JP5784634B2 - 金属表面のスケール調整 - Google Patents
金属表面のスケール調整 Download PDFInfo
- Publication number
- JP5784634B2 JP5784634B2 JP2012548143A JP2012548143A JP5784634B2 JP 5784634 B2 JP5784634 B2 JP 5784634B2 JP 2012548143 A JP2012548143 A JP 2012548143A JP 2012548143 A JP2012548143 A JP 2012548143A JP 5784634 B2 JP5784634 B2 JP 5784634B2
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- temperature
- adjustment
- metal object
- metal
- solution
- Prior art date
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- 229910052751 metal Inorganic materials 0.000 title claims description 100
- 239000002184 metal Substances 0.000 title claims description 100
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- 230000003750 conditioning effect Effects 0.000 claims description 58
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- 238000000034 method Methods 0.000 claims description 56
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- 238000012545 processing Methods 0.000 claims description 42
- 230000008569 process Effects 0.000 claims description 38
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 32
- 238000010438 heat treatment Methods 0.000 claims description 32
- 239000007864 aqueous solution Substances 0.000 claims description 29
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- 238000001816 cooling Methods 0.000 claims description 23
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- 239000000463 material Substances 0.000 claims description 18
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- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 21
- 239000011651 chromium Substances 0.000 description 20
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- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 6
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- 239000000376 reactant Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
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- VNNRSPGTAMTISX-UHFFFAOYSA-N chromium nickel Chemical compound [Cr].[Ni] VNNRSPGTAMTISX-UHFFFAOYSA-N 0.000 description 2
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- -1 halide carbonates Chemical class 0.000 description 2
- 238000007726 management method Methods 0.000 description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
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- 239000011733 molybdenum Substances 0.000 description 2
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- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 230000009257 reactivity Effects 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
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- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 description 1
- JYLNVJYYQQXNEK-UHFFFAOYSA-N 3-amino-2-(4-chlorophenyl)-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(CN)C1=CC=C(Cl)C=C1 JYLNVJYYQQXNEK-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910001182 Mo alloy Inorganic materials 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
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- 150000007522 mineralic acids Chemical class 0.000 description 1
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- PXHVJJICTQNCMI-BJUDXGSMSA-N nickel-58 Chemical compound [58Ni] PXHVJJICTQNCMI-BJUDXGSMSA-N 0.000 description 1
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- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 1
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- 235000019795 sodium metasilicate Nutrition 0.000 description 1
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- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
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- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/14—Cleaning or pickling metallic material with solutions or molten salts with alkaline solutions
- C23G1/19—Iron or steel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B1/00—Cleaning by methods involving the use of tools
- B08B1/20—Cleaning of moving articles, e.g. of moving webs or of objects on a conveyor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23B—TURNING; BORING
- B23B45/00—Hand-held or like portable drilling machines, e.g. drill guns; Equipment therefor
- B23B45/06—Hand-held or like portable drilling machines, e.g. drill guns; Equipment therefor driven by man-power
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G3/00—Apparatus for cleaning or pickling metallic material
- C23G3/02—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G3/00—Apparatus for cleaning or pickling metallic material
- C23G3/02—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously
- C23G3/021—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously by dipping
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G3/00—Apparatus for cleaning or pickling metallic material
- C23G3/02—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously
- C23G3/023—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously by spraying
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G3/00—Apparatus for cleaning or pickling metallic material
- C23G3/02—Apparatus for cleaning or pickling metallic material for cleaning wires, strips, filaments continuously
- C23G3/027—Associated apparatus, e.g. for pretreating or after-treating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B45/04—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for de-scaling, e.g. by brushing
- B21B45/06—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for de-scaling, e.g. by brushing of strip material
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Chemical Treatment Of Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29382110P | 2010-01-11 | 2010-01-11 | |
| US61/293,821 | 2010-01-11 | ||
| PCT/US2011/020479 WO2011085172A2 (en) | 2010-01-11 | 2011-01-07 | Metal surface scale conditioning |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013516551A JP2013516551A (ja) | 2013-05-13 |
| JP2013516551A5 JP2013516551A5 (enExample) | 2014-02-27 |
| JP5784634B2 true JP5784634B2 (ja) | 2015-09-24 |
Family
ID=44169987
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012548143A Active JP5784634B2 (ja) | 2010-01-11 | 2011-01-07 | 金属表面のスケール調整 |
Country Status (11)
| Country | Link |
|---|---|
| US (2) | US20130029054A1 (enExample) |
| EP (1) | EP2524062B1 (enExample) |
| JP (1) | JP5784634B2 (enExample) |
| KR (1) | KR101696640B1 (enExample) |
| CN (1) | CN102762771B (enExample) |
| BR (1) | BR112012016999A2 (enExample) |
| CA (1) | CA2786513A1 (enExample) |
| ES (1) | ES2704323T3 (enExample) |
| MX (1) | MX2012008097A (enExample) |
| TW (1) | TWI531683B (enExample) |
| WO (1) | WO2011085172A2 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101696640B1 (ko) | 2010-01-11 | 2017-01-17 | 콜렌코포레이션 | 금속 표면 스케일을 컨디셔닝하는 방법과 그 장치 |
| CN103305745B (zh) * | 2012-03-09 | 2016-04-27 | 宝山钢铁股份有限公司 | 一种高质量硅钢常化基板的生产方法 |
| KR20150054758A (ko) * | 2012-09-10 | 2015-05-20 | 휴렛-팩커드 디벨롭먼트 컴퍼니, 엘.피. | 1차 접속 테이블 및 2차 접속 테이블의 사용 |
| EP2937747A1 (de) * | 2014-04-24 | 2015-10-28 | Siemens Aktiengesellschaft | Auf Modellierung einer Beizlinie beruhende Optimierung einer Sequenz von zu beizenden Bändern |
| KR101589818B1 (ko) | 2014-07-02 | 2016-02-12 | 한국브라스트 주식회사 | 브라스트머신을 이용한 피 가공물의 증착물제거방법 |
| MX2018000797A (es) | 2015-07-22 | 2018-05-15 | Kolene Corp | Proceso de acondicionamiento de escamas para aleaciones de acero al carbono avanzado de alta resistencia. |
| CN105586603B (zh) * | 2015-11-23 | 2018-10-09 | 佛山市高明俊品金属制品有限公司 | 一种不锈钢氧化皮去除方法 |
| KR101859995B1 (ko) * | 2017-06-27 | 2018-05-24 | 에스큐시스템 주식회사 | 슬러지 제거장치 |
| EP3441180A1 (en) * | 2017-08-11 | 2019-02-13 | General Electric Company | Method of repairing superalloys |
| KR102521021B1 (ko) * | 2018-03-08 | 2023-04-12 | 상라오 징코 솔라 테크놀러지 디벨롭먼트 컴퍼니, 리미티드 | 태양 전지 패널용 플럭스 도포 부재 및 방법, 그리고 태양 전지 패널의 인터커넥터 부착 장치 |
| CN110614254B (zh) * | 2019-09-29 | 2021-02-05 | 山东大学 | 一种针对复杂污物的复合清洗方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2717845A (en) * | 1947-01-09 | 1955-09-13 | Roy E Carter | Metal descaling methods |
| US3174491A (en) * | 1963-10-23 | 1965-03-23 | Kolene Corp | Molten salt spray apparatus for descaling stainless steel |
| GB1101273A (en) * | 1964-04-16 | 1968-01-31 | Dynamit Nobel Ag | Improvements in or relating to the descaling of metal surfaces |
| US3260619A (en) | 1965-02-04 | 1966-07-12 | Kolene Corp | Methods and compositions for cleaning metal |
| DE1546113A1 (de) * | 1965-05-12 | 1970-12-17 | Dynamit Nobel Ag | Verfahren zur Verhinderung der Hydridzersetzung von natriumhydridhaltigen Schmelzen |
| JPS5334167B1 (enExample) * | 1968-08-17 | 1978-09-19 | ||
| US3617039A (en) * | 1968-04-26 | 1971-11-02 | Mitsubishi Heavy Ind Ltd | Descaling apparatus for steel |
| JPS5496458A (en) * | 1978-01-18 | 1979-07-30 | Ishikawajima Harima Heavy Ind Co Ltd | Method and apparatus for descaling of steel strip |
| US4317685A (en) * | 1980-06-06 | 1982-03-02 | General Electric Company | Method for removing a scale from a superalloy surface |
| US5221358A (en) * | 1991-08-16 | 1993-06-22 | Kolene Corporation | Descaling/deglassing salt composition and method |
| US5272798A (en) * | 1992-08-05 | 1993-12-28 | Kolene Corporation | Method and apparatus for descaling metal strip |
| ES2098769T3 (es) * | 1992-08-05 | 1997-05-01 | Kolene Corp | Procedimiento y aparato para descascarillar una banda de metal. |
| ATE221570T1 (de) | 1995-09-01 | 2002-08-15 | Procter & Gamble | Waschmittel enthaltend einen ton als flockungspolymer mit einer teilchengrösse von weniger als 250 micrometer |
| US6146692A (en) * | 1998-12-14 | 2000-11-14 | General Electric Company | Caustic process for replacing a thermal barrier coating |
| EP1072695B1 (en) * | 1999-01-26 | 2012-12-19 | Nippon Steel Corporation | Method of removing scales and preventing scale formation on metal material and apparatus therefore |
| US6450183B1 (en) | 1999-12-22 | 2002-09-17 | Kolene Corporation | Composition, apparatus, and method of conditioning scale on a metal surface |
| JP4694048B2 (ja) | 2001-06-15 | 2011-06-01 | 株式会社パーカーコーポレーション | ステンレス鋼の高速デスケーリング処理法 |
| US6776359B2 (en) * | 2001-11-06 | 2004-08-17 | Kolene Corporation | Spray nozzle configuration |
| US6878215B1 (en) * | 2004-05-27 | 2005-04-12 | General Electric Company | Chemical removal of a metal oxide coating from a superalloy article |
| DE102005012296A1 (de) * | 2005-03-17 | 2006-09-21 | Sms Demag Ag | Verfahren und Vorrichtung zum Entzundern eines Metallbandes |
| CN101285196B (zh) * | 2008-05-30 | 2010-10-13 | 重庆钢铁(集团)有限责任公司 | 航空管表面氧化皮处理工艺 |
| KR101696640B1 (ko) | 2010-01-11 | 2017-01-17 | 콜렌코포레이션 | 금속 표면 스케일을 컨디셔닝하는 방법과 그 장치 |
-
2011
- 2011-01-07 KR KR1020127020620A patent/KR101696640B1/ko not_active Expired - Fee Related
- 2011-01-07 ES ES11701570T patent/ES2704323T3/es active Active
- 2011-01-07 CN CN201180009691.6A patent/CN102762771B/zh not_active Expired - Fee Related
- 2011-01-07 BR BR112012016999A patent/BR112012016999A2/pt not_active Application Discontinuation
- 2011-01-07 EP EP11701570.1A patent/EP2524062B1/en not_active Not-in-force
- 2011-01-07 MX MX2012008097A patent/MX2012008097A/es not_active Application Discontinuation
- 2011-01-07 JP JP2012548143A patent/JP5784634B2/ja active Active
- 2011-01-07 WO PCT/US2011/020479 patent/WO2011085172A2/en not_active Ceased
- 2011-01-07 US US13/576,196 patent/US20130029054A1/en not_active Abandoned
- 2011-01-07 CA CA2786513A patent/CA2786513A1/en not_active Abandoned
- 2011-01-11 TW TW100100915A patent/TWI531683B/zh not_active IP Right Cessation
-
2016
- 2016-06-09 US US15/177,524 patent/US10006129B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| BR112012016999A2 (pt) | 2016-04-19 |
| KR20120123673A (ko) | 2012-11-09 |
| EP2524062A2 (en) | 2012-11-21 |
| JP2013516551A (ja) | 2013-05-13 |
| CN102762771B (zh) | 2014-10-01 |
| TWI531683B (zh) | 2016-05-01 |
| US20130029054A1 (en) | 2013-01-31 |
| WO2011085172A2 (en) | 2011-07-14 |
| TW201139743A (en) | 2011-11-16 |
| KR101696640B1 (ko) | 2017-01-17 |
| EP2524062B1 (en) | 2018-11-28 |
| US10006129B2 (en) | 2018-06-26 |
| CA2786513A1 (en) | 2011-07-14 |
| ES2704323T3 (es) | 2019-03-15 |
| MX2012008097A (es) | 2012-07-30 |
| CN102762771A (zh) | 2012-10-31 |
| US20160289847A1 (en) | 2016-10-06 |
| WO2011085172A3 (en) | 2011-09-15 |
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