JP6947750B2 - 分散アゾ染料、その製造方法及びその使用 - Google Patents
分散アゾ染料、その製造方法及びその使用 Download PDFInfo
- Publication number
- JP6947750B2 JP6947750B2 JP2018554387A JP2018554387A JP6947750B2 JP 6947750 B2 JP6947750 B2 JP 6947750B2 JP 2018554387 A JP2018554387 A JP 2018554387A JP 2018554387 A JP2018554387 A JP 2018554387A JP 6947750 B2 JP6947750 B2 JP 6947750B2
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- group
- formula
- dye
- dyes
- printing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 0 Cc(c(N=Nc(c(*)c(c(C(N1*)=O)c2)C1=O)c2Br)c(C)nc1*)c1C#N Chemical compound Cc(c(N=Nc(c(*)c(c(C(N1*)=O)c2)C1=O)c2Br)c(C)nc1*)c1C#N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/34—Monoazo dyes prepared by diazotising and coupling from other coupling components
- C09B29/36—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
- C09B29/3604—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
- C09B29/3617—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a six-membered heterocyclic with only one nitrogen as heteroatom
- C09B29/3621—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a six-membered heterocyclic with only one nitrogen as heteroatom from a pyridine ring
- C09B29/3639—Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a six-membered heterocyclic with only one nitrogen as heteroatom from a pyridine ring from a pyridine ring containing one or more amino groups
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0041—Blends of pigments; Mixtured crystals; Solid solutions mixtures containing one azo dye
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Description
R2およびR3はそれぞれ他方のものとは独立に、水素原子、未置換またはシアノ基、カルボキシ基、ヒドロキシ基、C1−C6アルコキシ基もしくはC2−C8アルコキシアルコキシ基で置換されたC1−C12アルキル基、未置換またはシアノ基、カルボキシ基、ヒドロキシ基、C1−C12アルキル基、C1−C6アルコキシ基もしくはC2−C8アルコキシアルコキシ基で置換されたC6−C24アリール基、または未置換またはシアノ基、カルボキシ基、ヒドロキシ基、C1−C12アルキル基、C1−C6アルコキシ基もしくはC2−C8アルコキシアルコキシ基で置換されたC7−C25アラルキル基である。)で表されるアゾ染料に関する。
に従って、式(1a)の染料の合成によって、製造することができる。
101a)で表される染料
m.p.(融点)=217〜226℃
λmax=527nm(λmax=吸収波長最大値、DMFで測定)
C 52.3% 52.4%
H 4.9% 4.9%
N 18.8% 18.6%
1H−NMR(CDCl3,250MHz):δ=11.49(1H,−NH),8.08(s,1H),7.05(1H,−NH),3.69−3.82(m,6H),3.61(t,J=6.1,2H),3.45−3.50(m,2H),3.44(s,3H),3.33(s,3H),2.83(s,3H),1.91−2.00(m,4H),1.31(t,J=7.2,3H)
λmax=527nm(λmax=吸収波長最大値、DMFで測定)
C 60.22% 59.90%
H 5.83% 6.0%
N 21.61% 21.20%
1H−NMR(CDCl3,250MHz):δ=11.35(1H,−NH),8.22(s,1H),8.105(s,1H),6.96(1H,−NH),3.69−3.83(m,6H),3.61(t,J=5.45,2H),3.45−3.50(m,2H),3.44(s,3H),3.32(s,3H),2.74(s,3H),1.93−2.04(m,4H),1.30(t,J=7.2,3H)
II.1 ポリエステルの染色
製造例I.1で製造した式(101)で表される染料15重量部を、市販の分散剤4.4部と共に合計100部の水性分散液中で粉砕した。この配合物を使用して、135℃の
高温吸尽法により、織られたポリエステル上に1%の染色(染料および基材に基づく)が生成された。
式(101)で表される染料の代わりに式(102)で表される染料を用いて、適用例II.1を繰り返した。試験結果:染色物の耐光堅牢性はAATCC 61試験およびISO 105試験の結果と同様に優れていた。
Claims (8)
- 少なくとも1種の請求項1に記載の式(1)で表されるアゾ染料および少なくとも1種のさらなる分散染料を含む、二色性または三色性の染料混合物。
- 半合成のまたは合成の疎水性繊維材料を染色または捺染する方法であって、請求項1に記載の式(1)で表される染料を前記材料に塗布するかまたは前記材料中に混和することを含む方法。
- 半合成または合成の疎水性繊維材料の染色または捺染における請求項1に記載の式(1)で表される染料の使用。
- 織物材料の染色または捺染における請求項1に記載の式(1)で表される染料の使用。
- 請求項3に記載の方法により染色または捺染された半合成の疎水性繊維材料。
- 請求項3に記載の方法により染色または捺染された合成の疎水性繊維材料。
- 請求項3に記載の方法により染色または捺染された織物材料。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP16171373 | 2016-05-25 | ||
EP16171373.0 | 2016-05-25 | ||
PCT/EP2016/081232 WO2017202480A1 (en) | 2016-05-25 | 2016-12-15 | Disperse azo dyes, a process for the preparation thereof and the use thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2019521195A JP2019521195A (ja) | 2019-07-25 |
JP6947750B2 true JP6947750B2 (ja) | 2021-10-13 |
Family
ID=56080366
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2018554387A Active JP6947750B2 (ja) | 2016-05-25 | 2016-12-15 | 分散アゾ染料、その製造方法及びその使用 |
Country Status (10)
Country | Link |
---|---|
US (1) | US10934435B2 (ja) |
EP (1) | EP3464475B1 (ja) |
JP (1) | JP6947750B2 (ja) |
KR (1) | KR20190013893A (ja) |
CN (1) | CN109312168A (ja) |
BR (1) | BR112018068579B8 (ja) |
ES (1) | ES2930020T3 (ja) |
PT (1) | PT3464475T (ja) |
TW (1) | TWI707002B (ja) |
WO (1) | WO2017202480A1 (ja) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP4143266B1 (en) * | 2021-07-13 | 2023-11-01 | Sun Chemical Corporation | Stable inkjet dispersions and inks |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2260827C3 (de) | 1972-12-13 | 1980-11-13 | Basf Ag, 6700 Ludwigshafen | 2,6-Diaminopyridine, Verfahren zu ihrer Herstellung und ihre Verwendung als Kupplungskomponenten für Azofarbstoffe |
DE2263458A1 (de) * | 1972-12-27 | 1974-07-04 | Basf Ag | 2,6-diaminopyridin-farbstoffe |
US4012372A (en) | 1973-07-02 | 1977-03-15 | Eastman Kodak Company | Phthalimidyl-azo-tetrahydro-quinoline compounds |
US3980634A (en) | 1973-07-02 | 1976-09-14 | Eastman Kodak Company | Phthalimidyl-azo aniline type compounds and polyester fibers dyed therewith |
US3878189A (en) | 1973-07-02 | 1975-04-15 | Eastman Kodak Co | Azo dye compounds from amino-1,2-benzisothiazolon-1,1-dioxides |
AT373930B (de) * | 1975-10-29 | 1984-03-12 | Basf Ag | Farbstoffzubereitungen fuer das faerben und bedrucken von cellulose und cellulosehaltigem textilmaterial |
DE19623411A1 (de) * | 1996-06-12 | 1997-12-18 | Basf Ag | Farbstoffmischungen |
TWI243192B (en) | 1998-12-31 | 2005-11-11 | Ciba Sc Holding Ag | Phthalimidyl azo pigments, method for producing same and utilization thereof |
PT1358274E (pt) | 2001-02-07 | 2011-04-05 | Huntsman Adv Mat Switzerland | Corante à base de ftalimidilo azo, processo para a sua preparação e uso do mesmo |
DE10244998A1 (de) * | 2002-09-26 | 2004-04-01 | Basf Ag | Vorbehandlungsflotte zur Vorbereitung von textilen Substraten für den Ink-Jet-Druck |
AU2003276247A1 (en) * | 2002-11-11 | 2004-06-03 | Ciba Specialty Chemicals Holding Inc. | Phthalimidyl-azo dyes, process for their preparation and their use |
JP2006510772A (ja) * | 2002-12-19 | 2006-03-30 | チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド | フタルイミジルアゾ染料、その製造方法、およびその使用 |
JP2004209771A (ja) * | 2002-12-27 | 2004-07-29 | Fuji Photo Film Co Ltd | 光情報記録媒体 |
EP1664420A2 (en) * | 2003-09-08 | 2006-06-07 | Ciba SC Holding AG | Process for printing or dyeing cellulose/polyester mixed fibres |
CA2589737A1 (en) * | 2004-12-13 | 2006-06-22 | Nippon Kayaku Kabushiki Kaisha | Novel azo compound or salt, ink composition containing such azo compound, and colored material |
EP1974006A1 (en) | 2006-01-18 | 2008-10-01 | Ciba Specialty Chemicals Holding Inc. | Process for the treatment of fiber materials |
EP2337820B1 (en) * | 2008-10-21 | 2013-05-15 | Huntsman Advanced Materials (Switzerland) GmbH | Azo dyes, a process for the preparation thereof and the use thereof |
JP2010209202A (ja) * | 2009-03-10 | 2010-09-24 | Fujifilm Corp | インク組成物及びインクジェット記録方法 |
PT2513229E (pt) * | 2009-12-16 | 2014-07-14 | Huntsman Adv Mat Switzerland | Corantes azo dispersos, um processo para o seu fabrico e o seu uso |
DK2655518T3 (da) * | 2010-12-20 | 2016-03-14 | Huntsman Adv Mat Switzerland | Dispersions-azo-farvestoffer |
KR102146686B1 (ko) * | 2012-07-27 | 2020-08-24 | 훈츠만 어드밴스트 머티리얼스(스위처랜드) 게엠베하 | 분산 아조 염료, 이의 제조방법 및 이의 용도 |
US9574617B2 (en) | 2014-07-25 | 2017-02-21 | Dana Automotive Systems Group, Llc | Constant velocity joint boot assembly |
-
2016
- 2016-12-02 TW TW105139863A patent/TWI707002B/zh active
- 2016-12-15 EP EP16809445.6A patent/EP3464475B1/en active Active
- 2016-12-15 KR KR1020187037400A patent/KR20190013893A/ko not_active Application Discontinuation
- 2016-12-15 PT PT168094456T patent/PT3464475T/pt unknown
- 2016-12-15 ES ES16809445T patent/ES2930020T3/es active Active
- 2016-12-15 BR BR112018068579A patent/BR112018068579B8/pt active IP Right Grant
- 2016-12-15 CN CN201680086056.0A patent/CN109312168A/zh active Pending
- 2016-12-15 US US16/197,603 patent/US10934435B2/en active Active
- 2016-12-15 WO PCT/EP2016/081232 patent/WO2017202480A1/en unknown
- 2016-12-15 JP JP2018554387A patent/JP6947750B2/ja active Active
Also Published As
Publication number | Publication date |
---|---|
BR112018068579B8 (pt) | 2023-05-16 |
EP3464475A1 (en) | 2019-04-10 |
CN109312168A (zh) | 2019-02-05 |
US10934435B2 (en) | 2021-03-02 |
US20190153230A1 (en) | 2019-05-23 |
TWI707002B (zh) | 2020-10-11 |
BR112018068579A2 (pt) | 2019-02-12 |
WO2017202480A1 (en) | 2017-11-30 |
KR20190013893A (ko) | 2019-02-11 |
BR112018068579B1 (pt) | 2022-10-04 |
JP2019521195A (ja) | 2019-07-25 |
EP3464475B1 (en) | 2022-08-17 |
TW201741401A (zh) | 2017-12-01 |
PT3464475T (pt) | 2022-11-22 |
ES2930020T3 (es) | 2022-12-05 |
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