JP7456743B2 - 剥離剤組成物 - Google Patents
剥離剤組成物 Download PDFInfo
- Publication number
- JP7456743B2 JP7456743B2 JP2019178887A JP2019178887A JP7456743B2 JP 7456743 B2 JP7456743 B2 JP 7456743B2 JP 2019178887 A JP2019178887 A JP 2019178887A JP 2019178887 A JP2019178887 A JP 2019178887A JP 7456743 B2 JP7456743 B2 JP 7456743B2
- Authority
- JP
- Japan
- Prior art keywords
- methyl
- ethyl
- butyl
- ethylhexyl
- linoleate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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- 239000000203 mixture Substances 0.000 title claims description 25
- -1 propyl elaidate Chemical compound 0.000 claims description 67
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 51
- 239000000194 fatty acid Substances 0.000 claims description 51
- 229930195729 fatty acid Natural products 0.000 claims description 51
- 150000004665 fatty acids Chemical class 0.000 claims description 51
- 239000002253 acid Substances 0.000 claims description 29
- 239000003795 chemical substances by application Substances 0.000 claims description 19
- 150000002148 esters Chemical class 0.000 claims description 18
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 17
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 15
- 229940040452 linolenate Drugs 0.000 claims description 10
- 239000001149 (9Z,12Z)-octadeca-9,12-dienoate Substances 0.000 claims description 8
- QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 claims description 8
- 229940049918 linoleate Drugs 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 229940066675 ricinoleate Drugs 0.000 claims description 6
- WTTJVINHCBCLGX-UHFFFAOYSA-N (9trans,12cis)-methyl linoleate Natural products CCCCCC=CCC=CCCCCCCCC(=O)OC WTTJVINHCBCLGX-UHFFFAOYSA-N 0.000 claims description 5
- LNJCGNRKWOHFFV-UHFFFAOYSA-N 3-(2-hydroxyethylsulfanyl)propanenitrile Chemical compound OCCSCCC#N LNJCGNRKWOHFFV-UHFFFAOYSA-N 0.000 claims description 5
- PKIXXJPMNDDDOS-UHFFFAOYSA-N Methyl linoleate Natural products CCCCC=CCCC=CCCCCCCCC(=O)OC PKIXXJPMNDDDOS-UHFFFAOYSA-N 0.000 claims description 5
- QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 claims description 5
- 229940073769 methyl oleate Drugs 0.000 claims description 5
- LVGKNOAMLMIIKO-UHFFFAOYSA-N Elaidinsaeure-aethylester Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC LVGKNOAMLMIIKO-UHFFFAOYSA-N 0.000 claims description 4
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 4
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 4
- DVWSXZIHSUZZKJ-UHFFFAOYSA-N 18:3n-3 Natural products CCC=CCC=CCC=CCCCCCCCC(=O)OC DVWSXZIHSUZZKJ-UHFFFAOYSA-N 0.000 claims description 3
- XUQBFMJGHHYFCP-UHFFFAOYSA-N 2-(2-chloroethyl)-3,4,5,6-tetrahydro-1h-2-benzazocine;hydrochloride Chemical compound Cl.C1N(CCCl)CCCCC2=CC=CC=C21 XUQBFMJGHHYFCP-UHFFFAOYSA-N 0.000 claims description 3
- FDVCQFAKOKLXGE-UHFFFAOYSA-N 216978-79-9 Chemical compound C1CC(C)(C)C2=CC(C=O)=CC3=C2N1CCC3(C)C FDVCQFAKOKLXGE-UHFFFAOYSA-N 0.000 claims description 3
- HHVGFXQQBNQVIO-UHFFFAOYSA-N C(CCC)OC(C=CC=CC=CC=CC=CC=CCCCCCCCCC)=O Chemical compound C(CCC)OC(C=CC=CC=CC=CC=CC=CCCCCCCCCC)=O HHVGFXQQBNQVIO-UHFFFAOYSA-N 0.000 claims description 3
- 229920000064 Ethyl eicosapentaenoic acid Polymers 0.000 claims description 3
- QYDYPVFESGNLHU-ZHACJKMWSA-N Methyl (9E)-9-octadecenoate Chemical compound CCCCCCCC\C=C\CCCCCCCC(=O)OC QYDYPVFESGNLHU-ZHACJKMWSA-N 0.000 claims description 3
- QWDCYFDDFPWISL-UHFFFAOYSA-N UNPD207407 Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(=O)OC QWDCYFDDFPWISL-UHFFFAOYSA-N 0.000 claims description 3
- SNXPWYFWAZVIAU-UHFFFAOYSA-N arachidonic acid ethyl ester Natural products CCCCCC=CCC=CCC=CCC=CCCCC(=O)OCC SNXPWYFWAZVIAU-UHFFFAOYSA-N 0.000 claims description 3
- OFIDNKMQBYGNIW-UHFFFAOYSA-N arachidonic acid methyl ester Natural products CCCCCC=CCC=CCC=CCC=CCCCC(=O)OC OFIDNKMQBYGNIW-UHFFFAOYSA-N 0.000 claims description 3
- SVGGKWILBMPIJV-UTJQPWESSA-N butyl (9z,12z)-octadeca-9,12-dienoate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCCCC SVGGKWILBMPIJV-UTJQPWESSA-N 0.000 claims description 3
- WIBFFTLQMKKBLZ-OUKQBFOZSA-N butyl (e)-octadec-9-enoate Chemical compound CCCCCCCC\C=C\CCCCCCCC(=O)OCCCC WIBFFTLQMKKBLZ-OUKQBFOZSA-N 0.000 claims description 3
- AMUBFTQQLDHNQU-SEYXRHQNSA-N butyl (z)-docos-13-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(=O)OCCCC AMUBFTQQLDHNQU-SEYXRHQNSA-N 0.000 claims description 3
- HGWAKQDTQVDVRP-OKULMJQMSA-N butyl (z,12r)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(=O)OCCCC HGWAKQDTQVDVRP-OKULMJQMSA-N 0.000 claims description 3
- QWDCYFDDFPWISL-JEBPEJKESA-N cis-5,8,11,14,17-eicosapentaenoic acid methyl ester Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(=O)OC QWDCYFDDFPWISL-JEBPEJKESA-N 0.000 claims description 3
- VCDLWFYODNTQOT-UHFFFAOYSA-N docosahexaenoic acid methyl ester Natural products CCC=CCC=CCC=CCC=CCC=CCC=CCCC(=O)OC VCDLWFYODNTQOT-UHFFFAOYSA-N 0.000 claims description 3
- 229940066279 eicosapentaenoate Drugs 0.000 claims description 3
- WFZQLUSOXHIVKL-QXMHVHEDSA-N ethyl (13Z)-docosenoate Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(=O)OCC WFZQLUSOXHIVKL-QXMHVHEDSA-N 0.000 claims description 3
- ITNKVODZACVXDS-YATCGRJWSA-N ethyl (4e,7e,10e,13e,16e,19e)-docosa-4,7,10,13,16,19-hexaenoate Chemical compound CCOC(=O)CC\C=C\C\C=C\C\C=C\C\C=C\C\C=C\C\C=C\CC ITNKVODZACVXDS-YATCGRJWSA-N 0.000 claims description 3
- SSQPWTVBQMWLSZ-AAQCHOMXSA-N ethyl (5Z,8Z,11Z,14Z,17Z)-icosapentaenoate Chemical compound CCOC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CC SSQPWTVBQMWLSZ-AAQCHOMXSA-N 0.000 claims description 3
- AZXVZUBIFYQWJK-KWRJMZDGSA-N ethyl (z,12r)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(=O)OCC AZXVZUBIFYQWJK-KWRJMZDGSA-N 0.000 claims description 3
- SNXPWYFWAZVIAU-GKFVBPDJSA-N ethyl arachidonate Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(=O)OCC SNXPWYFWAZVIAU-GKFVBPDJSA-N 0.000 claims description 3
- 229940031016 ethyl linoleate Drugs 0.000 claims description 3
- FMMOOAYVCKXGMF-MURFETPASA-N ethyl linoleate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCC FMMOOAYVCKXGMF-MURFETPASA-N 0.000 claims description 3
- LVGKNOAMLMIIKO-QXMHVHEDSA-N ethyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC LVGKNOAMLMIIKO-QXMHVHEDSA-N 0.000 claims description 3
- 229940093471 ethyl oleate Drugs 0.000 claims description 3
- JELGPLUONQGOHF-KTKRTIGZSA-N ethyl palmitoleate Chemical compound CCCCCC\C=C/CCCCCCCC(=O)OCC JELGPLUONQGOHF-KTKRTIGZSA-N 0.000 claims description 3
- ZYNDJIBBPLNPOW-UHFFFAOYSA-N eurucic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCCCCCC(=O)OC ZYNDJIBBPLNPOW-UHFFFAOYSA-N 0.000 claims description 3
- XSCIEKYDPGHXMD-YPKPFQOOSA-N heptyl (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCCCCCCC XSCIEKYDPGHXMD-YPKPFQOOSA-N 0.000 claims description 3
- 229960002600 icosapent ethyl Drugs 0.000 claims description 3
- FMMOOAYVCKXGMF-UHFFFAOYSA-N linoleic acid ethyl ester Natural products CCCCCC=CCC=CCCCCCCCC(=O)OCC FMMOOAYVCKXGMF-UHFFFAOYSA-N 0.000 claims description 3
- AJAMRCUNWLZBDF-UHFFFAOYSA-N linoleic acid propyl ester Natural products CCCCCC=CCC=CCCCCCCCC(=O)OCCC AJAMRCUNWLZBDF-UHFFFAOYSA-N 0.000 claims description 3
- OFIDNKMQBYGNIW-ZKWNWVNESA-N methyl arachidonate Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(=O)OC OFIDNKMQBYGNIW-ZKWNWVNESA-N 0.000 claims description 3
- ZYNDJIBBPLNPOW-KHPPLWFESA-N methyl erucate Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(=O)OC ZYNDJIBBPLNPOW-KHPPLWFESA-N 0.000 claims description 3
- DVWSXZIHSUZZKJ-YSTUJMKBSA-N methyl linolenate Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(=O)OC DVWSXZIHSUZZKJ-YSTUJMKBSA-N 0.000 claims description 3
- IZFGRAGOVZCUFB-HJWRWDBZSA-N methyl palmitoleate Chemical group CCCCCC\C=C/CCCCCCCC(=O)OC IZFGRAGOVZCUFB-HJWRWDBZSA-N 0.000 claims description 3
- WIBFFTLQMKKBLZ-SEYXRHQNSA-N n-butyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCCCC WIBFFTLQMKKBLZ-SEYXRHQNSA-N 0.000 claims description 3
- RWSPHQOPNBVTAO-UTJQPWESSA-N pentyl (9z,12z)-octadeca-9,12-dienoate Chemical compound CCCCCOC(=O)CCCCCCC\C=C/C\C=C/CCCCC RWSPHQOPNBVTAO-UTJQPWESSA-N 0.000 claims description 3
- YEUKJHYLBPPSQJ-SEYXRHQNSA-N pentyl (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCCCCC YEUKJHYLBPPSQJ-SEYXRHQNSA-N 0.000 claims description 3
- XEIOPEQGDSYOIH-MURFETPASA-N propan-2-yl (9z,12z)-octadeca-9,12-dienoate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OC(C)C XEIOPEQGDSYOIH-MURFETPASA-N 0.000 claims description 3
- AJAMRCUNWLZBDF-MURFETPASA-N propyl linoleate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCCC AJAMRCUNWLZBDF-MURFETPASA-N 0.000 claims description 3
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 claims description 2
- BMSHSDASEVJHHE-FORXSXPXSA-N 2-ethylhexyl (5z,8z,11z,14z)-icosa-5,8,11,14-tetraenoate Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(=O)OCC(CC)CCCC BMSHSDASEVJHHE-FORXSXPXSA-N 0.000 claims description 2
- PSAAPHZQPIWZFX-HDXUUTQWSA-N 2-ethylhexyl (9z,12z)-octadeca-9,12-dienoate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCC(CC)CCCC PSAAPHZQPIWZFX-HDXUUTQWSA-N 0.000 claims description 2
- MZOUHAVBUNKLBO-UHFFFAOYSA-N CCCCCCCCCC=CC=CC=CC=CC=CC=CC(=O)OCC(CC)CCCC Chemical compound CCCCCCCCCC=CC=CC=CC=CC=CC=CC(=O)OCC(CC)CCCC MZOUHAVBUNKLBO-UHFFFAOYSA-N 0.000 claims description 2
- VCTNVUCRSOTNFA-SNPVRQPZSA-N butyl (5z,8z,11z,14z)-icosa-5,8,11,14-tetraenoate Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(=O)OCCCC VCTNVUCRSOTNFA-SNPVRQPZSA-N 0.000 claims description 2
- QQNROWCMALTXCD-XQOKXTRKSA-N butyl (9z,12z,15z)-octadeca-9,12,15-trienoate Chemical compound CCCCOC(=O)CCCCCCC\C=C/C\C=C/C\C=C/CC QQNROWCMALTXCD-XQOKXTRKSA-N 0.000 claims description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
- 229940090028 ethyl linolenate Drugs 0.000 claims description 2
- JYYFMIOPGOFNPK-AGRJPVHOSA-N ethyl linolenate Chemical compound CCOC(=O)CCCCCCC\C=C/C\C=C/C\C=C/CC JYYFMIOPGOFNPK-AGRJPVHOSA-N 0.000 claims description 2
- JYYFMIOPGOFNPK-UHFFFAOYSA-N ethyl linolenate Natural products CCOC(=O)CCCCCCCC=CCC=CCC=CCC JYYFMIOPGOFNPK-UHFFFAOYSA-N 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 239000003973 paint Substances 0.000 description 34
- 230000000694 effects Effects 0.000 description 22
- 238000000576 coating method Methods 0.000 description 13
- 239000011248 coating agent Substances 0.000 description 12
- 239000002904 solvent Substances 0.000 description 11
- 239000002562 thickening agent Substances 0.000 description 10
- 125000004432 carbon atom Chemical group C* 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 229910052625 palygorskite Inorganic materials 0.000 description 7
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 6
- 229960004488 linolenic acid Drugs 0.000 description 6
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 6
- 239000001993 wax Substances 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
- 230000005923 long-lasting effect Effects 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 description 4
- HPEUJPJOZXNMSJ-UHFFFAOYSA-N Methyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC HPEUJPJOZXNMSJ-UHFFFAOYSA-N 0.000 description 4
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- 229920000178 Acrylic resin Polymers 0.000 description 3
- 239000004925 Acrylic resin Substances 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
- UDSFAEKRVUSQDD-UHFFFAOYSA-N Dimethyl adipate Chemical compound COC(=O)CCCCC(=O)OC UDSFAEKRVUSQDD-UHFFFAOYSA-N 0.000 description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 3
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 239000004113 Sepiolite Substances 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 125000005233 alkylalcohol group Chemical group 0.000 description 3
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 229940125904 compound 1 Drugs 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- XTDYIOOONNVFMA-UHFFFAOYSA-N dimethyl pentanedioate Chemical compound COC(=O)CCCC(=O)OC XTDYIOOONNVFMA-UHFFFAOYSA-N 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 3
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229910052624 sepiolite Inorganic materials 0.000 description 3
- 235000019355 sepiolite Nutrition 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 229920003002 synthetic resin Polymers 0.000 description 3
- 239000000057 synthetic resin Substances 0.000 description 3
- QYGBYAQGBVHMDD-XQRVVYSFSA-N (z)-2-cyano-3-thiophen-2-ylprop-2-enoic acid Chemical compound OC(=O)C(\C#N)=C/C1=CC=CS1 QYGBYAQGBVHMDD-XQRVVYSFSA-N 0.000 description 2
- QEGNUYASOUJEHD-UHFFFAOYSA-N 1,1-dimethylcyclohexane Chemical compound CC1(C)CCCCC1 QEGNUYASOUJEHD-UHFFFAOYSA-N 0.000 description 2
- FYGHSUNMUKGBRK-UHFFFAOYSA-N 1,2,3-trimethylbenzene Chemical compound CC1=CC=CC(C)=C1C FYGHSUNMUKGBRK-UHFFFAOYSA-N 0.000 description 2
- KVNYFPKFSJIPBJ-UHFFFAOYSA-N 1,2-diethylbenzene Chemical compound CCC1=CC=CC=C1CC KVNYFPKFSJIPBJ-UHFFFAOYSA-N 0.000 description 2
- QWUWMCYKGHVNAV-UHFFFAOYSA-N 1,2-dihydrostilbene Chemical compound C=1C=CC=CC=1CCC1=CC=CC=C1 QWUWMCYKGHVNAV-UHFFFAOYSA-N 0.000 description 2
- CHLICZRVGGXEOD-UHFFFAOYSA-N 1-Methoxy-4-methylbenzene Chemical compound COC1=CC=C(C)C=C1 CHLICZRVGGXEOD-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- NIEHEMAZEULEKB-UHFFFAOYSA-N 1-ethyl-2-methoxybenzene Chemical compound CCC1=CC=CC=C1OC NIEHEMAZEULEKB-UHFFFAOYSA-N 0.000 description 2
- HDNRAPAFJLXKBV-UHFFFAOYSA-N 1-ethyl-4-methoxybenzene Chemical compound CCC1=CC=C(OC)C=C1 HDNRAPAFJLXKBV-UHFFFAOYSA-N 0.000 description 2
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-heptanol Chemical compound CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 description 2
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 2
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 2
- UWNADWZGEHDQAB-UHFFFAOYSA-N 2,5-dimethylhexane Chemical group CC(C)CCC(C)C UWNADWZGEHDQAB-UHFFFAOYSA-N 0.000 description 2
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 2
- YPQSPODHFDGVAC-UHFFFAOYSA-N Butyl heptanoate Chemical compound CCCCCCC(=O)OCCCC YPQSPODHFDGVAC-UHFFFAOYSA-N 0.000 description 2
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
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Landscapes
- Paints Or Removers (AREA)
- Working Measures On Existing Buildindgs (AREA)
Description
旧塗膜を剥離する方法としては、サンダー処理、ブラスト処理、高圧水噴射、タガネハツリ等の物理的手法、薬剤、溶剤を利用した化学的手法等が挙げられるが、最近では、下地損傷、粉塵飛散等の問題、環境配慮等の観点から、二塩基酸エステル系溶剤を使用した剥離剤が用いられるようになっている。(例えば、特許文献1等)
1.二塩基酸エステルを含む剥離剤組成物であって、
さらに、脂肪酸モノエステルと、脂肪族炭化水素化合物及び芳香族炭化水素化合物を含み、
前記脂肪酸モノエステルが、パルミトレイン酸メチル、パルミトレイン酸エチル、オレイン酸メチル、オレイン酸エチル、オレイン酸プロピル、オレイン酸ブチル、オレイン酸ペンチル、オレイン酸ヘプチル、オレイン酸-2-エチルヘキシル、エライジン酸メチル、エライジン酸エチル、エライジン酸プロピル、エライジン酸ブチル、エライジン酸ペンチル、エライジン酸-2-エチルヘキシル、リノール酸メチル、リノール酸エチル、リノール酸プロピル、リノール酸イソプロピル、リノール酸ブチル、リノール酸ペンチル、リノール酸ヘキシル、リノール酸ヘプチル、リノール酸-2-エチルヘキシル、リノレン酸メチル、リノレン酸エチル、リノレン酸プロピル、リノレン酸ブチル、リノレン酸ペンチル、リノレン酸ヘキシル、リノレン酸ヘプチル、リノレン酸-2-エチルヘキシル、アラキドン酸メチル、アラキドン酸エチル、アラキドン酸ブチル、アラキドン酸-2-エチルヘキシル、エイコセン酸メチル、エイコセン酸エチル、エイコセン酸ブチル、エイコセン酸ヘプチル、エイコセン酸-2-エチルヘキシル、エイコサペンタエン酸メチル、エイコサペンタエン酸エチル、エイコサペンタエン酸ブチル、エイコサペンタエン酸-2-エチルヘキシル、エルカ酸メチル、エルカ酸エチル、エルカ酸ブチル、エルカ酸-2-エチルヘキシル、ドコサヘキサエン酸メチル、ドコサヘキサエン酸エチル、ドコサヘキサエン酸ブチル、ドコサヘキサエン酸-2-エチルヘキシル、リシノール酸メチル、リシノール酸エチル、リシノール酸ブチル、リシノール酸ヘプチル、リシノール酸-2-エチルヘキシルから選ばれる1種または2種以上の不飽和脂肪酸モノエステルを含む、
ことを特徴とする剥離剤組成物。
2.前記二塩基酸エステルと、前記脂肪酸モノエステルとの混合比率(重量比率)が、20:80から80:20であることを特徴とする1.に記載の剥離剤組成物。
本発明は、二塩基酸エステルと脂肪酸モノエステルとが相溶しやすく、二塩基酸エステルと脂肪酸モノエステルとを混合することで旧塗膜内へと浸透しやすくなり、二塩基酸エステルの剥離効果を素早く発揮させる(速効性)ことができるとともに、脂肪酸モノエステルが揮発しにくく、二塩基酸エステルの剥離効果を長時間持続させる(持続性)ことができることを見出したものである。
さらに本発明では、脂肪族炭化水素化合物及び/または芳香族炭化水素化合物を含むことで、上記速効性、持続性を高めることができることを見出したものである。すなわち脂肪族炭化水素化合物及び/または芳香族炭化水素化合物は、旧塗膜内へと浸透しやすく、また塗膜を軟化させやすいため、上記剥離効果(速効性、持続性)に優れた剥離剤組成物を得ることができる。特に脂肪族炭化水素化合物を含む場合は、剥離効果の持続性を向上させることができ、芳香族炭化水素化合物を含む場合は、剥離効果の速効性を向上させることができる。
また本発明では、10℃以上の常温ではもちろんのこと、10℃未満の低温下においても、剥離効果の速効性、持続性に優れたものである。
具体的には、コハク酸ジメチル、グルタル酸ジメチル、アジピン酸ジメチル、フタル酸ジメチル、マレイン酸ジメチル、コハク酸ジエチル、グルタル酸ジエチル、アジピン酸ジエチル、フタル酸ジエチル、マレイン酸ジエチル、コハク酸ジイソブチル、グルタル酸ジイソブチル、アジピン酸ジイソブチル、フタル酸ジイソブチル、マレイン酸ジイソブチル、コハク酸ジブチル、グルタル酸ジブチル、アジピン酸ジブチル、フタル酸ジブチル、マレイン酸ジブチル、コハク酸ジヘキシル、グルタル酸ジヘキシル、アジピン酸ジヘキシル、フタル酸ジヘキシル、マレイン酸ジヘキシル、コハク酸ジ-2-エチルヘキシル、グルタル酸ジ-2-エチルヘキシル、アジピン酸ジ-2-エチルヘキシル、フタル酸ジ-2-エチルヘキシル、マレイン酸ジ-2-エチルヘキシル等が挙げられ、これらのうち1種または2種以上を用いることができる。本発明では特に、グルタル酸ジメチル、アジピン酸ジメチルから選ばれる1種以上を含むことが好ましい。
二塩基酸エステルの含有量は、組成物全量に対し、15重量%以上70重量%以下、さらには25重量%以上65重量%以下であることが好ましい。二塩基酸エステルは、主に剥離効果を付与する成分で、上記含有量であることにより優れた剥離効果を発揮することができる。
具体的には、ヘキサン酸メチル、ヘキサン酸エチル、ヘキサン酸ブチル、ヘキサン酸ヘキシル、ヘキサン酸ヘプチル、ヘキサン酸オクチル、ヘプタン酸メチル、ヘプタン酸エチル、ヘプタン酸プロピル、ヘプタン酸ブチル、ヘプタン酸ヘキシル、ヘプタン酸オクチル、オクタン酸メチル、オクタン酸エチル、オクタン酸プロピル、オクタン酸ブチル、オクタン酸ペンチル、オクタン酸ヘキシル、オクタン酸ヘプチル、オクタン酸オクチル、ノナン酸メチル、ノナン酸エチル、ノナン酸プロピル、ノナン酸ブチル、ノナン酸ペンチル、ノナン酸ヘプチル、デカン酸メチル、デカン酸エチル、デカン酸プロピル、デカン酸ブチル、デカン酸ヘキシル、デカン酸ヘプチル、ドデカン酸メチル、ドデカン酸エチル、ドデカン酸プロピル、ドデカン酸ブチル、ドデカン酸ヘキシル、ドデカン酸ヘプチル、ドデカン酸オクチル、テトラデカン酸メチル、テトラデカン酸エチル、テトラデカン酸プロピル、テトラデカン酸ブチル、テトラデカン酸テトラデシル、ヘキサデカン酸メチル、ヘキサデカン酸エチル、ヘキサデカン酸プロピル、ヘキサデカン酸ブチル、ヘキサデカン酸2-エチルヘキシル、オクタデカン酸メチル、オクタデカン酸エチル、オクタデカン酸プロピル、オクタデカン酸ブチル、オクタデカン酸2-エチルヘキシル、オクタデカン酸オクタデシル、エイコサン酸メチル、エイコサン酸エチル等の飽和脂肪酸モノエステル、
パルミトレイン酸メチル、パルミトレイン酸エチル、オレイン酸メチル、オレイン酸エチル、オレイン酸プロピル、オレイン酸ブチル、オレイン酸ペンチル、オレイン酸ヘプチル、オレイン酸-2-エチルヘキシル、エライジン酸メチル、エライジン酸エチル、エライジン酸プロピル、エライジン酸ブチル、エライジン酸ペンチル、エライジン酸-2-エチルヘキシル、リノール酸メチル、リノール酸エチル、リノール酸プロピル、リノール酸イソプロピル、リノール酸ブチル、リノール酸ペンチル、リノール酸ヘキシル、リノール酸ヘプチル、リノール酸-2-エチルヘキシル、リノレン酸メチル、リノレン酸エチル、リノレン酸プロピル、リノレン酸ブチル、リノレン酸ペンチル、リノレン酸ヘキシル、リノレン酸ヘプチル、リノレン酸-2-エチルヘキシル、アラキドン酸メチル、アラキドン酸エチル、アラキドン酸ブチル、アラキドン酸-2-エチルヘキシル、エイコセン酸メチル、エイコセン酸エチル、エイコセン酸ブチル、エイコセン酸ヘプチル、エイコセン酸-2-エチルヘキシル、エイコサペンタエン酸メチル、エイコサペンタエン酸エチル、エイコサペンタエン酸ブチル、エイコサペンタエン酸-2-エチルヘキシル、エルカ酸メチル、エルカ酸エチル、エルカ酸ブチル、エルカ酸-2-エチルヘキシル、ドコサヘキサエン酸メチル、ドコサヘキサエン酸エチル、ドコサヘキサエン酸ブチル、ドコサヘキサエン酸-2-エチルヘキシル、リシノール酸メチル、リシノール酸エチル、リシノール酸ブチル、リシノール酸ヘプチル、リシノール酸-2-エチルヘキシル等の不飽和脂肪酸モノエステル、
あるいはヤシ油脂肪酸、パーム油脂肪酸、ナタネ油脂肪酸、大豆油脂肪酸、水添大豆油脂肪酸、亜麻仁油脂肪酸、桐油脂肪酸、トール油脂肪酸、脱水ヒマシ油脂肪酸、ヒマシ油脂肪酸、ブドウ種子油脂肪酸、黒クミン油脂肪酸、カボチャ核油脂肪酸、ボラージ種子油脂肪酸、小麦胚種油脂肪酸、菜種油脂肪酸、ヒマワリ油脂肪酸、ピーナッツ油脂肪酸、杏仁油脂肪酸、ピスタチオ油脂肪酸、アーモンド油脂肪酸、オリーブ油脂肪酸、マカデミアナッツ油脂肪酸、アボカド油脂肪酸、シーバックソーン油脂肪酸、ごま油脂肪酸、大麻油脂肪酸、ヘーゼルナッツ油脂肪酸、サクラソウ油脂肪酸、野ばら油脂肪酸、ベニバナ油脂肪酸、くるみ油脂肪酸等のモノエステル、バイオディーゼル等が挙げられ、これらのうち1種または2種以上を用いることができる。
本発明では特に、不飽和脂肪酸モノエステルを含むことが好ましく、特にオレイン酸メチル、リノール酸メチル、リノレン酸メチル等から選ばれる1種または2種以上を好ましく用いることができる。
脂肪酸モノエステルの含有量は、二塩基酸エステルと脂肪酸モノエステルとの混合比率(重量比率)で、20:80から80:20、さらには30:70から70:30であることが好ましい。
このような混合比率であることにより、剥離効果の速効性、持続性に優れた剥離剤組成物を得ることができる。
脂肪族炭化水素化合物を含む場合、脂肪族炭化水素化合物の含有量は、組成物全量に対し、1重量%以上20重量%以下、さらには2重量%以上15重量%以下であることが好ましい。脂肪族炭化水素化合物を含むことによって、特に、剥離効果の持続性を向上させることができる。
芳香族炭化水素化合物を含む場合、芳香族炭化水素化合物の含有量は、組成物全量に対し、5重量%以上50重量%以下、さらには10重量%以上40重量%以下であることが好ましい。芳香族炭化水素化合物を含むことによって、特に、剥離効果の速効性を向上させることができる。
本発明では特に、含窒素溶剤、芳香族アルコールから選ばれる1種以上を好ましく用いることができる。
本発明では特に、セピオライト及び/またはパリゴルスカイトを含むことが好ましく、旧塗膜を軟化させやすく、剥離可能の状態を長時間保持することができる。なおパリゴルスカイトは、アタパルジャイトともいい、本発明ではパリゴルスカイトとアタパルジャイトは同義で扱う。
増粘剤の含有量は、本発明の効果を損なわない限り特に限定されないが、組成物全量に対しその合計量で、0.1重量%以上15重量%以下、さらには0.5重量%以上10重量%以下であることが好ましい。
アミン化合物としては、例えば、モノメチルアミン、モノエチルアミン、イソプロピルアミン、モノブチルアミン、シクロヘキシルアミン、モノエタノールアミン、ジエタノールアミン、トリエタノールアミン、イソプロパノールアミン等が挙げられる。
旧塗膜としては、例えば、JIS K5621「一般用さび止めペイント」、JIS K5651「アミノアルキド樹脂塗料」、JIS K5658「建築用耐候性上塗り塗料」、JIS K5659「鋼構造物用耐候性塗料」、JIS K5660「つや有合成樹脂エマルションペイント」、JIS K5663「合成樹脂エマルションペイント」、JIS K5668「合成樹脂エマルション模様塗料」、JIS K5670「アクリル樹脂系非水分散形塗料」、JIS A6909「建築用仕上塗材」等が挙げられる。
・二塩基酸エステル1:フタル酸ジメチル
・二塩基酸エステル2:グルタル酸ジメチル
・二塩基酸エステル3:コハク酸ジメチル
・二塩基酸エステル4:アジピン酸ジメチル
・脂肪酸モノエステル1:オクタデカン酸メチル
・脂肪酸モノエステル2:オクタデカン酸オクタデシル
・脂肪酸モノエステル3:オレイン酸メチル
・脂肪酸モノエステル4:リノール酸メチル
・脂肪族炭化水素化合物1:パラフィン
・芳香族炭化水素化合物1:ソルベッソ100
・芳香族炭化水素化合物1:キシレン
・溶剤1:N-メチルピロリドン
・溶剤2:ベンジルアルコール
・増粘剤1:セピオライト
・増粘剤2:パリゴルスカイト
・増粘剤3:ベントナイト
温度23度、相対湿度50%の環境下および温度5℃の環境下にて、それぞれ下記に示す旧塗膜面が垂直となるように置き、表1に示す剥離用組成物を下記に示す所要量でローラー塗りし、下記の試験を実施した。
旧塗膜1:スレート板(300×300×6mm)の片面に、アクリル樹脂、酸化チタンを主成分とするアクリル樹脂エナメルを吹付け、塗膜厚0.2mmの塗膜を形成させ、これを促進耐候性試験機「アイスーパーUVテスター」(岩崎電気株式会社製)にて400時間曝露させたものを旧塗膜とした。剥離用組成物所要量0.5kg/m2。
旧塗膜2:スレート板(300×300×6mm)の片面に、アクリルシリコン樹脂、酸化チタンを主成分とするアクリルシリコン樹脂塗料を吹付け、塗膜厚0.2mmの塗膜を形成させ、これを促進耐候性試験機「アイスーパーUVテスター」(岩崎電気株式会社製)にて400時間曝露させたものを旧塗膜とした。剥離用組成物所要量0.5kg/m2。
塗付後3時間後、ヘラを用いて塗膜剥離を行い、その度合いを、「5」(問題無くスムーズに剥離でき、優れた剥離効果を示した。)から「1」(剥離が困難であり、剥離効果に劣っていた。)の5段階で評価した。結果は表1に示す。
塗付後48時間後、ヘラを用いて塗膜剥離を行い、その度合いを評価した。評価は試験1と同様である。結果は表1に示す。
Claims (2)
- 二塩基酸エステルを含む剥離剤組成物であって、
さらに、脂肪酸モノエステルと、脂肪族炭化水素化合物及び芳香族炭化水素化合物を含み、
前記脂肪酸モノエステルが、パルミトレイン酸メチル、パルミトレイン酸エチル、オレイン酸メチル、オレイン酸エチル、オレイン酸プロピル、オレイン酸ブチル、オレイン酸ペンチル、オレイン酸ヘプチル、オレイン酸-2-エチルヘキシル、エライジン酸メチル、エライジン酸エチル、エライジン酸プロピル、エライジン酸ブチル、エライジン酸ペンチル、エライジン酸-2-エチルヘキシル、リノール酸メチル、リノール酸エチル、リノール酸プロピル、リノール酸イソプロピル、リノール酸ブチル、リノール酸ペンチル、リノール酸ヘキシル、リノール酸ヘプチル、リノール酸-2-エチルヘキシル、リノレン酸メチル、リノレン酸エチル、リノレン酸プロピル、リノレン酸ブチル、リノレン酸ペンチル、リノレン酸ヘキシル、リノレン酸ヘプチル、リノレン酸-2-エチルヘキシル、アラキドン酸メチル、アラキドン酸エチル、アラキドン酸ブチル、アラキドン酸-2-エチルヘキシル、エイコセン酸メチル、エイコセン酸エチル、エイコセン酸ブチル、エイコセン酸ヘプチル、エイコセン酸-2-エチルヘキシル、エイコサペンタエン酸メチル、エイコサペンタエン酸エチル、エイコサペンタエン酸ブチル、エイコサペンタエン酸-2-エチルヘキシル、エルカ酸メチル、エルカ酸エチル、エルカ酸ブチル、エルカ酸-2-エチルヘキシル、ドコサヘキサエン酸メチル、ドコサヘキサエン酸エチル、ドコサヘキサエン酸ブチル、ドコサヘキサエン酸-2-エチルヘキシル、リシノール酸メチル、リシノール酸エチル、リシノール酸ブチル、リシノール酸ヘプチル、リシノール酸-2-エチルヘキシルから選ばれる1種または2種以上の不飽和脂肪酸モノエステルを含む、
ことを特徴とする剥離剤組成物。 - 前記二塩基酸エステルと、前記脂肪酸モノエステルとの混合比率(重量比率)が、20:80から80:20であることを特徴とする請求項1に記載の剥離剤組成物。
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