JP6393308B2 - ポリアミド製造プロセスにおける抽出水の連続的再循環方法およびその装置 - Google Patents
ポリアミド製造プロセスにおける抽出水の連続的再循環方法およびその装置 Download PDFInfo
- Publication number
- JP6393308B2 JP6393308B2 JP2016504519A JP2016504519A JP6393308B2 JP 6393308 B2 JP6393308 B2 JP 6393308B2 JP 2016504519 A JP2016504519 A JP 2016504519A JP 2016504519 A JP2016504519 A JP 2016504519A JP 6393308 B2 JP6393308 B2 JP 6393308B2
- Authority
- JP
- Japan
- Prior art keywords
- premixer
- stream
- caprolactam
- water
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/46—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13161146.9 | 2013-03-26 | ||
| EP13161146.9A EP2784102B1 (de) | 2013-03-26 | 2013-03-26 | Verfahren und Vorrichtung zur kontinuierlichen Rückführung von Extraktwässern im Polyamidherstellungsprozess |
| PCT/EP2014/051660 WO2014154379A1 (de) | 2013-03-26 | 2014-01-28 | Verfahren und vorrichtung zur kontinuierlichen rückführung von extraktwässern im polyamidherstellungsprozess |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016514741A JP2016514741A (ja) | 2016-05-23 |
| JP2016514741A5 JP2016514741A5 (enExample) | 2018-05-10 |
| JP6393308B2 true JP6393308B2 (ja) | 2018-09-19 |
Family
ID=47913316
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016504519A Expired - Fee Related JP6393308B2 (ja) | 2013-03-26 | 2014-01-28 | ポリアミド製造プロセスにおける抽出水の連続的再循環方法およびその装置 |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP2784102B1 (enExample) |
| JP (1) | JP6393308B2 (enExample) |
| KR (1) | KR102106077B1 (enExample) |
| CN (1) | CN105073831B (enExample) |
| ES (1) | ES2564676T3 (enExample) |
| PL (1) | PL2784102T3 (enExample) |
| SA (1) | SA515361011B1 (enExample) |
| TW (1) | TWI630222B (enExample) |
| WO (1) | WO2014154379A1 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI662065B (zh) * | 2016-11-29 | 2019-06-11 | 德商伍德英汎達 費雪有限責任公司 | 於尼龍-6的生產中回收清洗水萃取物之技術 |
| CN107051345A (zh) * | 2017-01-25 | 2017-08-18 | 江苏永通新材料科技有限公司 | 一种用于生产聚酰胺切片的低聚物分离器 |
| WO2020221920A1 (en) * | 2019-05-01 | 2020-11-05 | Novochem Green Additives 4 B.V. | Recycling eutectic composition |
| CN114426769B (zh) * | 2020-09-22 | 2024-11-05 | 中国石油化工股份有限公司 | 己内酰胺水解开环聚合制备尼龙6过程中回收的己内酰胺及其环状低聚体混合物的应用 |
| CN116888314A (zh) * | 2021-03-16 | 2023-10-13 | 东丽株式会社 | 尼龙6纤维、以及材料再循环聚己酰胺树脂颗粒及其制造方法 |
| JPWO2022196407A1 (enExample) * | 2021-03-16 | 2022-09-22 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2501348C3 (de) | 1975-01-15 | 1988-02-11 | Basf Ag, 6700 Ludwigshafen | Kontinuierliches Verfahren zur Herstellung von Polyamiden aus epsilon-Caprolactam |
| DE3729853A1 (de) | 1987-09-05 | 1989-03-23 | Basf Ag | Verfahren zur aufarbeitung von destillationsrueckstaenden, die bei der reinigung von caprolactam anfallen |
| US5077381A (en) | 1990-06-01 | 1991-12-31 | Basf Corporation | Constant compositioin recycle of nylon 6 polymerization wash water |
| DE4405161A1 (de) * | 1994-02-18 | 1995-08-24 | Huels Chemische Werke Ag | Verfahren zur kontinuierlichen hydrolytischen Polymerisation von Laurinlactam |
| DE19531990A1 (de) | 1995-08-30 | 1997-05-15 | Polymer Eng Gmbh | Verfahren zur kontinuierlichen Herstellung von Polyamid 6 unter Verwendung von Rücklactam |
| DE19752181A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur Herstellung von Polyamiden |
| DE19752183A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur kontinuierlichen Extraktion von Polyamid |
| DE19801267B4 (de) | 1998-01-15 | 2005-03-24 | Inventa-Fischer Gmbh | Verfahren zur Herstellung von PA-6 Granulat und dessen Verwendung |
| NL1010161C2 (nl) * | 1998-09-23 | 2000-03-24 | Dsm Nv | Proces voor de productie van polyamide-6 uitgaande èpsilon-caprolactam. |
| HUP0105495A2 (en) * | 1999-02-11 | 2002-05-29 | Basf Ag | Method for producing polyamide 6 of a low extract content, high viscosity stability and low remonomerization rate |
| DE19925906A1 (de) | 1999-06-07 | 2000-12-14 | Basf Ag | Verfahren zur Herstellung von Polyamiden aus Lactamen und Polyamid-Extrakten |
| DE19962573A1 (de) * | 1999-12-23 | 2001-07-05 | Basf Ag | Verfahren zur Herstellung von Polyamiden |
| US6479620B1 (en) * | 2001-06-01 | 2002-11-12 | E. I. Du Pont De Nemours And Company | Process for converting caprolactam to nylon 6 |
| EP1829594B8 (en) * | 2004-12-15 | 2012-04-18 | Asahi Kasei Chemicals Corporation | Industrial evaporation apparatus |
| CN101437870A (zh) * | 2006-05-04 | 2009-05-20 | Uhde英万达·费希尔公开股份有限公司 | 一种连续生产聚酰胺颗粒的方法 |
| WO2008049786A1 (de) * | 2006-10-24 | 2008-05-02 | Basf Se | Verwendung von wendelrohrverdampfern bei der herstellung von polyamiden |
| ES2632205T3 (es) * | 2008-12-12 | 2017-09-11 | Basf Se | Procedimiento para la fabricación continua de copoliamidas a partir de lactamas y de sales diaminas y ácidos dicarboxílicos |
| PL2532698T3 (pl) * | 2011-06-08 | 2016-12-30 | Sposób i urządzenie do bezpośredniej, ciągłej modyfikacji stopionych polimerów |
-
2013
- 2013-03-26 EP EP13161146.9A patent/EP2784102B1/de active Active
- 2013-03-26 PL PL13161146T patent/PL2784102T3/pl unknown
- 2013-03-26 ES ES13161146.9T patent/ES2564676T3/es active Active
-
2014
- 2014-01-28 CN CN201480018316.1A patent/CN105073831B/zh active Active
- 2014-01-28 KR KR1020157020019A patent/KR102106077B1/ko active Active
- 2014-01-28 JP JP2016504519A patent/JP6393308B2/ja not_active Expired - Fee Related
- 2014-01-28 WO PCT/EP2014/051660 patent/WO2014154379A1/de not_active Ceased
- 2014-02-19 TW TW103105401A patent/TWI630222B/zh active
-
2015
- 2015-09-07 SA SA515361011A patent/SA515361011B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES2564676T3 (es) | 2016-03-28 |
| KR20160010393A (ko) | 2016-01-27 |
| TW201437259A (zh) | 2014-10-01 |
| CN105073831B (zh) | 2017-05-03 |
| SA515361011B1 (ar) | 2017-05-23 |
| EP2784102B1 (de) | 2015-12-09 |
| TWI630222B (zh) | 2018-07-21 |
| CN105073831A (zh) | 2015-11-18 |
| PL2784102T3 (pl) | 2016-06-30 |
| KR102106077B1 (ko) | 2020-05-28 |
| WO2014154379A1 (de) | 2014-10-02 |
| EP2784102A1 (de) | 2014-10-01 |
| JP2016514741A (ja) | 2016-05-23 |
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