JP7152178B2 - Deterioration diagnosis method for oil-filled electrical equipment - Google Patents

Deterioration diagnosis method for oil-filled electrical equipment Download PDF

Info

Publication number
JP7152178B2
JP7152178B2 JP2018087920A JP2018087920A JP7152178B2 JP 7152178 B2 JP7152178 B2 JP 7152178B2 JP 2018087920 A JP2018087920 A JP 2018087920A JP 2018087920 A JP2018087920 A JP 2018087920A JP 7152178 B2 JP7152178 B2 JP 7152178B2
Authority
JP
Japan
Prior art keywords
oil
insulating paper
deterioration
filled electrical
electrical equipment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2018087920A
Other languages
Japanese (ja)
Other versions
JP2019194522A (en
Inventor
極 宮島
伸治 宮本
歌那 遠山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Aichi Electric Co Ltd
Original Assignee
Aichi Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aichi Electric Co Ltd filed Critical Aichi Electric Co Ltd
Priority to JP2018087920A priority Critical patent/JP7152178B2/en
Publication of JP2019194522A publication Critical patent/JP2019194522A/en
Application granted granted Critical
Publication of JP7152178B2 publication Critical patent/JP7152178B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Spectrometry And Color Measurement (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Housings And Mounting Of Transformers (AREA)

Description

本発明は、メンテナンス時等に変圧器などの油入電気機器の劣化状態を診断する方法及び当該劣化診断に必要な基準の作製方法に関する。 TECHNICAL FIELD The present invention relates to a method for diagnosing the state of deterioration of an oil-filled electrical device such as a transformer during maintenance or the like, and a method for creating a reference necessary for the deterioration diagnosis.

変圧器などの油入電気機器の劣化診断は、絶縁紙の分解生成物である絶縁油中の一酸化炭素、二酸化炭素などのガス濃度を測定したり、絶縁油中のフルフラール濃度を測定することで間接的に行っていたが、これらの測定は、分析室に設置された油中ガス測定装置(ガスクロマトグラフ)やフルフラール測定装置(液体クロマトグラフ)で行う必要があったので、変圧器等から抽出した絶縁油を一旦分析室に持ち込まなければならず、迅速な分析ができなかった。 Deterioration diagnosis of oil-filled electrical equipment such as transformers is performed by measuring the concentration of gases such as carbon monoxide and carbon dioxide in the insulating oil, which are the decomposition products of insulating paper, and measuring the concentration of furfural in the insulating oil. However, these measurements had to be performed with a gas-in-oil measuring device (gas chromatograph) or furfural measuring device (liquid chromatograph) installed in the analysis room, so the The extracted insulating oil had to be brought to the analysis room once, which prevented rapid analysis.

他方、このような問題を解決できる手段として、絶縁材料に複数波長の光を照射して、その反射吸光度差あるいは反射吸光度比を利用して絶縁紙の劣化を判定する装置が提案されている(下記特許文献1参照)。当該装置は可搬型であるので、変圧器等を設置した現場に持ち込み、直接劣化度合いを分析することが可能である。 On the other hand, as a means for solving such problems, an apparatus has been proposed in which an insulating material is irradiated with light of multiple wavelengths and the deterioration of the insulating paper is determined using the difference or ratio of reflection absorbance ( See Patent Document 1 below). Since the device is portable, it can be brought to the site where the transformer or the like is installed and the degree of deterioration can be analyzed directly.

特許第3440759号Patent No. 3440759

然るに、上記特許文献1記載の装置は、光ファイバーセンサを用いて二波長間の反射吸光度の差から材料(絶縁材料)の劣化度を診断するものであるので、その構成が特殊であり、一般的に高価となる問題点がある。 However, the device described in Patent Document 1 uses an optical fiber sensor to diagnose the degree of deterioration of the material (insulating material) from the difference in the reflection absorbance between two wavelengths, so its configuration is special and general. has the problem of being expensive.

本発明は、前述の問題点を解決できるものであり、高価な装置を用いることなく油入電気機器の劣化診断を迅速に行うことのできる方法を提供するものである。 SUMMARY OF THE INVENTION The present invention is intended to solve the aforementioned problems, and to provide a method for quickly diagnosing deterioration of an oil-filled electrical device without using an expensive device.

請求項1記載の発明は、空気を抜いたり、不活性ガスを封入するための通気孔およびバルブを備えることで、油入電気機器の劣化防止仕様を模擬できるステンレス製の容器内に絶縁油及び絶縁紙を密閉収容して当該容器を加熱し、予定の加熱時間が経過する毎に絶縁紙からその一部を採取して、採取した絶縁紙の一部を冷却した後、当該絶縁紙の一部を使用して平均重合度を測定し、かつ、採取した絶縁紙の残部を、色相を明瞭とすべく脱脂処理して平均重合度の測定値における色見本とするとともに、当該色見本の色相と平均重合度の相関関係を色差基準とし、かつ、劣化診断対象である油入電気機器から絶縁油を抜油、もしくは電気機器本体を吊り上げ、もしくは一部を採取して絶縁を大気中に露出させた後、該絶縁を色見本の油浸状態同士または、脱脂処理による非油浸状態同士で色差を測定し、当該色差を用いて前記色差基準から平均重合度を推定することに特徴を有する。 According to the first aspect of the invention, insulating oil and insulating oil are placed in a stainless steel container that can simulate the deterioration prevention specifications of oil-filled electrical equipment by providing a vent hole and a valve for removing air and enclosing inert gas. Insulating paper is hermetically housed and the container is heated, a part of the insulating paper is sampled every time the predetermined heating time elapses, and after cooling a part of the sampled insulating paper, a part of the insulating paper is The average degree of polymerization is measured using a part, and the remainder of the sampled insulating paper is degreased to clarify the hue and used as a color sample in the measured value of the average degree of polymerization, and the hue of the color sample and the average degree of polymerization as a color difference standard, and remove the insulating oil from the oil-filled electrical equipment that is the target of deterioration diagnosis, or lift the electrical equipment body, or extract a part and expose the insulating paper to the atmosphere. Then, the insulating paper is measured for color difference between the oil-immersed states of the color sample or between the non-oil-immersed states after the degreasing treatment, and the average degree of polymerization is estimated from the color difference standard using the color difference. have

請求項2記載の発明は、請求項1記載の絶縁を白色の色基準と共にホワイトバランスの調整を行って画像撮影し、当該撮影画像と色見本を比較して、色相が近い色見本の平均重合度を、前記色差基準を使用して把握することに特徴を有する。 In the invention of claim 2, an image of the insulating paper of claim 1 is adjusted with a white color reference and the white balance is adjusted, and the photographed image and the color sample are compared, and the average of the color samples with similar hues is obtained. It is characterized in that the degree of polymerization is determined using the color difference criteria.

請求項3記載の発明は、請求項1記載の絶縁を新品の絶縁紙と同一条件で撮影し、前記絶縁と新品の絶縁紙の色差を前記色差基準と比較することで、油入電気機器の劣化度合いを診断することに特徴を有する。 According to the invention of claim 3, the insulating paper of claim 1 is photographed under the same conditions as the new insulating paper, and the color difference between the insulating paper and the new insulating paper is compared with the color difference standard, so that the oil-filled electricity It is characterized by diagnosing the degree of deterioration of equipment.

請求項1記載の発明によれば、油入電気機器の劣化診断に使用する機材を安価に構成することができる。また、前記機材を構成する容器をステンレス製とすることによって、保管中や恒温槽で加熱した場合でも腐食しない。さらに、色見本と色差基準を使用して、油入電気機器の劣化状態を容易に把握することができる。しかも、油入電気機器の劣化防止仕様を容易に模擬できるとともに、油入電気機器を構成する絶縁色見本の油浸・非油浸状態を統一することができ、劣化診断の精度を高めることができる。特に、前記絶縁色見本を脱脂処理により非油浸状態とすることによって、色相が明瞭となり、より一層、劣化診断の精度を高めることができる。 According to the first aspect of the invention, equipment used for diagnosing deterioration of oil-filled electrical equipment can be constructed at low cost. In addition, by using stainless steel for the container constituting the equipment, corrosion does not occur even during storage or when heated in a constant temperature bath. Furthermore, the deterioration state of the oil-filled electrical equipment can be easily grasped by using the color sample and the color difference standard. In addition , it is possible to easily simulate the deterioration prevention specifications of oil-filled electrical equipment, and it is possible to unify the oil-immersed and non-oil-immersed states of the insulating paper and color samples that make up the oil-filled electrical equipment, improving the accuracy of deterioration diagnosis. be able to. In particular, by degreasing the insulating paper and the color sample so that they are not immersed in oil, the hue becomes clearer and the accuracy of deterioration diagnosis can be further improved.

請求項2記載の発明によれば、ホワイトバランスの調整をすることによって、照明や天候の違いに影響されることなく、油入電気機器を構成する絶縁の色相を正確に捉えることができる。 According to the second aspect of the invention, by adjusting the white balance, the hue of the insulating paper constituting the oil-filled electrical equipment can be accurately captured without being affected by differences in illumination and weather.

請求項3記載の発明によれば、色差基準を用いれば、油入電気機器を構成する絶縁と新品の絶縁紙から油入電気機器の劣化度合いを判断することが可能となる。 According to the third aspect of the invention, by using the color difference standard, it is possible to determine the degree of deterioration of the oil-filled electrical equipment from the insulating paper constituting the oil-filled electrical equipment and the new insulating paper.

本発明の実施例に係る色見本作製器の断面図である。1 is a cross-sectional view of a color sample maker according to an embodiment of the present invention; FIG. 本発明の実施例に係る加熱時間毎の絶縁紙の平均重合度と色相の相関関係を示す散布図である。FIG. 5 is a scatter diagram showing the correlation between the average degree of polymerization and hue of insulating paper for each heating time according to the example of the present invention.

本発明の実施例1について図1及び図2を用いて説明する。図1は本発明の実施形態に係る色見本の作製器Aを示している。図1において、1は作製器Aを構成する収容容器であり、収容容器1には、劣化診断対象の油入電気機器に使用されるのと同種の絶縁紙2及び絶縁油3が収容されている。 Embodiment 1 of the present invention will be described with reference to FIGS. 1 and 2. FIG. FIG. 1 shows a color sample maker A according to an embodiment of the present invention. In FIG. 1, reference numeral 1 denotes a container that constitutes a fabricator A. The container 1 contains insulating paper 2 and insulating oil 3 of the same type as those used in the oil-filled electrical equipment to be diagnosed for deterioration. there is

4は収納容器1のフランジ部5に開けられた貫通孔であり、6は収納容器1の上部開口部を閉塞する蓋である。7はフランジ部5の貫通孔4に対応する位置に開けられた蓋6の貫通孔であり、8は蓋6とフランジ部5の間に挟まれて収容容器1内の密閉を保つためのOリングなどのパッキンである。 Reference numeral 4 denotes a through hole formed in the flange portion 5 of the storage container 1, and 6 a lid for closing the upper opening of the storage container 1. As shown in FIG. 7 is a through hole of the lid 6 opened at a position corresponding to the through hole 4 of the flange portion 5, and 8 is sandwiched between the lid 6 and the flange portion 5 to keep the container 1 sealed. It is a packing such as a ring.

9は貫通孔4と貫通孔7に通すボルトであり、10はプレートワッシャ、11はスプリングワッシャを示している。12はボルト9に螺合されるナットであり、収容容器1と蓋2を締結している。 Reference numeral 9 denotes a bolt to be passed through the through holes 4 and 7, 10 denotes a plate washer, and 11 denotes a spring washer. A nut 12 is screwed onto the bolt 9 and fastens the container 1 and the lid 2 .

13は収納容器1内の空気を抜いたり、不活性ガスを封入するために蓋2に開けられた複数の通気孔であり、14は通気孔13に取り付けられた通気管、15は通気管14の先端に取り付けられたバルブである。 Reference numeral 13 denotes a plurality of vent holes in the lid 2 for removing air from the storage container 1 and enclosing inert gas therein; 14 is a vent pipe attached to the vent hole 13; is a valve attached to the tip of the

次に上記構成の作製器Aを用いて、油入電気機器の劣化診断に使用する機材(色差基準)を作製する方法について説明する。 Next, a method of manufacturing equipment (color difference standard) used for deterioration diagnosis of oil-filled electrical equipment using the manufacturing device A having the above configuration will be described.

上記構成の作製器Aは、パッキン8の存在によって収容容器1内部を密閉できる構造となっており、バルブ15に図示しない真空ポンプを接続して一定時間動作させることで、収容容器1内の空間を真空にする。 The preparation device A having the above configuration has a structure that can seal the inside of the container 1 by the presence of the packing 8. By connecting a vacuum pump (not shown) to the valve 15 and operating it for a certain period of time, the space inside the container 1 is to a vacuum.

ここで、劣化診断対象である油入電気機器が不活性ガスを封入している場合は、収容容器1内を真空状態にした後、同種類の不活性ガスを、通気管14を介して収容容器1内に封入することで、劣化診断対象の油入電気機器のケース内の環境と同条件にする。無圧密封の場合は、上面空間を真空のままとする。空気密封式の場合は、空気を密封する。 Here, if the oil-filled electrical equipment to be diagnosed for deterioration contains an inert gas, the same kind of inert gas is contained through the ventilation pipe 14 after the inside of the container 1 is evacuated. By enclosing it in the container 1, the same environment as in the case of the oil-filled electrical equipment to be diagnosed for deterioration is created. In the case of pressureless sealing, the top space is kept under vacuum. In the case of the airtight type, the air is sealed.

この状態で、作製器Aを図示しない恒温槽に入れて、例えば、120~140℃で加熱し、所定時間(過去の経験則によって、劣化診断指標とする重合度が得られると予想した時間)が経過する毎に、作製器Aを恒温槽から取り出し、常温まで冷却する。この収容容器1及び蓋6は金属製であれば良いが、恒温槽で加熱されることを考慮して、保管中や加熱の影響で収容容器が腐食しないステンレス製とすることが望ましい。
In this state, the preparation device A is placed in a constant temperature bath (not shown) and heated at, for example, 120 to 140 ° C. for a predetermined time (time expected to obtain the degree of polymerization as a deterioration diagnostic index according to past empirical rules). Each time , the preparation device A is taken out from the constant temperature bath and cooled to room temperature. The containing container 1 and the lid 6 may be made of metal, but considering that they will be heated in a constant temperature bath, they are preferably made of stainless steel so that the containing container does not corrode during storage or under the influence of heating.

恒温槽から取り出した作製器Aからナット12、ボルト9を外し、蓋6を開けて、収容容器1内の絶縁紙2から、平均重合度測定に必要な量の絶縁紙を取り出す。 The nut 12 and bolt 9 are removed from the preparation device A taken out of the constant temperature bath, the lid 6 is opened, and the amount of insulating paper necessary for measuring the average degree of polymerization is taken out from the insulating paper 2 in the container 1 .

必要量を取り出した後は、再度、蓋6を収容容器1に被せ、蓋6をボルト9及びナット12で収容容器1に締結する。その後、図示しない真空ポンプを起動することで、収容容器1内を再度真空状態にして、収容容器1内の絶縁紙2と絶縁油3を脱気し、及び、これに加えて、前記油入電気機器が不活性ガスを封入している場合は、同種の不活性ガスを封入する。 After taking out the required amount, the container 1 is covered with the lid 6 again, and the lid 6 is fastened to the container 1 with the bolt 9 and the nut 12 . After that, by activating a vacuum pump (not shown), the inside of the container 1 is again evacuated, the insulating paper 2 and the insulating oil 3 in the container 1 are degassed, and in addition to this, the oil-filled If the electrical equipment is filled with an inert gas, fill it with the same type of inert gas.

その後、作製器Aを再び、恒温槽に入れて加熱し、再度、所定時間(過去の経験則によって、劣化診断指標とする重合度が得られると予想した時間)が経過したら作製器Aを恒温槽から取り出し、以降、前述したと同様の動作を繰り返す。 After that, the preparation device A is again placed in the constant temperature bath and heated, and after a predetermined time (the time expected to obtain the degree of polymerization as a deterioration diagnostic index based on past empirical rules) has passed, the preparation device A is kept at a constant temperature. After removing from the bath, the same operation as described above is repeated.

一方、必要量取り出した絶縁紙はその一部を試料として脱脂、漂白処理後、銅エチレンジアミン、または銅アンモニア溶液に溶解し粘度法によって平均重合度を測定し、取り出した絶縁紙の色相と平均重合度の関係を導く。絶縁紙の平均重合度の測定にはGPC(液体クロマトグラフ)や光散乱などの方法を用いてもよい。 On the other hand, a part of the insulation paper taken out in the necessary amount was degreased and bleached, dissolved in copper ethylenediamine or cuprammonium solution as a sample, and the average degree of polymerization was measured by the viscosity method. It guides the relationship of degrees. A method such as GPC (liquid chromatograph) or light scattering may be used to measure the average degree of polymerization of the insulating paper.

このように、絶縁紙2は所定時間(過去の経験則によって、劣化診断指標とする重合度が得られると予想した時間)が経過する毎に必要量取り出され、その都度、脱脂処理後、平均重合度の測定が行われるので、作製器Aから取り出すまでの加熱時間に応じた絶縁紙2の色相と平均重合度の関係を導くことができる。 In this way, the required amount of the insulating paper 2 is taken out every time a predetermined time (the time expected to obtain the degree of polymerization as a deterioration diagnosis index according to past empirical rules) has passed, and each time, after degreasing, the average Since the degree of polymerization is measured, the relationship between the hue of the insulating paper 2 and the average degree of polymerization according to the heating time until it is taken out of the preparation device A can be derived.

試料とした一部を除いた絶縁紙(以下、残絶縁紙という)は劣化診断の色見本として活用する。JEM1463「変圧器用絶縁紙の平均重合度評価基準」において、絶縁紙の平均重合度450以下で寿命レベル、平均重合度250以下で危険レベルとの判定基準がある。このため、平均重合度250及び平均重合度450の色見本を作製して劣化診断に活用することで、油入電気機器の利用限界を判定することが可能となる。なお、残絶縁紙を脱脂処理することにより、残絶縁紙の色相を明瞭にすることができる。 Insulating paper from which a part of the sample was removed (hereinafter referred to as residual insulating paper) is used as a color sample for deterioration diagnosis. In JEM1463 "Evaluation Standards for Average Degree of Polymerization of Insulating Paper for Transformers", there is a criterion that an average degree of polymerization of 450 or less for insulating paper is a life level, and an average degree of polymerization of 250 or less is a dangerous level. Therefore, by preparing color samples with an average degree of polymerization of 250 and an average degree of polymerization of 450 and using them for deterioration diagnosis, it is possible to determine the usage limit of the oil-filled electrical equipment. By degreasing the remaining insulating paper, the hue of the remaining insulating paper can be made clear.

ここで、絶縁紙2が加熱劣化の進行によってどのように色相の変化を生じるか説明すると、最初、薄黄色であった絶縁紙2は、加熱による劣化が進行するにつれ濃い黄色から茶色に変化し、さらに劣化が進行すると黒ずんだ色に変化する。 Here, an explanation will be given of how the insulating paper 2 changes in hue as heat deterioration progresses. The insulating paper 2, which was light yellow at first, changes from dark yellow to brown as the heat deterioration progresses. , and when the deterioration progresses further, it changes to a dark color.

図2の散布図は絶縁紙の平均重合度と色相の変化量(新品の絶縁紙と前記色見本との間の色の差を、色差という。)の相関関係を示している。図2に示すとおり、前記相関関係は明瞭であるので、劣化診断対象である油入電気機器を構成する絶縁紙を測色計で測色すれば、図2の散布図を利用して前記油入電気機器の劣化度の判定が可能となる。 The scatter diagram of FIG. 2 shows the correlation between the average degree of polymerization of insulating paper and the amount of hue change (the color difference between new insulating paper and the color sample is called color difference). As shown in FIG. 2, the correlation is clear, so if the insulating paper constituting the oil-filled electrical equipment to be diagnosed for deterioration is colorimetrically measured with a colorimeter, the scatter diagram of FIG. It becomes possible to determine the degree of deterioration of the incoming electrical equipment.

このとき、前記油入電気機器の絶縁紙と前記の色見本の関係は、(1)絶縁紙が油浸で色見本が非油浸の場合、(2)絶縁紙が油浸で色見本も油浸の場合、(3)絶縁紙が非油浸で色見本も非油浸の場合、(4)絶縁紙が非油浸で色見本が油浸の場合が考えられる。前記絶縁紙は油入電気機器の絶縁油に浸かった状態であるので、一般に(1)または(2)の場合の色差の関係を用いて診断する。状況が許せば変圧器の絶縁紙と前記の色見本を脱脂し双方とも非油浸状態とすることで、色相が明瞭になり両者の色差が明確になることから、より劣化診断の精度を高めることができる。 At this time, the relationship between the insulating paper of the oil-filled electrical equipment and the color sample is as follows: (1) when the insulating paper is oil-immersed and the color sample is not oil-immersed, (2) when the insulating paper is oil-immersed and the color sample is also In the case of oil immersion, (3) the insulating paper is not immersed in oil and the color sample is also not immersed in oil, and (4) the insulating paper is not immersed in oil and the color sample is oil immersed. Since the insulating paper is in a state of being soaked in the insulating oil of the oil-filled electrical equipment, the diagnosis is generally made using the color difference relationship in case (1) or (2). If the situation permits, the insulation paper of the transformer and the color sample are degreased and both are not immersed in oil, so that the hue becomes clear and the color difference between the two becomes clear, so the accuracy of deterioration diagnosis is further improved. be able to.

つづいて、劣化診断対象である油入電気機器の実施例2に係る劣化診断方法の具体例を説明する。まず、劣化診断対象となる油入電気機器から絶縁油を抜く、電気機器本体を吊り上げる、一部を採取する等により絶縁物を露出させた後、油入電気機器を構成する絶縁物と白色の色見本(JIS Z8102「物体色の色名」等)を並べ、デジタルカメラ等の撮影機材を使用して、ホワイトバランスの調整を行ながら白色の色見本が適確な白さに写るように色調を補正して撮影する。 Next, a specific example of the deterioration diagnosis method according to the second embodiment of the oil-filled electrical equipment, which is the object of deterioration diagnosis, will be described. First, remove the insulating oil from the oil-filled electrical equipment to be diagnosed for deterioration, lift the main body of the electrical equipment, extract a part, etc. to expose the insulator. Arrange the color samples (JIS Z8102 "color name of the object color", etc.), and use shooting equipment such as a digital camera to adjust the white balance while adjusting the color tone so that the white color sample appears in the correct whiteness. Shoot after compensating for

ホワイトバランスの調整はデジタルカメラのプリセットホワイトバランスを使っても良いし、手動で設定するマニュアルホワイトバランスを使用しても良い。ホワイトバランスの調整をすることによって、照明や天候の違いに影響されることなく、油入電気機器を構成する絶縁物の色相を正確に捉えることができる。 White balance may be adjusted using the preset white balance of the digital camera, or manual white balance that is set manually may be used. By adjusting the white balance, it is possible to accurately capture the hue of the insulators that make up the oil-filled electrical equipment without being affected by differences in lighting and weather.

撮影対象となる絶縁物が狭部に存在する場合は、内視鏡ファイバースコープのような撮影機材を利用して撮影してもよい。 If the insulating object to be photographed exists in a narrow area, photographing equipment such as an endoscope fiberscope may be used to photograph it.

このようにして撮影した画像は前述した色見本と比較され、その中から色相が一致するか最も近い色見本を特定する。次に、前述した色差基準を用いて特定した色見本に対応する平均重合度を求める。このようにして絶縁物の平均重合度を求めれば、油入電気機器の劣化度合いを診断することが可能となる。 The image taken in this way is compared with the aforementioned color samples to identify the color sample that matches or is closest in hue. Next, the average degree of polymerization corresponding to the specified color sample is determined using the color difference standard described above. By obtaining the average degree of polymerization of the insulator in this way, it is possible to diagnose the degree of deterioration of the oil-filled electrical equipment.

つづいて、劣化診断対象である油入電気機器の実施例3に係る劣化診断方法の具体例を説明する。まず、劣化診断対象となる油入電気機器から絶縁油を抜く、電気機器本体を吊り上げる、一部を採取する等により絶縁物を露出させ、新品の絶縁紙を同条件で、デジタルカメラ等の撮影機材を使用して撮影する。 Next, a specific example of the method for diagnosing deterioration according to the third embodiment of the oil-filled electrical equipment to be diagnosed for deterioration will be described. First, remove the insulating oil from the oil-filled electrical equipment to be diagnosed for deterioration, lift the electrical equipment body, extract a part, etc. to expose the insulating material, and photograph the new insulating paper under the same conditions with a digital camera, etc. Take pictures with equipment.

撮影した画像で、油入電気機器の絶縁紙と新品の絶縁紙の色相の色差を比較し、請求項2によって作成した平均重合度と色相の相関関係を示す散布図から、色差に当てはまる前記絶縁物の平均重合度を求めることで、油入電気機器の劣化度合いを判断することが可能となる。 In the photographed images, the color difference in hue between the insulating paper of the oil-filled electrical equipment and the new insulating paper is compared, and from the scatter diagram showing the correlation between the average degree of polymerization and the hue created by claim 2, the insulation that applies to the color difference By obtaining the average degree of polymerization of the product, it becomes possible to determine the degree of deterioration of the oil-filled electrical equipment.

以上説明したように、本発明の劣化診断方法によれば、従来のように、油入電気機器から抽出した絶縁油を分析室に持ち帰って、ガスクロマトグラフや液体クロマトグラフによって劣化診断する必要はなく、油入電気機器が設置された現場で迅速に劣化診断をおこなうことができる。 As described above, according to the method of diagnosing deterioration of the present invention, it is not necessary to bring the insulating oil extracted from the oil-filled electrical equipment back to the analysis room and diagnose the deterioration using a gas chromatograph or a liquid chromatograph, unlike the conventional method. , it is possible to quickly diagnose deterioration at the site where oil-filled electrical equipment is installed.

また、上記劣化診断は、絶縁紙と絶縁油の収容容器と、収容容器内を密閉する蓋体からなる作製器およびこれを加熱する恒温槽があればよいので、従来の装置と比較してその構成が簡素であり、安価に構成することができる。 In addition, the deterioration diagnosis described above only requires a fabricating device comprising a container for insulating paper and insulating oil, a lid for sealing the container, and a constant temperature bath for heating the device. The configuration is simple and can be configured at low cost.

さらに、本発明の作製器A内は劣化診断対象となる油入電気機器のケース内とほぼ同じ環境に設定できるので、作製器A内で作製する色見本は劣化診断対象となる油入電気機器のケース内で劣化した絶縁紙と近似する色相及び色差となり、劣化診断の精度を高くすることができる。 Furthermore, since the inside of the preparation device A of the present invention can be set to be almost the same environment as the inside of the case of the oil-filled electrical device to be diagnosed for deterioration, the color sample produced in the preparation device A can be used for the oil-filled electrical device to be diagnosed for deterioration. In this case, the hue and color difference are similar to those of the deteriorated insulating paper, and the accuracy of deterioration diagnosis can be improved.

1 収納容器
2 絶縁紙
3 絶縁油
4、7 貫通孔
5 フランジ部
6 蓋
8 パッキン
9 ボルト
10 プレートワッシャ
11 スプリングワッシャ
12 ナット
13 通気孔
14 通気管
15 バルブ
A 色見本作製器
1 Storage Container 2 Insulating Paper 3 Insulating Oil 4, 7 Through Hole 5 Flange Part 6 Lid 8 Packing 9 Bolt 10 Plate Washer 11 Spring Washer 12 Nut 13 Vent Hole 14 Ventilation Pipe 15 Valve A Color Sample Producer

Claims (3)

空気を抜いたり、不活性ガスを封入するための通気孔およびバルブを備えることで、油入電気機器の劣化防止仕様を模擬できるステンレス製の容器内に絶縁油及び絶縁紙を密閉収容して当該容器を加熱し、予定の加熱時間が経過する毎に絶縁紙からその一部を採取して、採取した絶縁紙の一部を冷却した後、当該絶縁紙の一部を使用して平均重合度を測定し、かつ、採取した絶縁紙の残部を、色相を明瞭とすべく脱脂処理して平均重合度の測定値における色見本とするとともに、当該色見本の色相と平均重合度の相関関係を色差基準とし、かつ、劣化診断対象である油入電気機器から絶縁油を抜油、もしくは電気機器本体を吊り上げ、もしくは一部を採取して絶縁を大気中に露出させた後、該絶縁を色見本の油浸状態同士または、脱脂処理による非油浸状態同士で色差を測定し、当該色差を用いて前記色差基準から平均重合度を推定することを特徴とする油入電気機器の劣化診断方法。 Insulating oil and insulating paper are hermetically housed in a stainless steel container that can mimic the anti-degradation specifications of oil-filled electrical equipment by providing vents and valves for removing air and enclosing inert gas. Heat the container, collect a part of the insulating paper each time the scheduled heating time has passed, cool a part of the collected insulating paper, and then use a part of the insulating paper to measure the average degree of polymerization. is measured, and the remainder of the sampled insulating paper is degreased to clarify the hue and used as a color sample for the measured value of the average degree of polymerization, and the correlation between the hue of the color sample and the average degree of polymerization The insulating paper is exposed to the atmosphere by extracting the insulating oil from the oil-filled electrical equipment that is used as a color difference standard and is the target of deterioration diagnosis, or by lifting the main body of the electrical equipment, or extracting a part of it, and then removing the insulating paper . Deterioration of oil-filled electrical equipment characterized by measuring the color difference between color samples in oil-immersed states or between non-oil-immersed states after degreasing, and estimating the average degree of polymerization from the color difference standard using the color difference. diagnostic method. 前記絶縁を白色の色基準と共にホワイトバランスの調整を行って画像撮影し、当該撮影画像と色見本を比較し、色相が近い色見本の平均重合度を、前記色差基準を使用して把握することによって、油入電気機器の劣化度合いを診断することを特徴とする請求項1記載の油入電気機器の劣化診断方法。 The insulating paper is photographed together with a white color reference after adjusting the white balance, the photographed image and the color sample are compared, and the average degree of polymerization of the color sample having a similar hue is grasped using the color difference reference. 2. The method for diagnosing deterioration of an oil-filled electrical device according to claim 1, wherein the degree of deterioration of the oil-filled electrical device is diagnosed by means of the oil-filled electrical device. 前記絶縁を新品の絶縁紙と同一条件で撮影し、当該絶縁物と新品の絶縁紙の色差を前記色差基準と比較することで、油入電気機器の劣化度合いを診断することを特徴とする請求項1記載の油入電気機器の劣化診断方法。 The insulating paper is photographed under the same conditions as the new insulating paper, and the color difference between the insulating material and the new insulating paper is compared with the color difference standard, thereby diagnosing the degree of deterioration of the oil-filled electrical equipment. The method for diagnosing deterioration of an oil-filled electrical device according to claim 1 .
JP2018087920A 2018-04-30 2018-04-30 Deterioration diagnosis method for oil-filled electrical equipment Active JP7152178B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2018087920A JP7152178B2 (en) 2018-04-30 2018-04-30 Deterioration diagnosis method for oil-filled electrical equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2018087920A JP7152178B2 (en) 2018-04-30 2018-04-30 Deterioration diagnosis method for oil-filled electrical equipment

Publications (2)

Publication Number Publication Date
JP2019194522A JP2019194522A (en) 2019-11-07
JP7152178B2 true JP7152178B2 (en) 2022-10-12

Family

ID=68469588

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018087920A Active JP7152178B2 (en) 2018-04-30 2018-04-30 Deterioration diagnosis method for oil-filled electrical equipment

Country Status (1)

Country Link
JP (1) JP7152178B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021007126A (en) * 2019-06-28 2021-01-21 愛知電機株式会社 Manufacturing method of color sample/color difference standard and deterioration diagnosis method of oil-filled electric device using color difference standard

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021096194A (en) * 2019-12-19 2021-06-24 愛知電機株式会社 Method of preparing tensile strength standard and deterioration diagnosis method for oil-filled electric equipment using tensile strength
CN112861920B (en) * 2021-01-15 2024-06-14 佛山科学技术学院 Palm oil heating time prediction system and method

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002005840A (en) 2000-06-20 2002-01-09 Aichi Electric Co Ltd Method and apparatus for diagnosis of deterioration of oil-filled electrical apparatus
JP2002367842A (en) 2001-06-04 2002-12-20 Mitsubishi Electric Corp Method for evaluating degree of deterioration in coil insulating paper
JP2003207440A (en) 2002-01-11 2003-07-25 Chubu Electric Power Co Inc Method of measuring degree of degradation of electric insulating paper
JP2003344262A (en) 2002-05-28 2003-12-03 Mitsubishi Electric Corp Method for diagnosing degree of deterioration of high polymer material
US20050072964A1 (en) 2003-10-02 2005-04-07 Rapp Kevin J. Additive for dielectric fluid
JP2008083035A (en) 2006-09-01 2008-04-10 Chubu Electric Power Co Inc Degradation determining method and apparatus for determining degradation of cellulose fibers
JP2012021846A (en) 2010-07-13 2012-02-02 Chubu Electric Power Co Inc Method for estimating degree of deterioration of cellulose fiber
JP2012160670A (en) 2011-02-02 2012-08-23 Chugoku Electric Power Co Inc:The Deterioration diagnosis device of oil-immersed transformer

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06767Y2 (en) * 1987-07-08 1994-01-05 日本石油株式会社 Lubricating oil simple life judging device
JPS6420604A (en) * 1987-07-16 1989-01-24 Mitsubishi Electric Corp Examination of deterioration of insulator in oil-insulated electric equipment
JPH04220547A (en) * 1990-12-21 1992-08-11 Tokyo Electric Power Co Inc:The Method and apparatus for judging deterioration degree of insulating material
JPH0743414A (en) * 1993-07-26 1995-02-14 Sumitomo Metal Ind Ltd Aging diagnostic method of insulating paper for oil-filled electric equipment
JP3310786B2 (en) * 1994-08-22 2002-08-05 富士写真フイルム株式会社 Color thermal recording paper package and color thermal printer

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002005840A (en) 2000-06-20 2002-01-09 Aichi Electric Co Ltd Method and apparatus for diagnosis of deterioration of oil-filled electrical apparatus
JP2002367842A (en) 2001-06-04 2002-12-20 Mitsubishi Electric Corp Method for evaluating degree of deterioration in coil insulating paper
JP2003207440A (en) 2002-01-11 2003-07-25 Chubu Electric Power Co Inc Method of measuring degree of degradation of electric insulating paper
JP2003344262A (en) 2002-05-28 2003-12-03 Mitsubishi Electric Corp Method for diagnosing degree of deterioration of high polymer material
US20050072964A1 (en) 2003-10-02 2005-04-07 Rapp Kevin J. Additive for dielectric fluid
JP2008083035A (en) 2006-09-01 2008-04-10 Chubu Electric Power Co Inc Degradation determining method and apparatus for determining degradation of cellulose fibers
JP2012021846A (en) 2010-07-13 2012-02-02 Chubu Electric Power Co Inc Method for estimating degree of deterioration of cellulose fiber
JP2012160670A (en) 2011-02-02 2012-08-23 Chugoku Electric Power Co Inc:The Deterioration diagnosis device of oil-immersed transformer

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021007126A (en) * 2019-06-28 2021-01-21 愛知電機株式会社 Manufacturing method of color sample/color difference standard and deterioration diagnosis method of oil-filled electric device using color difference standard
JP7344021B2 (en) 2019-06-28 2023-09-13 愛知電機株式会社 Deterioration diagnosis method for oil-filled electrical equipment

Also Published As

Publication number Publication date
JP2019194522A (en) 2019-11-07

Similar Documents

Publication Publication Date Title
JP7152178B2 (en) Deterioration diagnosis method for oil-filled electrical equipment
EP3087534B1 (en) Analysis device, system and program
US10605741B2 (en) Accurate colorimetric based test strip reader system
TWI617797B (en) Oil spill detection system
JP6807259B2 (en) Insulation oil deterioration diagnosis system and method of transformer
US9222903B2 (en) Method of determining the softening- or dropping point
JP2017049030A (en) Device, system, program and method for measuring deterioration level of edible oil
JP4860576B2 (en) Cellulose fiber degradation determination method and degradation determination apparatus
JP7344021B2 (en) Deterioration diagnosis method for oil-filled electrical equipment
JP2021015123A (en) Fat condition measurement device and fryer
CN111856381A (en) Disassembling and defect checking method of oil-immersed upright current transformer
JP2017026495A (en) Degradation information acquisition device, degradation information acquisition system, degradation information acquisition method and degradation information acquisition program
JP2021096194A (en) Method of preparing tensile strength standard and deterioration diagnosis method for oil-filled electric equipment using tensile strength
Kon et al. Estimation of the oxidative deterioration of turbine oil using membrane patch color
ES2334002A1 (en) Systems and methods for quantitatively assessing the quality of an image produced by an imaging system
JP6844976B2 (en) Deterioration information acquisition device, deterioration information acquisition system, deterioration information acquisition method and deterioration information acquisition program
JP2017120233A (en) Degradation information acquisition device, degradation information acquisition system, degradation information acquisition method, and degradation information acquisition program
CN116482079A (en) Detection method and system based on laser-induced breakdown spectroscopy
JP2020101392A (en) Appearance inspection method for lithium ion battery and appearance inspection device for lithium ion battery
CN114907970A (en) Sterility detection mechanism and method for incubator
JP5984045B2 (en) Automated method and apparatus for judging natural deterioration of synthetic fiber safety ropes etc. by the degree of fading of surface color
JP2017122606A (en) Method and device for determining moisture state of cooking target rice, rice immersion time determination device, and rice cooking facility
JPH04220547A (en) Method and apparatus for judging deterioration degree of insulating material
RU2615034C2 (en) Method for determining flash point in closed crucible of petroleum oil fractions
JP2020003350A (en) Oil leakage detection system and oil leakage detection method

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20210419

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20211213

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20220222

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220405

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20220726

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220823

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20220927

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20220929

R150 Certificate of patent or registration of utility model

Ref document number: 7152178

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150