JP7372454B2 - 洗剤組成物 - Google Patents
洗剤組成物 Download PDFInfo
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- JP7372454B2 JP7372454B2 JP2022515929A JP2022515929A JP7372454B2 JP 7372454 B2 JP7372454 B2 JP 7372454B2 JP 2022515929 A JP2022515929 A JP 2022515929A JP 2022515929 A JP2022515929 A JP 2022515929A JP 7372454 B2 JP7372454 B2 JP 7372454B2
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- aqueous liquid
- detergent composition
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- 239000000203 mixture Substances 0.000 title claims description 285
- 239000003599 detergent Substances 0.000 title claims description 118
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 66
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- 239000007788 liquid Substances 0.000 claims description 51
- 229920001296 polysiloxane Polymers 0.000 claims description 46
- 125000000217 alkyl group Chemical group 0.000 claims description 37
- 125000004432 carbon atom Chemical group C* 0.000 claims description 33
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- 125000003118 aryl group Chemical group 0.000 claims description 25
- 239000004744 fabric Substances 0.000 claims description 25
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
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- IIGMITQLXAGZTL-UHFFFAOYSA-N octyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCCCCCCC IIGMITQLXAGZTL-UHFFFAOYSA-N 0.000 claims description 9
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- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 6
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- 125000001424 substituent group Chemical group 0.000 description 4
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- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 3
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- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
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- UWHZIFQPPBDJPM-BQYQJAHWSA-N trans-vaccenic acid Chemical compound CCCCCC\C=C\CCCCCCCCCC(O)=O UWHZIFQPPBDJPM-BQYQJAHWSA-N 0.000 description 1
- 239000005051 trimethylchlorosilane Substances 0.000 description 1
- 125000000026 trimethylsilyl group Chemical group [H]C([H])([H])[Si]([*])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
- C11D3/3734—Cyclic silicones
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/37—Mixtures of compounds all of which are anionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0026—Low foaming or foam regulating compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
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Description
本明細書の水性液体洗剤組成物は、好ましくは、洗濯洗剤組成物であり、より好ましくは、HE洗濯機及び北米の家庭で従来見られる上部投入型の家庭用洗濯機の両方における使用を意味する、両用水性液体洗濯洗剤組成物である。洗浄及び適切な泡立ちレベルを組み合わせたこれらの組成物の利点は、この市場で最もよく見られるが、このような組成物は、当然のことながら、他の洗濯洗浄及び一般的な洗浄分野で使用され得る。
本明細書の洗剤組成物は、濃縮された水性液体又はゲル形態の洗濯洗剤組成物であり得る。本発明の洗剤組成物の水含有量は、組成物の少なくとも1重量%、代替的に約1重量%~約45重量%、代替的に約10重量%~約40重量%の水である。一実施形態では、組成物は、組成物の約35重量%~約99重量%、代替的に約40重量%~約90重量%の水を含む。
本明細書の洗剤組成物は、組成物の約1重量%~約60重量%、代替的に約5重量%~約50重量%、代替的に約15重量%~約35重量%の界面活性剤系を含む。一実施形態では、洗剤組成物は、組成物の約20重量%~約30重量%の界面活性剤系を含む。
本明細書の洗剤組成物は、界面活性剤系の10重量%~約50重量%の非イオン性界面活性剤を含む。一実施形態では、洗剤組成物は、界面活性剤系の約15重量%~約45重量%、代替的に20重量%~40重量%の非イオン性界面活性剤を含む。本開示の組成物は、組成物の約2重量%~約20重量%、又は約3重量%~約16重量%の非イオン性界面活性剤を含み得る。
本明細書の洗剤組成物は、界面活性剤系の0重量%~約10重量%の石鹸を含み得る。「脂肪酸カルボキシレート」とも称される石鹸は、脂肪酸の中和によって形成され、一般式:
RCOO-M+
(式中、Rは、典型的には直鎖又は分枝鎖であってよいC9~C21アルキル基であり、Mはカチオンである)を有する一級カルボキシレート又は石鹸を形成する。特定の実施形態では、RはC9~C17アルキルであり、より具体的には、RはC11~C15である。
本明細書の界面活性剤系は、界面活性剤系の0重量%~約65重量%、代替的に約15重量%~約50重量%の、他のアニオン性界面活性剤、カチオン性界面活性剤、両性界面活性剤、双極性界面活性剤、及びこれらの混合物から選択される追加の界面活性剤を更に含み得る。
洗剤組成物は、AESに加えて、1つ以上の他のアニオン性界面活性剤を含み得る。本来、W.M.Linfield,Marcel Dekker編「Surfactant Science Series」,Vol.7に開示されているような、洗剤組成物の技術分野で既知の全てのアニオン性界面活性剤を使用してもよい。
カチオン性界面活性剤:本発明において有用であるカチオン性界面活性剤は、水溶性、水分散性、又は水不溶性であり得る。このようなカチオン性界面活性剤は、少なくとも1つの四級化窒素及び少なくとも1つの長鎖ヒドロカルビル基を有する。2つ、3つ又は更には4つの長鎖ヒドロカルビル基を含む化合物もまた含まれている。例としては、C12アルキルトリメチルアンモニウムクロリドなどのアルキルトリメチルアンモニウム塩、又はそれらのヒドロキシアルキル置換類似物が挙げられる。当該技術分野で既知の組成物は、例えば、C12アルキルトリメチルアンモニウムクロリドなどの、1%以上のカチオン性界面活性剤を含み得る。このようなカチオン性界面活性剤は、カチオンに帯電した有機部分である。理論に束縛されることを意図するものではないが、カチオン性界面活性剤は、組成物中のアニオン性界面活性剤とイオン対を形成することができ、かつ付着助剤を妨げることができる。本発明の好ましい実施形態では、このようなカチオンに帯電した有機部分、特にカチオン性界面活性剤の使用が回避される。
本発明の流体洗濯洗剤組成物に使用するのに好適な両性又は双極性の洗浄性界面活性剤としては、ヘアケア又は他のパーソナルケアクレンジングにおける使用が既知のものが挙げられる。好適な双極性又は両性界面活性剤の非限定的な例は、米国特許第5,104,646号(Bolich Jr.ら)、同第5,106,609号(Bolich Jr.ら)に記載されている。
本明細書の洗剤組成物は、組成物の約0.001重量%~約4.0重量%の、シリコーン消泡剤化合物、シリコーン油及び疎水性粒子の消泡剤化合物、及びこれらの混合物から選択される消泡剤を含む。一実施形態では、本明細書の洗剤組成物は、組成物の約0.01重量%~約2.0重量%、代替的に0.05重量%~約1.0重量%のシリコーン消泡剤を含む。(いかなるキャリアも含まない活性物質の量による百分率。)
a)約80~約92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、ステアリン酸オクチル中約5~約14%のMQ樹脂、及び約3~約7%の変性シリカの混合物、
b)約78~約92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、ステアリン酸オクチル中約3~約10%のMQ樹脂、約4~約12%の変性シリカの混合物、並びに
c)これらの混合物、から選択され、
百分率は消泡剤の重量による。
i)一次充填剤、好ましくは変性シリカと組み合わせた、アリール又はアルカリール置換基を有するオルガノ変性シリコーンポリマー、及び
ii)シリコーン樹脂、好ましくはM/Q樹脂、の混合物から選択される。
ただし合計d+e≦3であり、オルガノポリシロキサン樹脂中、式(II)の全ての単位の50%未満において、合計d+eは2である。
本明細書で有用な消泡剤としては、米国特許第6,251,586号及び同第6,251,587号(両方ともDow Corning)に記載されているシリコーン消泡剤が挙げられる。かかる消泡剤は、(A)式X--Ph(式中、Xは、炭素原子を介してケイ素に結合される二価の脂肪族有機基を意味し、Phは、芳香族基を意味する)である少なくとも1つのケイ素結合置換基を有するオルガノポリシロキサン物質と、(B)有機ケイ素樹脂と、(C)疎水性充填剤と、を含む。芳香族基は、非置換でも置換されていてもよい。
本明細書の洗剤組成物は、組成物の約0.01重量%~約2.5重量%の構造化剤を含む。
本明細書で有用な外部構造化剤としては、天然由来及び/又は合成ポリマー構造化剤、結晶性ヒドロキシル含有構造化剤、並びにこれらの混合物であるものが挙げられる。
R3は、R1又はHであり、
R4は、独立して、少なくとも1つのヒドロキシル基を含むC10~C22アルキル又はアルケニルである);
Mは、Na+、K+、Mg++、若しくはAl3+、又はHである);及び
iii)これらの混合物。
(x+a)は、11~17であり、(y+b)は、11~17であり、
(z+c)は、11~17である。好ましくは、x=y=z=10及び/又はa=b=c=5である。
Z-(CH(OH))a-Z’
(式中、aは2~4であり、好ましくは2であり、Z及びZ’は疎水性基であり、特にC6~C20アルキル又はシクロアルキル、C6~C24アルカリール又はアラルキル、C6~C20アリール又はこれらの混合物から選択される)の化合物が挙げられる。任意選択的に、Zは1個以上の非極性酸素原子をエーテル又はエステル内にあるようなものとして含有することができる。
本明細書で使用される場合、「内部構造化剤」は、組成物の内部構造を形成するために、処方の選択された要素を使用することを意味する。このような内部構造化液体洗濯洗剤又はゲル組成物は、石鹸、又は硫酸ナトリウムと組み合わせて脂肪酸を含んでよく、アルキルポリエトキシサルフェートを含む1つ以上の界面活性剤を使用してラメラ相の形成によってゲル化構造を形成することができる。
本明細書の洗剤組成物は、組成物の約0.01重量%~約10.0重量%の洗濯補助剤を含んでよい。任意の従来の洗濯洗剤成分を使用することができる。本明細書で有用な洗濯補助剤の例としては、酵素、酵素安定剤、蛍光増白剤、粒子物質、ヒドロトロープ、香料及び他の臭気制御剤、汚れ懸濁ポリマー及び/又は汚れ遊離ポリマー、抑泡剤、布地ケア効果剤、pH調整剤、移染防止剤、防腐剤、色相染料、非布地直接染料、カプセル化活性物質(例えば香料マイクロカプセル又はカプセル化漂白剤)、並びにこれらの混合物が挙げられる。
本明細書の洗剤組成物は、洗浄性能及び/又は布地ケア効果を提供する1つ以上の洗浄性酵素を含み得る。好適な酵素の例としては、ヘミセルラーゼ、ペルオキシダーゼ、プロテアーゼ、セルラーゼ、キシラナーゼ、リパーゼ、ホスホリパーゼ、エステラーゼ、クチナーゼ、ペクチナーゼ、ケラタナーゼ、レダクターゼ、オキシダーゼ、フェノールオキシダーゼ、リポキシゲナーゼ、リグニナーゼ、プルラナーゼ、タンナーゼ、ペントサナーゼ、マラナーゼ、β-グルカナーゼ、アラビノシダーゼ、ヒアルロニダーゼ、コンドロイチナーゼ、ラッカーゼ、及び既知のアミラーゼ、又はこれらの組み合わせが挙げられる。好ましい酵素の組み合わせは、アミラーゼとともに、プロテアーゼ、リパーゼ、クチナーゼ及び/又はセルラーゼのような従来の洗浄性酵素のカクテルを含むものである。洗浄性酵素は、米国特許第6,579,839号により詳細に記載されている。
酵素は、カルシウム及び/又はマグネシウム化合物、ホウ素化合物及び置換されたホウ酸、芳香族ホウ酸エステル、ペプチド及びペプチド誘導体、ポリオール、低分子量カルボン酸塩、比較的疎水性の有機化合物[例えば、特定のエステル、ジアルキルグリコールエーテル(diakyl glycol ethers)、アルコール、又はアルコールアルコキシレート]、カルシウムイオン源に加えてアルキルエーテルカルボン酸塩、ベンズアミジン次亜塩素酸塩、低級脂肪族アルコール及びカルボン酸、N,N-ビス(カルボキシメチル)セリン塩;(メタ)アクリル酸-(メタ)アクリル酸エステルコポリマー及びPEG;リグニン化合物、ポリアミドオリゴマー、グリコール酸又はその塩;ポリヘキサメチレンビグアニド又はN,N-ビス-3-アミノ-プロピル-ドデシルアミン又は塩;並びにこれらの混合物のような任意の既知の安定剤系を使用して安定化できる。
織物用の蛍光性白色化剤としても既知であるものが、本発明の流体洗濯洗剤組成物において有用な洗濯用補助剤である。好適な使用レベルは、流体洗濯洗剤組成物の0.001重量%~1重量%である。増白剤は、例えば欧州特許第686691(B)号に開示されており、疎水性タイプ及び親水性タイプを含む。本明細書での使用には、増白剤49(Brightener 49)及び増白剤15(Brightener 15)が好ましい。
色相染料、シェーディング染料、色相剤、及びロイコ染料は、流体洗濯洗剤組成物において布地シェーディング剤として有用な洗濯用補助剤である。洗濯におけるこれらの材料の歴史は長く、何年も前の「洗濯用青味剤」の使用に端を発する。より最近の開発としては、亜鉛又はアルミニウムの中心原子を有するスルホン化フタロシアニン染料の使用が挙げられ、更により最近では、その色相又はシェーディング効果のために多種多様な他の青色及び/又は紫色染料が使用されている。例えば、国際公開第2009/087524(A1)号、同第2009/087034(A1)号、及びこれらの参照文献を参照されたい。
流体洗濯洗剤組成物は、粘土、抑泡剤、カプセル化した感受性成分、例えば、カプセル化形態の香料、漂白剤及び酵素、又は真珠光沢剤、顔料粒子、雲母などの審美補助剤などの、粒子物質を含み得る。好適な使用レベルは、流体洗濯洗剤組成物の0.0001重量%~5重量%、又は0.1重量%~1重量%である。
一実施形態では、本明細書の洗剤組成物は、香料を含む。存在する場合、香料は、典型的には、本組成物中に、組成物の0.001重量%~10重量%、好ましくは0.01重量%~5重量%、より好ましくは0.1重量%~3重量%の濃度で組み込まれる。一実施形態では、本発明の洗剤組成物の香料は、250℃以上の沸点及び3.0以上のClogPを有する1つ以上の持続性香料成分を、より好ましくは香料の少なくとも25重量%の濃度で含む。好適な香料、香料成分、及び香料キャリアは、米国特許第5,500,138号及び米国特許出願公開第2002/0035053(A1)号に記載されている。
本明細書の洗剤組成物は、任意選択的に、例えば、組成物の0重量%~15重量%、1重量%~10重量%、3重量%~6重量%などの有効量のヒドロトロープを含み、その結果、流体洗濯洗剤組成物は水に相溶性である。本明細書で使用するのに好適なヒドロトロープとしては、米国特許第3,915,903号に開示されているような、アニオン型のヒドロトロープ、特にキシレンスルホン酸ナトリウム、キシレンスルホン酸カリウム、及びキシレンスルホン酸アンモニウム、トルエンスルホン酸ナトリウム、トルエンスルホン酸カリウム、及びトルエンスルホン酸アンモニウム、クメンスルホン酸ナトリウム、クメンスルホン酸カリウム、クメンスルホン酸ナトリウム、及びクメンスルホン酸アンモニウム、並びにこれらの混合物が挙げられる。
組成物は1つ以上のポリマーを含んでよい。その全てが任意選択的に改質されてもよい非限定的な例としては、国際公開第2016/041676号に記載される、ポリエチレンイミン、カルボキシメチルセルロース、ポリ(ビニルピロリドン)、ポリ(エチレングリコール)、ポリ(ビニルアルコール)、ポリ(ビニルピリジン-N-オキシド)、ポリ(ビニルイミダゾール)、ポリカルボキシレート、又はアルコキシル化置換フェノール(ASP)が挙げられる。ASP分散剤の例としては、Clariantから入手可能なHostapal Bv Conc S1000が挙げられるがこれに限定されない。
ビス((C2H5O)(C2H4O)n)(CH3)-N+-CxH2x-N+-(CH3)-ビス((C2H5O)(C2H4O)n)(式中、nは20~30、xは3~8)を有するポリマー又はその硫酸化若しくはスルホン化した変異体である。ポリプロポキシル化-ポリエトキシル化両親媒性ポリエチレンイミン誘導体もまた、より高いグリース除去及び乳化を達成するために含まれてよい。これらは、好ましくは内側ポリエチレンオキシドブロック及び外側ポリプロピレンオキシドブロックを有するアルコキシル化ポリアルキレンイミンを含んでいてもよい。洗剤組成物はまた、向上した飲料染み除去に有用な未変性ポリエチレンイミンを含有してもよい。様々な分子量のPEIが、BASF Corporationから商品名Lupasol(登録商標)で市販されている。好適なPEIの例としては、Lupasol FG(登録商標)、Lupasol G-35(登録商標)が挙げられるが、これらに限定されない。
ポリアミンは、グリース除去を改善することが知られている。性能のために好ましい環状及び線状アミンは、1,3-ビス(メチルアミン)-シクロヘキサン、4-メチルシクロヘキサン-1,3-ジアミン(BASFにより供給されるBaxxodur ECX 210)、1,3プロパンジアミン、1,6ヘキサンジアミン、1,3ペンタンジアミン(Invistaにより供給されるDytek EP)、2-メチル1,5ペンタンジアミン(Invistaにより供給されるDytek A)である。米国特許第6710023号は、少なくとも3つのプロトン化可能な(protonable)アミンを含有する当該ジアミン及びポリアミンを含有する食器手洗い用組成物を開示している。本発明のポリアミンは、洗浄pHよりも高い少なくとも1つのpKaを有し、少なくとも2つのpkaは約6を超え、洗浄pHよりも低い。好ましいポリアミンは、Dow、BASF、及びHuntmanから市販されるジエチレントリアミン、テトラエチレンペンタミン、ヘキサエチルヘキサミン、ヘプタエチルヘプタミン、オクタエチルオクタミン、ノネチルノナミン、及びこれらの混合物からなる群から選択される。特に好ましいポリエーテルアミンは、米国特許第9752101号、同第9487739号、同第9631163号に記載されるように親油性変性されている。
本発明のいくつかの実施形態では、流体洗濯洗剤組成物は、ポリビニルアルコールなどの水溶性フィルム材料に封入されて、単位用量のパウチを形成する。いくつかの実施形態では、単位用量のパウチは1区画又は多区画パウチを含み、本発明の液体洗濯洗剤組成物を任意の他の従来の粉末又は液体洗剤組成物とともに使用することができる。好適なパウチ及び水溶性フィルム材料の例は、米国特許第6,881,713号、同第6,815,410号、及び同第7,125,828号に示されている。
本明細書の洗剤組成物は、衣服又は他の家庭用織物(シート、タオルなど)などの織物衣類を処理するために使用することができる。
a)水溶液で織物を処理する工程であって、水溶液が、約0.01g/L~約1g/Lの線状アルキルベンゼンスルホネート(linear alkyl benzyne sulfonate)界面活性剤、及び約0.1mg/L~約100mg/Lのシリコーン消泡剤を含むような相対的な量で、水及び洗剤組成物の混合物を含む、工程と、
b)織物をすすぎ及び乾燥させる工程と、を含み、
ここで、水性液体洗剤組成物は、組成物の約1重量%~約60重量%の界面活性剤の界面活性剤系であって、当該界面活性剤系が、
i)線状アルキルベンゼンスルホネート、
ii)1重量%~30重量%のアルキルエトキシル化サルフェート界面活性剤を含む、界面活性剤系と、
b)組成物の約0.001重量%~約4.0重量%の、シリコーン樹脂及び変性シリカである一次充填剤と組み合わせた、アリール又はアルキルアリール置換基を有するオルガノ変性シリコーンポリマーから選択される消泡剤と、
c)組成物の約0.01重量%~約2.5重量%の構造化剤と、を含み、
ここで、線状アルキルベンゼンスルホネートとアルキルエトキシル化サルフェート界面活性剤との比率は、1.1:1~10:1である。
本発明による洗剤組成物
2Dow Corningが供給した、米国特許第6521586号に記載されるように調製された、消泡剤ブレンド:80~92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、5~14%のステアリン酸オクチル中のMQ樹脂、及び3~7%の変性シリカ
3AESのアルキル部分が、約13.9~約14.6個の炭素原子を含む、C12~C15のEO2.5Sのアルキルエトキシサルフェート(Alklyethoxy Sulfate)。
Whirlpool Duet HT高効率前投入型自動洗浄機におけるHE使用時泡形成観察は、48gの処方A及びD及び59gの処方B及びDを各々順番に入れ、洗浄サイクルの長さ及び泡の量について画像評価尺度を使用してモニタリングしながら、70°F、0グレイン/ガロンの硬度の水を使用して、清潔なバラストとともに標準洗浄サイクル(試料毎に別個のサイクル)を実施することにより行う。結果は、48g入れた処方A、処方D、59g入れた処方B及び処方Dは、洗浄サイクルにかかる時間の長さの望ましくない自動的延長、あるいは増加した水の消費をもたらす、過剰な泡立ちにより引き起こされる製造業者が作製した洗濯機の泡ロックを引き起こさないことを示す。
a)組成物の約1重量%~約60重量%の界面活性剤系であって、当該界面活性剤系が、
i)線状アルキルベンゼンスルホネート、
ii)1重量%~30重量%のアルキルエトキシル化サルフェート界面活性剤を含む、界面活性剤系と、
b)組成物の約0.001重量%~約4.0重量%の、シリコーン樹脂及び変性シリカである一次充填剤と組み合わせた、アリール又はアルキルアリール置換基を有するオルガノ変性シリコーンポリマーから選択される消泡剤と、
c)組成物の約0.01重量%~約2.5重量%の構造化剤であって、当該構造化剤が、結晶性ヒドロキシル含有安定剤、ポリマーガム、及びこれらの混合物から選択される、構造化剤と、を含み、
線状アルキルベンゼンスルホネートとアルキルエトキシル化サルフェート界面活性剤との比率が、1.1:1~10:1である、水性液体洗剤組成物。
B.線状アルキルベンゼンスルホネートとアルキルエトキシル化サルフェート界面活性剤との比率が、1.2:1~5:1である、段落Aに記載の水性液体洗剤組成物。
C.組成物が、アミンオキシドを更に含む、段落A又はBに記載の水性液体洗剤組成物。
D.界面活性剤系が、アニオン性界面活性剤、カチオン性界面活性剤、双極性界面活性剤、及びこれらの混合物からなる群から選択される追加の界面活性剤を更に含む、段落A~Cのいずれか1つに記載の水性液体洗剤組成物。
E.消泡剤が、
a)約80~約92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、ステアリン酸オクチル中約5~約14%のMQ樹脂、及び約3~約7%の変性シリカの混合物、
b)約78~約92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、ステアリン酸オクチル中約3~約10%のMQ樹脂、約4~約12%の変性シリカの混合物、並びに
c)これらの混合物、から選択され、
百分率が消泡剤の重量による、段落A~Dのいずれか1つに記載の水性液体洗剤組成物。
F.界面活性剤系が、約30重量%~約75重量%のLASを含む、段落A~Eのいずれか1つに記載の水性液体洗剤組成物。
G.界面活性剤系が、10重量%~50重量%の非イオン性界面活性剤、好ましくは2重量%~20重量%の非イオン性界面活性剤を含む、段落A~Fのいずれか1つに記載の水性液体洗剤組成物。
H.組成物が、0.01~0.2のシリコーン消泡剤を含む、段落A~Gのいずれか1つに記載の水性液体洗剤組成物。
I.組成物が、組成物の約15重量%~約35重量%の界面活性剤系を含む、段落A~Hのいずれか1つに記載の水性液体洗剤組成物。
J.組成物が、組成物の約0.01重量%~約2.0重量%のシリコーン消泡剤を含む、段落A~Iのいずれか1つに記載の水性液体洗剤組成物。
K.界面活性剤系が、界面活性剤系の2重量%~20重量%の非イオン性界面活性剤を含む、段落A~Jのいずれか1つに記載の水性液体洗剤組成物。
L.組成物が、組成物の約0.02重量%~約10.0重量%の、酵素、酵素安定剤、蛍光増白剤、粒子物質、ヒドロトロープ、香料及び他の臭気制御剤、汚れ懸濁ポリマー及び/又は汚れ遊離ポリマー、布地ケア効果剤、pH調整剤、移染防止剤、防腐剤、色相染料、非布地直接染料、カプセル化活性物質、並びにこれらの混合物からなる群から選択される洗濯補助剤を更に含む、段落A~Kのいずれか1つに記載の水性液体洗剤組成物。
M.組成物が、香料マイクロカプセル、色相染料、又はこれらの混合物を更に含む、段落A~Lのいずれか1つに記載の水性液体洗剤組成物。
N.水性液体洗剤組成物で織物衣類を処理する家庭用の方法であって、当該方法が、
a)水溶液で織物を処理する工程であって、水溶液が、約0.01g/L~約1g/Lの線状アルキルベンゼンスルホネート界面活性剤、及び約0.1mg/L~約100mg/Lのシリコーン消泡剤を含むような相対的な量で、水及び段落A~Mのいずれか1つに記載の洗剤組成物の混合物を含む、工程と、
b)織物をすすぎ及び乾燥させる工程と、を含む、方法。
O.アルキルエトキシル化サルフェート界面活性剤(AES)のアルキル部分が、平均して、13.7~約16個の炭素原子分布、より好ましくは13.9~約14.6個の炭素原子分布を含む、段落A~Nのいずれか1つに記載の水性液体洗剤組成物。
P.界面活性剤系が、界面活性剤系の30重量%未満のアルキルエトキシル化サルフェート界面活性剤、好ましくは界面活性剤系の2重量%~10重量%のアルキルエトキシル化サルフェート界面活性剤を含む、段落A~Oのいずれか1つに記載の水性液体洗剤組成物。
Claims (10)
- 泡適合性及び改善された洗浄を有する水性液体洗剤組成物であって、前記組成物は、
a)前記組成物の1重量%~60重量%の界面活性剤系であって、前記界面活性剤系が、
i)前記界面活性剤系の40重量%~60重量%の線状アルキルベンゼンスルホネート、
ii)前記界面活性剤系の1重量%~15重量%のアルキルエトキシル化サルフェート界面活性剤、及び
iii)前記界面活性剤系の10重量%~50重量%の非イオン性界面活性剤を含む、界面活性剤系と、
b)前記組成物の0.001重量%~4.0重量%の、アリール置換基を有するオルガノ変性シリコーンポリマー、アルキルアリール置換基を有するオルガノ変性シリコーンポリマーから選択される消泡剤であって、前記消泡剤が、シリコーン樹脂及び一次充填剤と組み合わされる、消泡剤と、
c)前記組成物の0.01重量%~2.5重量%の構造化剤であって、前記構造化剤が、結晶性ヒドロキシル含有安定剤、ポリマーガム、及びこれらの混合物から選択される、構造化剤と、を含み、
線状アルキルベンゼンスルホネートとアルキルエトキシル化サルフェート界面活性剤との重量比が、1.1:1~10:1である、水性液体洗剤組成物。 - 前記組成物が、アミンオキシドを更に含む、請求項1に記載の水性液体洗剤組成物。
- 前記界面活性剤系が、アニオン性界面活性剤、カチオン性界面活性剤、双極性界面活性剤、及びこれらの混合物からなる群から選択される追加の界面活性剤を更に含む、請求項1又は2に記載の水性液体洗剤組成物。
- 前記消泡剤が、
a)80~92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、5~14%のステアリン酸オクチル中のMQ樹脂、及び3~7%の変性シリカの混合物、
b)78~92%のエチルメチル、メチル(2-フェニルプロピル)シロキサン、3~10%のステアリン酸オクチル中のMQ樹脂、4~12%の変性シリカの混合物、並びに
c)これらの混合物、から選択され、
百分率が前記消泡剤の重量による、請求項1~3のいずれか一項に記載の水性液体洗剤組成物。 - 前記界面活性剤系が、前記界面活性剤系の10重量%~20重量%の非イオン性界面活性剤を含む、請求項1~4のいずれか一項に記載の水性液体洗剤組成物。
- 前記組成物が、前記組成物の0.02重量%~10.0重量%の、酵素、酵素安定剤、蛍光増白剤、粒子物質、ヒドロトロープ、香料、及び他の臭気制御剤、汚れ懸濁ポリマー及び/又は汚れ遊離ポリマー、布地ケア効果剤、pH調整剤、移染防止剤、防腐剤、色相染料、非布地直接染料、カプセル化活性物質、並びにこれらの混合物からなる群から選択される洗濯補助剤を更に含む、請求項1~5のいずれか一項に記載の水性液体洗剤組成物。
- 前記組成物が、香料マイクロカプセル、色相染料、又はこれらの混合物を更に含む、請求項1~6のいずれか一項に記載の水性液体洗剤組成物。
- 水性液体洗剤組成物で織物衣類を処理する家庭用の方法であって、前記方法が、
a)水溶液で織物を処理する工程であって、前記水溶液が、0.01g/L~1g/Lの線状アルキルベンゼンスルホネート界面活性剤、及び0.1mg/L~100mg/Lのシリコーン消泡剤を含むような相対的な量で、水及び請求項1~7のいずれか一項に記載の洗剤組成物の混合物を含む、工程と、
b)前記織物をすすぎ及び乾燥させる工程と、を含む、方法。 - 前記アルキルエトキシル化サルフェート界面活性剤のアルキル部分が、平均して、13.7~16個の炭素原子分布を含む、請求項1~7のいずれか一項に記載の水性液体洗剤組成物。
- 前記界面活性剤系が、前記界面活性剤系の2重量%~10重量%のアルキルエトキシル化サルフェート界面活性剤を含む、請求項1~7及び9のいずれか一項に記載の水性液体洗剤組成物。
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