- 前記増粘組成物が、前記化粧品組成物の総重量に対して、1重量%~80重量%、または5重量%~70重量%、または10重量%~50重量%の範囲の量で存在する、請求項12に記載の化粧品組成物。
- 前記増粘組成物の植物油以外の植物油;前記増粘組成物の炭化水素油以外の炭化水素油;植物バター;脂肪エーテルおよび脂肪アルコール;油性エステル;アルカンおよびシリコーン油の中から選択される少なくとも1種の脂肪物質;および/または少なくとも1種の添加剤を含む、請求項12または13に記載の化粧品組成物。
- 前記添加剤が乳化剤から選択される、請求項14に記載の化粧品組成物。
- 局所塗布のための、請求項1~9のいずれかに記載の増粘組成物の使用、または請求項12~15のいずれか一項に記載の化粧品組成物の使用。
- 皮膚若しくは毛髪用のケア製品として、メイクアップ製品として、毛髪製品として、メイクアップリムーバ製品として、付香された製品として、日焼け止め製品として、またはリップケア製品として局所塗布するための、請求項16に記載の使用。
- 請求項1~9のいずれか一項に記載の増粘組成物または請求項12~15のいずれか一項に記載の化粧品組成物を、皮膚、唇または皮膚付属器に塗布する少なくとも1つの工程を含む、皮膚、唇または皮膚付属器の美容処置のための美容処置方法。
- 局所塗布のための日焼け止め組成物であって、前記日焼け止め組成物が、(i)少なくとも1種の日焼け止めフィルタと、(ii)請求項1~9のいずれか一項に記載の少なくとも1種の増粘組成物と、を含む、日焼け止め組成物。
- 前記増粘組成物が、前記日焼け止め組成物の総重量に対して、1重量%~80重量%、または5重量%~70重量%、または10重量%~50重量%の範囲の量で存在する、請求項19に記載の日焼け止め組成物。
- 日焼け止め製品として使用するための、請求項1~9のいずれか一項に記載の増粘組成物または請求項20に記載の日焼け止め組成物。
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FR1900252A FR3091653B1 (fr) | 2019-01-10 | 2019-01-10 | Composition epaississante biosourcee |
FR1900252 | 2019-01-10 | ||
PCT/FR2020/050031 WO2020144440A1 (fr) | 2019-01-10 | 2020-01-10 | Composition epaississante biosourcee comprenant un poly(farnésène) |
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WO2023194289A1 (en) * | 2022-04-04 | 2023-10-12 | Dsm Ip Assets B.V. | Improve the water resistance of cosmetic compositions comprising pigments |
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JP2012502136A (ja) | 2008-09-04 | 2012-01-26 | アムイリス ビオテクフノロジエス,インコーポレイテッド | ファルネセン共重合体 |
US20130251846A1 (en) | 2010-12-02 | 2013-09-26 | Wm. Wrigley Jr. Company | Chewing gum base containing polyfarnesene and chewing gum products made there from |
JP2013241609A (ja) | 2012-02-24 | 2013-12-05 | Kuraray Co Ltd | ゴム組成物及びタイヤ |
WO2018029143A1 (fr) | 2016-08-08 | 2018-02-15 | Avril | Procédé d'obtention de matériaux, matériaux en tant que tels et leurs utilisations |
JP2019532142A (ja) | 2016-09-15 | 2019-11-07 | フィナ テクノロジー,インコーポレイティド | ファルネセン系マクロモノマー並びにその製造及び使用方法 |
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FR3091653B1 (fr) | 2023-01-13 |
CN113226266B (zh) | 2023-08-08 |
WO2020144440A1 (fr) | 2020-07-16 |
JP2022517180A (ja) | 2022-03-07 |
EP3908248A1 (fr) | 2021-11-17 |
FR3091653A1 (fr) | 2020-07-17 |
CN113226266A (zh) | 2021-08-06 |
US20220110840A1 (en) | 2022-04-14 |
EP3908248B1 (fr) | 2023-03-01 |
KR20210113981A (ko) | 2021-09-17 |
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