JP6732443B2 - 染毛化粧料 - Google Patents
染毛化粧料 Download PDFInfo
- Publication number
- JP6732443B2 JP6732443B2 JP2015245337A JP2015245337A JP6732443B2 JP 6732443 B2 JP6732443 B2 JP 6732443B2 JP 2015245337 A JP2015245337 A JP 2015245337A JP 2015245337 A JP2015245337 A JP 2015245337A JP 6732443 B2 JP6732443 B2 JP 6732443B2
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- Prior art keywords
- agent
- hair
- dye
- acid
- examples
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000118 hair dye Substances 0.000 title claims description 51
- 239000002537 cosmetic Substances 0.000 title claims description 38
- 239000003795 chemical substances by application Substances 0.000 claims description 175
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 claims description 57
- 238000004043 dyeing Methods 0.000 claims description 47
- 239000000975 dye Substances 0.000 claims description 45
- 235000004515 gallic acid Nutrition 0.000 claims description 29
- 229940074391 gallic acid Drugs 0.000 claims description 28
- TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 claims description 19
- 239000001263 FEMA 3042 Substances 0.000 claims description 19
- LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 claims description 19
- LRBQNJMCXXYXIU-QWKBTXIPSA-N gallotannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@H]2[C@@H]([C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-QWKBTXIPSA-N 0.000 claims description 19
- 229940033123 tannic acid Drugs 0.000 claims description 19
- 235000015523 tannic acid Nutrition 0.000 claims description 19
- 229920002258 tannic acid Polymers 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 12
- 150000002505 iron Chemical class 0.000 claims description 11
- HSDSBIUUVWRHTM-UHFFFAOYSA-N 4-(2-nitroanilino)phenol Chemical compound C1=CC(O)=CC=C1NC1=CC=CC=C1[N+]([O-])=O HSDSBIUUVWRHTM-UHFFFAOYSA-N 0.000 claims description 4
- TWLMSPNQBKSXOP-UHFFFAOYSA-N 6358-09-4 Chemical compound NC1=CC([N+]([O-])=O)=CC(Cl)=C1O TWLMSPNQBKSXOP-UHFFFAOYSA-N 0.000 claims description 4
- PNENOUKIPPERMY-UHFFFAOYSA-N HC Yellow No. 4 Chemical compound OCCNC1=CC=C([N+]([O-])=O)C=C1OCCO PNENOUKIPPERMY-UHFFFAOYSA-N 0.000 claims description 4
- NJZCRXQWPNNJNB-UHFFFAOYSA-N 2-[2-nitro-4-(trifluoromethyl)anilino]ethanol Chemical compound OCCNC1=CC=C(C(F)(F)F)C=C1[N+]([O-])=O NJZCRXQWPNNJNB-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 description 56
- 238000009472 formulation Methods 0.000 description 40
- 230000000694 effects Effects 0.000 description 34
- -1 alkali metal salts Chemical class 0.000 description 19
- 239000003921 oil Substances 0.000 description 18
- 235000019198 oils Nutrition 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 230000001590 oxidative effect Effects 0.000 description 11
- 238000002360 preparation method Methods 0.000 description 11
- 238000011156 evaluation Methods 0.000 description 10
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 10
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 239000000284 extract Substances 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- 230000002087 whitening effect Effects 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 6
- 150000002894 organic compounds Chemical class 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 5
- 239000003963 antioxidant agent Substances 0.000 description 5
- 235000006708 antioxidants Nutrition 0.000 description 5
- 229960002089 ferrous chloride Drugs 0.000 description 5
- 239000011790 ferrous sulphate Substances 0.000 description 5
- 235000003891 ferrous sulphate Nutrition 0.000 description 5
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 150000002430 hydrocarbons Chemical class 0.000 description 5
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 5
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 5
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 5
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 4
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 4
- 125000005907 alkyl ester group Chemical group 0.000 description 4
- 239000001099 ammonium carbonate Substances 0.000 description 4
- 239000004202 carbamide Substances 0.000 description 4
- 229940082500 cetostearyl alcohol Drugs 0.000 description 4
- 239000006071 cream Substances 0.000 description 4
- 239000002552 dosage form Substances 0.000 description 4
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000002736 nonionic surfactant Substances 0.000 description 4
- 239000000419 plant extract Substances 0.000 description 4
- 229960004889 salicylic acid Drugs 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 4
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 3
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
- 206010020751 Hypersensitivity Diseases 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000006096 absorbing agent Substances 0.000 description 3
- MCDLETWIOVSGJT-UHFFFAOYSA-N acetic acid;iron Chemical compound [Fe].CC(O)=O.CC(O)=O MCDLETWIOVSGJT-UHFFFAOYSA-N 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 150000005215 alkyl ethers Chemical class 0.000 description 3
- 208000030961 allergic reaction Diseases 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 3
- 235000010323 ascorbic acid Nutrition 0.000 description 3
- 229960005070 ascorbic acid Drugs 0.000 description 3
- 239000011668 ascorbic acid Substances 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 239000010696 ester oil Substances 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 159000000014 iron salts Chemical class 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- 239000002562 thickening agent Substances 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- 239000008158 vegetable oil Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000000080 wetting agent Substances 0.000 description 3
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 description 2
- 229940058015 1,3-butylene glycol Drugs 0.000 description 2
- LEEDMQGKBNGPDN-UHFFFAOYSA-N 2-methylnonadecane Chemical compound CCCCCCCCCCCCCCCCCC(C)C LEEDMQGKBNGPDN-UHFFFAOYSA-N 0.000 description 2
- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 description 2
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- PMVSDNDAUGGCCE-TYYBGVCCSA-L Ferrous fumarate Chemical class [Fe+2].[O-]C(=O)\C=C\C([O-])=O PMVSDNDAUGGCCE-TYYBGVCCSA-L 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 2
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 244000305267 Quercus macrolepis Species 0.000 description 2
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 description 2
- 239000002280 amphoteric surfactant Substances 0.000 description 2
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- 239000003242 anti bacterial agent Substances 0.000 description 2
- 239000004599 antimicrobial Substances 0.000 description 2
- 239000000981 basic dye Substances 0.000 description 2
- FUWUEFKEXZQKKA-UHFFFAOYSA-N beta-thujaplicin Chemical compound CC(C)C=1C=CC=C(O)C(=O)C=1 FUWUEFKEXZQKKA-UHFFFAOYSA-N 0.000 description 2
- 235000019437 butane-1,3-diol Nutrition 0.000 description 2
- 239000004106 carminic acid Substances 0.000 description 2
- 235000012730 carminic acid Nutrition 0.000 description 2
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 2
- 239000003093 cationic surfactant Substances 0.000 description 2
- 229960000541 cetyl alcohol Drugs 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
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- VFLDPWHFBUODDF-FCXRPNKRSA-N curcumin Chemical compound C1=C(O)C(OC)=CC(\C=C\C(=O)CC(=O)\C=C\C=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-FCXRPNKRSA-N 0.000 description 2
- PGRHXDWITVMQBC-UHFFFAOYSA-N dehydroacetic acid Chemical compound CC(=O)C1C(=O)OC(C)=CC1=O PGRHXDWITVMQBC-UHFFFAOYSA-N 0.000 description 2
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 2
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- VFPFQHQNJCMNBZ-UHFFFAOYSA-N ethyl gallate Chemical compound CCOC(=O)C1=CC(O)=C(O)C(O)=C1 VFPFQHQNJCMNBZ-UHFFFAOYSA-N 0.000 description 2
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 2
- 229940093915 gynecological organic acid Drugs 0.000 description 2
- 230000037308 hair color Effects 0.000 description 2
- HLUCICHZHWJHLL-UHFFFAOYSA-N hematein Chemical compound C12=CC=C(O)C(O)=C2OCC2(O)C1=C1C=C(O)C(=O)C=C1C2 HLUCICHZHWJHLL-UHFFFAOYSA-N 0.000 description 2
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 2
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 description 2
- 229910000360 iron(III) sulfate Inorganic materials 0.000 description 2
- 229940057995 liquid paraffin Drugs 0.000 description 2
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 2
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- ZQBAKBUEJOMQEX-UHFFFAOYSA-N phenyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OC1=CC=CC=C1 ZQBAKBUEJOMQEX-UHFFFAOYSA-N 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
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- 102000004169 proteins and genes Human genes 0.000 description 2
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- ZEARLPPIUCBHRP-UHFFFAOYSA-N 2-[4-chloro-5-(2-hydroxyethylamino)-2-nitroanilino]ethanol Chemical compound OCCNC1=CC(NCCO)=C([N+]([O-])=O)C=C1Cl ZEARLPPIUCBHRP-UHFFFAOYSA-N 0.000 description 1
- UIVPNOBLHXUKDX-UHFFFAOYSA-N 3,5,5-trimethylhexyl 3,5,5-trimethylhexanoate Chemical compound CC(C)(C)CC(C)CCOC(=O)CC(C)CC(C)(C)C UIVPNOBLHXUKDX-UHFFFAOYSA-N 0.000 description 1
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Description
[1]少なくとも第1剤、第2剤および第3剤を含んで構成される染毛化粧料であって、
前記第1剤は、没食子酸、タンニン酸およびそれらの誘導体からなる群から選択される少なくとも1種を含み、
前記第2剤は鉄塩を含み、
前記第3剤はHC染料を含み、
第3剤が第1剤および第2剤の後に毛髪へ塗布される、染毛化粧料。
[2]前記HC染料は、黄色系HC染料および/またはオレンジ系HC染料を含む、前記[1]に記載の染毛化粧料。
[3]前記第1剤と前記第2剤をこの順にまたは同時に毛髪へ塗布した後、第1剤および第2剤を洗浄し、次いで前記第3剤を塗布することを含む、前記[1]または[2]に記載の染毛化粧料を用いる染毛方法。
本発明の染毛化粧料は、初めに、没食子酸、タンニン酸またはそれらの誘導体を含む第1剤と、鉄塩を含む第2剤を毛髪に塗布し、その後HC染料を含む第3剤を塗布することにより、高い染毛効果および白髪かくし効果を示すとともに、染毛後の毛髪に青みを抑えた自然な色調を与えることができる。第1剤および第2剤を毛髪に塗布する方法としては、例えば、(i)初めに第1剤を毛髪に塗布し、一定時間放置した後、第1剤を洗い流すことなく第2剤を塗布し、さらに一定時間放置する方法、(ii)第1剤および第2剤を同時に毛髪に塗布し、一定時間放置する方法、および、(iii)第1剤および第2剤を混合して得た組成物を毛髪に塗布し、一定時間放置する方法などが挙げられる。染毛効果の観点からは、第1剤および第2剤を毛髪に塗布する方法としては前記(i)の方法が好ましい。
表1に示す組成に従い、以下のようにして、処方例1〜4の製剤を調製した。
油相成分として、流動パラフィン、セトステアリルアルコールおよびポリオキシエチレンセトステアリルエーテル30EOを混合し、十分に加熱溶解させた。水相成分として、水酸化カリウムおよび炭酸水素アンモニウムを除く油相成分以外の成分を混合し、十分に加熱溶解させた。次いで、撹拌しながら加熱溶解した油相成分に水相成分を加えて乳化した。得られた乳化物を冷却し、pHを8とする量の水酸化カリウム、および水に溶解させた炭酸水素アンモニウムを添加して、処方例1〜4の各製剤を得た。
表2に示す処方に従い、以下のようにして、処方例I〜IVの製剤を調製した。
(1)処方例IおよびIIの製剤の調製
水相成分として、常温の精製水に、硫酸第一鉄または塩化第一鉄を加え、さらに、アスコルビン酸を加えて混合した。油相成分として、セトステアリルアルコールおよびポリオキシエチレンセトステアリルエーテル30EOを混合し、十分に加熱溶解させた。次いで、撹拌しながら油相成分に水相成分を加えて乳化し、処方例IおよびIIの製剤を得た。得られた各製剤のpHは、それぞれ3程度であった。
常温の精製水に、硫酸第一鉄または塩化第一鉄を加え、さらに、アスコルビン酸を加えて撹拌溶解し、処方例IIIおよびIVの製剤を得た。得られた各製剤のpHは、それぞれ3程度であった。
表3および4に示す処方に従い、以下のようにして、処方例a〜oの製剤を調製した。
油相成分として、ステアラミドプロピルジメチルアミン、イソノナン酸イソノニル、ベヘントリモニウムクロリド、セトステアリルアルコール、およびセチルアルコールを混合し、十分に加熱溶解させた。前記油相成分以外の成分を水相成分として混合し、十分に加熱溶解させた。次いで、撹拌しながら加熱溶解した油相成分に水相成分を加えて乳化した。得られた乳化物を冷却して、処方例a〜oの各製剤を得た。得られた各製剤のpHは、それぞれ3程度であった。
表5に示す染毛化粧料の処方に従い、前記処方例1〜4、I〜IVおよびa〜oの製剤の組み合わせを変えた、実施例1〜19および比較例1〜4の染毛化粧料について、以下の方法に従い、染毛効果、白髪かくし効果および染毛後の色調を評価した。
(i)実施例1〜19ならびに比較例1および2
シャンプーおよびリンス処理した毛束1g(白髪率100%)に、表5に示す染毛化粧料の処方に従い、第1剤を2g塗布し、30℃、相対湿度65%下で15分間放置した。次いで、第2剤を2g塗布し、再度30℃、相対湿度65%下で15分間放置した。その後、毛束を流水で洗浄し、ドライヤーで乾燥させた。その後、第3剤を3g塗布し、30℃、相対湿度65%下で5分間放置後、流水で洗浄し、ドライヤーで乾燥させた。
シャンプーおよびリンス処理した毛束1g(白髪率100%)に、表5に示す染毛化粧料の処方に従い、第1剤目として処方例aまたはeの製剤を2g塗布し、5分放置後、流水で洗浄し、ドライヤーで乾燥させた。その後、第2剤目として処方例1の製剤を2g塗布し、30℃、相対湿度65%下で15分間放置した。次いで、第3剤目として処方例Iの製剤を2g塗布し、再度30℃、相対湿度65%下で15分間放置した。その後、毛束を流水で洗浄し、ドライヤーで乾燥させた。
以下に示す基準に従い、専門のパネラー5名により肉眼にて染毛効果を評価した。なお、5名のパネラーの評価が2つに分かれた場合は多い方の評価を採用し、3つ以上に分かれた場合は5名の評価が一致するか2つに分かれるまで再度評価を行った。
染毛効果の評価基準
◎:濃く染毛した。
○:はっきりと染毛した。
△:わずかに染毛した。
×:染毛しなかった。
以下に示す基準に従い、専門のパネラー5名により肉眼にて毛髪の色調(特に青みの強さ)を評価した。なお、5名のパネラーの評価が2つ又は3つ以上に分かれた場合には、上記と同様にして評価した。茶味を感じることにより、没食子酸、タンニン酸またはそれらの誘導体と鉄塩との反応により発色される青みを和らげることができるため、見た目に青みを抑えた自然な色調となる。
毛髪の色調の評価基準
◎:茶味を感じる
〇:茶味をやや感じる
△:やや青みが残っている
×:青みが強く残っている
(i)実施例1〜19ならびに比較例1および2
シャンプーおよびリンス処理した毛束2g(白髪率20%)に、表5に示す染毛化粧料の処方に従い、第1剤を4g塗布し、30℃、相対湿度65%下で15分間放置した。次いで、第2剤を4g塗布し、再度30℃、相対湿度65%下で15分間放置した。その後、毛束を流水で洗浄し、ドライヤーで乾燥させた。その後、第3剤を3g塗布し、30℃、相対湿度65%下で5分間放置後、流水で洗浄し、ドライヤーで乾燥させた。
シャンプーおよびリンス処理した毛束2g(白髪率20%)に、表5に示す染毛化粧料の処方に従い、第1剤目として処方例aまたはeの製剤を3g塗布し、5分放置後、流水で洗浄し、ドライヤーで乾燥させた。その後、第2剤目として処方例1の製剤を4g塗布し、30℃、相対湿度65%下で15分間放置した。次いで、第3剤目として処方例Iの製剤を4g塗布し、再度30℃、相対湿度65%下で15分間放置した。その後、毛束を流水で洗浄し、ドライヤーで乾燥させた。
以下に示す基準に従い、専門のパネラー5名により肉眼にて白髪かくし効果を評価した。なお、5名のパネラーの評価が2つ又は3つ以上に分かれた場合には、上記と同様にして評価した。
白髪かくし効果の評価基準
◎:白髪が目立たない
○:白髪がわずかに目立つ
△:白髪が目立つ
×:白髪が染まっていない
Claims (2)
- 少なくとも第1剤、第2剤および第3剤を含んで構成される染毛化粧料であって、
前記第1剤は、没食子酸、タンニン酸およびそれらの誘導体からなる群から選択される少なくとも1種を含み、
前記第2剤は鉄塩を含み、
前記第3剤は、HCイエロー2、HCイエロー4、HCイエロー13、HCオレンジ1および2−アミノ−6−クロロ−4−ニトロフェノールからなる群から選択される少なくとも1種のHC染料を含み、かつ、
HCイエロー4、HCイエロー13および/またはHCオレンジ1を含む場合、その含有量が、第3剤の総量に基づいてそれぞれ0.1〜0.5質量%であり、
HCイエロー2および/または2−アミノ−6−クロロ−4−ニトロフェノールを含む場合、その含有量が、第3剤の総量に基づいてそれぞれ0.05〜0.3質量%であり、
第3剤が第1剤および第2剤の後に毛髪へ塗布される、染毛化粧料。 - 前記第1剤と前記第2剤をこの順にまたは同時に毛髪へ塗布した後、第1剤および第2剤を洗浄し、次いで前記第3剤を塗布することを含む、請求項1に記載の染毛化粧料を用いる染毛方法。
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