JP6345657B2 - 気液分離器 - Google Patents
気液分離器 Download PDFInfo
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- JP6345657B2 JP6345657B2 JP2015522081A JP2015522081A JP6345657B2 JP 6345657 B2 JP6345657 B2 JP 6345657B2 JP 2015522081 A JP2015522081 A JP 2015522081A JP 2015522081 A JP2015522081 A JP 2015522081A JP 6345657 B2 JP6345657 B2 JP 6345657B2
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- 239000007788 liquid Substances 0.000 title claims description 189
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 48
- 238000005192 partition Methods 0.000 claims description 43
- 238000004587 chromatography analysis Methods 0.000 claims description 21
- 238000004808 supercritical fluid chromatography Methods 0.000 claims description 16
- 238000004891 communication Methods 0.000 claims description 12
- 239000012530 fluid Substances 0.000 claims description 12
- 238000011144 upstream manufacturing Methods 0.000 claims description 8
- 238000004128 high performance liquid chromatography Methods 0.000 claims description 7
- 238000004458 analytical method Methods 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000001514 detection method Methods 0.000 claims description 3
- 239000011877 solvent mixture Substances 0.000 claims description 3
- 239000000443 aerosol Substances 0.000 description 68
- 238000000926 separation method Methods 0.000 description 52
- 239000000203 mixture Substances 0.000 description 14
- 239000002904 solvent Substances 0.000 description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 230000004323 axial length Effects 0.000 description 4
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- 230000001133 acceleration Effects 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 238000012864 cross contamination Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000002032 methanolic fraction Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000007373 indentation Methods 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
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- 238000005516 engineering process Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000011044 inertial separation Methods 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D45/00—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
- B01D45/04—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by utilising inertia
- B01D45/08—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by utilising inertia by impingement against baffle separators
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/16—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the fluid carrier
- B01D15/166—Fluid composition conditioning, e.g. gradient
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
- B01D19/0052—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
- B01D19/0057—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused the centrifugal movement being caused by a vortex, e.g. using a cyclone, or by a tangential inlet
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D45/00—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
- B01D45/12—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D45/00—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
- B01D45/12—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces
- B01D45/16—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces generated by the winding course of the gas stream, the centrifugal forces being generated solely or partly by mechanical means, e.g. fixed swirl vanes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/0002—Casings; Housings; Frame constructions
- B01D46/0005—Mounting of filtering elements within casings, housings or frames
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/24—Particle separators, e.g. dust precipitators, using rigid hollow filter bodies
- B01D46/2403—Particle separators, e.g. dust precipitators, using rigid hollow filter bodies characterised by the physical shape or structure of the filtering element
- B01D46/2411—Filter cartridges
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D50/00—Combinations of methods or devices for separating particles from gases or vapours
- B01D50/20—Combinations of devices covered by groups B01D45/00 and B01D46/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04C—APPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
- B04C3/00—Apparatus in which the axial direction of the vortex flow following a screw-thread type line remains unchanged ; Devices in which one of the two discharge ducts returns centrally through the vortex chamber, a reverse-flow vortex being prevented by bulkheads in the central discharge duct
- B04C3/06—Construction of inlets or outlets to the vortex chamber
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04C—APPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
- B04C3/00—Apparatus in which the axial direction of the vortex flow following a screw-thread type line remains unchanged ; Devices in which one of the two discharge ducts returns centrally through the vortex chamber, a reverse-flow vortex being prevented by bulkheads in the central discharge duct
- B04C2003/006—Construction of elements by which the vortex flow is generated or degenerated
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/027—Liquid chromatography
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Physics & Mathematics (AREA)
- Geometry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Separating Particles In Gases By Inertia (AREA)
- Degasification And Air Bubble Elimination (AREA)
Description
12 チャンバ
14 側壁
15 流路
16 偏向器
17 偏向パネル
18 隙間
20 自由縁
22 ベース部分
24 仕切部材
26 貫通口
28 ホルダ
30 入口ダクト
32 入口
34 気体出口ダクト
36 出口
38 液体出口ダクト
40 収集部分
42 ホルダ
44 頭部分
46 底部分
48 蓋
50 封止部
52 封止部
54 封止部
60 入口チャンバ部分
62 流れチャンバ部分
64 収集チャンバ部分
100 クロマトグラフィシステム
102 CO2収納部
104 メタノール収納部
106 調製ステージ
108 調製ステージ
109 プローブ注入器
110 クロマトグラフィカラム
112 UV検出器
114 分光計
116 背圧調節器
118 熱交換器
120 分画器
122 主画分
130 気液分離器
132 入口
134 保護組立体
140 挿入物
142 中間部分
144 窪み
150 気液分離器
152 入口
154 湾曲部分
156 自由端
160 偏向器
161 偏向パネル
162 ベース部分
163 拡張部分
164 円筒部分
165 テーパ付き部分
166 端面
166a 面取り部分
167 内壁部分
168 環状流路
169 自由縁
170 偏向器
171 偏向パネル
172 ベース部分
173 拡張部分
174 円筒部分
175 テーパ付き部分
176 端面
176a 面取り部分
177 内壁部分
178 環状流路
179 自由縁
180 気液分離器
190 気液分離器
Claims (15)
- 軸方向(z)に延び、少なくとも収集チャンバ部分(64)へ延びる流れチャンバ部分(62)を有する円筒形のチャンバ(12)であって、下流の端部である底端部に遠位部分をさらに有し、反対側に位置する近位部分を、上流の端部である上端部に有するチャンバ(12)と、
流れチャンバ部分(62)に配置される偏向器(16;160;170)であって、該偏向器(16;160;170)とチャンバ(12)の側壁(14)との間に狭まる流路(15)を形成するように半径方向外側(r)および軸方向(z)に延び、その遠位端部に自由縁(20;169;179)を有し、閉じた面を備え、貫通口がない偏向パネル(17;161;171)を有する該偏向器と、
偏向パネル(17;161;171)によって遮蔽され、偏向パネル(17;161;171)によって流路(15)から分離され、近位方向において自由縁(20;169;179)から軸方向にオフセットして配置され、偏向パネル(17;161;171)の半径方向内側に面した側壁部分に面した、少なくとも1つの気体出口(36)と
を備える気液分離器であって、
入口ダクト(30)が、軸方向(z)にチャンバ(12)の近位部分に延び、該入口ダクト(30)が、チャンバ(12)の近位部分で複数の入口(32;132;152)に分岐し、該入口(32;132;152)は、チャンバ(12)の側壁部分(14)に向かって半径方向外側に延びており、
チャンバ(12)の遠位部分の液体収集部分(40)が、流体出口ダクト(38)と流体連通している、気液分離器。 - 偏向パネル(17)は実質的に円錐形である、請求項1に記載の気液分離器。
- 偏向パネル(161;171)は、半径方向外側に延びる拡張部分(163;173)、および軸方向に該拡張部分(163;173)に隣接して延びる円筒部分(164;174)を備える、請求項1に記載の気液分離器。
- 偏向パネル(17)の自由縁(20;169;179)は、円筒形のチャンバ(12)
の側壁(14)と共に環状の流れ隙間(18)を形成する、請求項1〜3のいずれか1項に記載の気液分離器。 - 少なくとも1つの気体出口(36)は、軸方向に延びる気体出口ダクト(34)と流体連通する、請求項1〜4のいずれか1項に記載の気液分離器。
- 偏向器(16;160;170)は、カップ形の偏向器(16;160;170)を形成するように偏向パネル(17;161;171)の近位部分と一体形成された、閉じたベース部分(22;162;172)を備える、請求項5に記載の気液分離器。
- 偏向器(16;160;170)は気体出口ダクト(34)の近位端部に配置される、請求項5または6に記載の気液分離器。
- 流れチャンバ部分(62)をその上流に配置された入口チャンバ部分(60)から分離するために、偏向器(16)の上流に配置され、チャンバ(12)の断面全体に延びる仕切部材(24)をさらに備える、請求項1〜7のいずれか1項に記載の気液分離器。
- 仕切部材(24)は、外側の半径方向の縁部に、チャンバ(12)の側壁(14)に隣接する軸方向の通路を形成する少なくとも1つの軸方向の貫通口(26)を備える、請求項8に記載の気液分離器。
- 入口ダクト(30)は、チャンバ(12)の内部で半径方向中央に配置され、さらに入口(32;132;152)の少なくとも1つと流体連通する、請求項1〜9のいずれか1項に記載の気液分離器。
- 少なくとも1つの入口(152)は、流れチャンバ部分(62)へ延び、自由端(156)が近位方向を向いた湾曲部分(154)を備える、請求項1〜7のいずれか1項に記載の気液分離器。
- 少なくとも1つの入口(152)は、入口チャンバ部分(60)へ延び、自由端(156)が近位方向を向いた湾曲部分(154)を備える、請求項8〜10のいずれか1項に記載の気液分離器。
- 少なくとも1つの溶媒混合物を収納および/または調製するための少なくとも1つのリザーバ(102、104)と、
クロマトグラフィカラム(110)と、
少なくとも1つの検出または分析ユニット(112、114)と、
請求項1〜12のいずれか1項に記載の少なくとも1つの気液分離器(10;130;150;180;190)と
を備えるクロマトグラフィシステム。 - 気液分離器(10;130;150;180;190)がCO2およびメタノールを分
離するように動作可能である、超臨界流体クロマトグラフィ(SFC)装置として設計される請求項13に記載のクロマトグラフィシステム。 - 少なくとも高速液体クロマトグラフィ(HPLC)型クロマトグラフィシステムの気液分離器に取って代わるように構成された請求項1〜12のいずれか1項に記載の気液分離器(10;130;150;180;190)を備える、HPLC型クロマトグラフィシステムをSFC型クロマトグラフィシステムに転換する転換キット。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP12176869 | 2012-07-18 | ||
EP12176869.1 | 2012-07-18 | ||
PCT/EP2013/065067 WO2014012962A1 (en) | 2012-07-18 | 2013-07-17 | Gas-liquid separator |
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JP2018097528A Division JP6805420B2 (ja) | 2012-07-18 | 2018-05-22 | 気液分離器 |
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Publication Number | Publication Date |
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JP2015527929A JP2015527929A (ja) | 2015-09-24 |
JP6345657B2 true JP6345657B2 (ja) | 2018-06-20 |
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JP2015522081A Active JP6345657B2 (ja) | 2012-07-18 | 2013-07-17 | 気液分離器 |
JP2018097528A Active JP6805420B2 (ja) | 2012-07-18 | 2018-05-22 | 気液分離器 |
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US (2) | US9649576B2 (ja) |
EP (2) | EP2874725B1 (ja) |
JP (2) | JP6345657B2 (ja) |
CN (2) | CN104470609B (ja) |
DK (1) | DK2874725T3 (ja) |
HK (1) | HK1206669A1 (ja) |
TR (1) | TR201802216T4 (ja) |
WO (1) | WO2014012962A1 (ja) |
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2013
- 2013-07-17 JP JP2015522081A patent/JP6345657B2/ja active Active
- 2013-07-17 US US14/414,740 patent/US9649576B2/en active Active
- 2013-07-17 WO PCT/EP2013/065067 patent/WO2014012962A1/en active Application Filing
- 2013-07-17 EP EP13737273.6A patent/EP2874725B1/en active Active
- 2013-07-17 EP EP17195609.7A patent/EP3290095B1/en active Active
- 2013-07-17 TR TR2018/02216T patent/TR201802216T4/tr unknown
- 2013-07-17 DK DK13737273.6T patent/DK2874725T3/en active
- 2013-07-17 CN CN201380037705.4A patent/CN104470609B/zh active Active
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CN104470609B (zh) | 2017-11-03 |
TR201802216T4 (tr) | 2018-03-21 |
EP3290095A1 (en) | 2018-03-07 |
CN107694217A (zh) | 2018-02-16 |
EP3290095B1 (en) | 2020-05-06 |
HK1206669A1 (en) | 2016-01-15 |
CN104470609A (zh) | 2015-03-25 |
US9649576B2 (en) | 2017-05-16 |
US20170225108A1 (en) | 2017-08-10 |
JP6805420B2 (ja) | 2020-12-23 |
US20150174508A1 (en) | 2015-06-25 |
EP2874725A1 (en) | 2015-05-27 |
CN107694217B (zh) | 2020-11-27 |
DK2874725T3 (en) | 2018-02-26 |
WO2014012962A1 (en) | 2014-01-23 |
JP2015527929A (ja) | 2015-09-24 |
JP2018149541A (ja) | 2018-09-27 |
EP2874725B1 (en) | 2017-11-22 |
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