JP6276265B2 - 固体照明に対する高安定なqd複合体及び開始剤のない重合を介したその作製方法 - Google Patents
固体照明に対する高安定なqd複合体及び開始剤のない重合を介したその作製方法 Download PDFInfo
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- JP6276265B2 JP6276265B2 JP2015525964A JP2015525964A JP6276265B2 JP 6276265 B2 JP6276265 B2 JP 6276265B2 JP 2015525964 A JP2015525964 A JP 2015525964A JP 2015525964 A JP2015525964 A JP 2015525964A JP 6276265 B2 JP6276265 B2 JP 6276265B2
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- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical group [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- YRHRIQCWCFGUEQ-UHFFFAOYSA-N thioxanthen-9-one Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3SC2=C1 YRHRIQCWCFGUEQ-UHFFFAOYSA-N 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
- WTKVMIIQXATOJO-UHFFFAOYSA-N trimethyl-(1,1,2,2-tetraphenyl-2-trimethylsilyloxyethoxy)silane Chemical compound C=1C=CC=CC=1C(C(O[Si](C)(C)C)(C=1C=CC=CC=1)C=1C=CC=CC=1)(O[Si](C)(C)C)C1=CC=CC=C1 WTKVMIIQXATOJO-UHFFFAOYSA-N 0.000 description 1
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 238000001429 visible spectrum Methods 0.000 description 1
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Description
−光源の光を生じるように構成される光源、
−光源の光の少なくとも一部を可視のコンバータの光に変えるように構成される光コンバータ、
を含む照明装置(「装置」)であって、光コンバータは、光コンバータナノ粒子が埋め込まれたポリマー母材を含み、ポリマー母材は、ラジカル(光開始剤)重合可能モノマーに基づき、さらに、ポリマー母材は、ポリマー母材の全重量に対して0ppmを超え且つ5ppm以下のラジカル開始剤に基づく材料を含有する、照明装置を提供する。特に、光コンバータは、カプセル化によって囲まれ、カプセル化は、O2への光コンバータの曝露を減らすように構成される。光コンバータとカプセル化との組み合わせは、光コンバータユニットとしても本明細書において示される。
(Y−)k−n−(X)−(−L)n
を有することができ、ここでkは、2、3、4又は5であり、さらにnは、k−nがゼロ以上であるように1、2、3、4又は5であり;Xは、O、OS、O−Se、O−N、O−P、O−As、S、S=0、S02、Se、Se=0、N、N=0、P、P=0、C=0、As又はAs=0であり;Y及びLのそれぞれは、独立して、H、OH、アリール、ヘテロアリール、又は、少なくとも1つの二重結合、少なくとも1つの三重結合若しくは少なくとも1つの二重結合及び三重結合を任意で含有するC2〜18炭化水素の直鎖若しくは枝分れ鎖である。炭化水素鎖は、任意で、1つ又は複数のC1〜4アルキル、C2〜4アルケニル、C2〜4アルキニル、C1〜4アルコキシ、ヒドロキシル、ハロ、アミノ、ニトロ、シアノ、C3〜5シクロアルキル、3〜5員ヘテロシクロアルキル、アリール、ヘテロアリール、C1〜4アルキルカルボニルオキシ、C1〜4アルキルオキシカルボニル、C1〜4アルキルカルボニル又はホルミルと置換することができる。炭化水素鎖は、任意で、−0−、−S−、−N(Ra)−、−N(Ra)−C(0)−0−、−0−C(0)−N(Ra)−、−N(Ra)−C(0)−N(Rb)−、−O−C(0)−0−、−P(Ra)−又は−P(0)(Ra)−によって分断することもできる。Ra及びRbのそれぞれは、独立して、水素、アルキル、アルケニル、アルキニル、アルコキシ、ヒドロキシルアルキル、ヒドロキシル又はハロアルキルである。アリール基は、置換又は未置換の環式芳香族基である。例として、フェニル、ベンジル、ナフチル、トリル、アントラシル、ニトロフェニル又はハロフェニルが挙げられる。ヘテロアリール基は、例えば、フリル、ピリジル、ピロリル、フェナントリル等、環において1つ又は複数のヘテロ原子を有したアリール基である。
− ラジカル重合可能モノマー、光コンバータナノ粒子、及び、任意でラジカル開始剤を含む混合物(「1つの開始混合物」又は「複数の開始材料」)を提供するステップ、
− 低酸素条件下、好ましくは、不活性雰囲気下で、ラジカル重合可能モノマーを重合させ、その結果、光コンバータナノ粒子が埋め込まれたポリマー母材を提供するステップであり、ポリマー母材の全重量に対して0ppmを超え且つ5ppm以下のラジカル開始剤が適用される、ステップ、
を含む。
複数の系を、異なる条件下で作製した。ここで、1つの実施例が以下に与えられる。
Claims (14)
- − 光源の光を生じるように構成される光源、
− 前記光源の光の少なくとも一部を可視のコンバータの光に変えるように構成される光コンバータ、
を含む照明装置であって、
前記光コンバータは、光コンバータナノ粒子が埋め込まれたポリマー母材を含み、前記ポリマー母材はラジカル重合可能モノマーに基づき、前記ポリマー母材は、前記ポリマー母材の全重量に対して0ppmを超え且つ5ppm以下のラジカル開始剤に基づく材料を含有し、さらに、前記光コンバータは、カプセル化によって囲まれ、前記カプセル化は、O2への前記光コンバータの曝露を減らすように構成される、照明装置。 - 前記ポリマー母材は、ポリビニルポリマー、ポリアクリレートポリマー及びチオール−エンポリマーを含む群から選択される、請求項1に記載の照明装置。
- 前記光コンバータは、O2及びH2Oを透過できないカプセル化によって囲まれる、請求項1又は2に記載の照明装置。
- 前記光コンバータナノ粒子は、CdS、CdSe、CdTe、ZnS、ZnSe、ZnTe、HgS、HgSe、HgTe、CdSeS、CdSeTe、CdSTe、ZnSeS、ZnSeTe、ZnSTe、HgSeS、HgSeTe、HgSTe、CdZnS、CdZnSe、CdZnTe、CdHgS、CdHgSe、CdHgTe、HgZnS、HgZnSe、HgZnTe、CdZnSeS、CdZnSeTe、CdZnSTe、CdHgSeS、CdHgSeTe、CdHgSTe、HgZnSeS、HgZnSeTe、HgZnSTe、GaN、GaP、GaAs、AlN、AlP、AlAs、InN、InP、InAs、GaNP、GaNAs、GaPAs、AlNP、AlNAs、AlPAs、InNP、InNAs、InPAs、GaAlNP、GaAlNAs、GaAlPAs、GaInNP、GaInNAs、GaInPAs、InAlNP、InAlNAs及びInAlPAsのナノ粒子を含む群から選択され、さらに、前記光コンバータは、前記光コンバータの全重量に対して0.001〜25wt.%の光コンバータナノ粒子を含む、請求項1乃至3のいずれか一項に記載の照明装置。
- 前記光コンバータナノ粒子は、CdS、CdSe、CdSe/CdS及びCdSe/CdS/ZnSのナノ粒子を含む群から選択される、請求項1乃至4のいずれか一項に記載の照明装置。
- 前記光コンバータナノ粒子は、コア−シェル量子ドット及びdots−in−rodsのナノ粒子のうち1つ又は複数を含む、請求項1乃至5のいずれか一項に記載の照明装置。
- 前記カプセル化は、前記光コンバータを含有する容器及びカバーを含み、前記容器及びカバーは互いに取り付けられ且つ前記光コンバータを囲む、請求項1乃至6のいずれか一項に記載の照明装置。
- バックライティングユニットを含む液晶表示素子であって、前記バックライティングユニットは、請求項1乃至7のいずれか一項に記載の照明装置を1つ又は複数含む、液晶表示素子。
- 請求項1乃至7のいずれか一項に記載の光コンバータ、及び、該光コンバータを囲むカプセル化を含む光コンバータユニットであって、前記カプセル化は、O2への前記光コンバータの曝露を減らすように構成される、光コンバータユニット。
- 光コンバータの生成のための方法であって、前記光コンバータは、光コンバータナノ粒子が埋め込まれたポリマー母材を含み、当該方法は、
− ラジカル重合可能モノマー、光コンバータナノ粒子、及び、任意でラジカル開始剤を含む混合物を提供するステップ、
− 低酸素条件下で、前記ラジカル重合可能モノマーを重合させ、その結果、前記光コンバータナノ粒子が埋め込まれたポリマー母材を提供するステップであり、前記ポリマー母材の全重量に対して0ppmを超え且つ5ppm以下のラジカル開始剤が適用される、ステップ、及び
− そのようにして得られた光コンバータを、カプセル化によって囲むステップ、
を含み、
重合させることは、300〜460nmの範囲の波長を有する放射を用いて前記ラジカル重合可能モノマーを照射することによって開始される、
方法。 - 重合させることは、350〜460nmの範囲の波長を有する放射を用いて前記ラジカル重合可能モノマーを照射することによって開始される、請求項10に記載の方法。
- 前記ラジカル重合可能モノマーは、ビニルモノマー、アクリレートモノマー、及び、チオールとジエンとの組み合わせを含む群から選択され、さらに、前記混合物は、前記混合物の全重量に対して0.001〜25wt.%の光コンバータナノ粒子を含む、請求項10又は11に記載の方法。
- 前記混合物を不活性ガス雰囲気において維持しながら、前記ラジカル重合可能モノマーを重合させるステップを含む、請求項10乃至12のいずれか一項に記載の方法。
- そのようにして得られた光コンバータを、酸素を透過できないカプセル化によって囲むステップをさらに含む、請求項10乃至13のいずれか一項に記載の方法。
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