JP5691634B2 - 有機el表示装置用カラーフィルタ、及びそれを具備する有機el表示装置 - Google Patents
有機el表示装置用カラーフィルタ、及びそれを具備する有機el表示装置 Download PDFInfo
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- JP5691634B2 JP5691634B2 JP2011039434A JP2011039434A JP5691634B2 JP 5691634 B2 JP5691634 B2 JP 5691634B2 JP 2011039434 A JP2011039434 A JP 2011039434A JP 2011039434 A JP2011039434 A JP 2011039434A JP 5691634 B2 JP5691634 B2 JP 5691634B2
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- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 150000001651 triphenylamine derivatives Chemical class 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- UGCDBQWJXSAYIL-UHFFFAOYSA-N vat blue 6 Chemical compound O=C1C2=CC=CC=C2C(=O)C(C=C2Cl)=C1C1=C2NC2=C(C(=O)C=3C(=CC=CC=3)C3=O)C3=CC(Cl)=C2N1 UGCDBQWJXSAYIL-UHFFFAOYSA-N 0.000 description 1
- 239000000984 vat dye Substances 0.000 description 1
- KOTVVDDZWMCZBT-UHFFFAOYSA-N vat violet 1 Chemical compound C1=CC=C[C]2C(=O)C(C=CC3=C4C=C(C=5C=6C(C([C]7C=CC=CC7=5)=O)=CC=C5C4=6)Cl)=C4C3=C5C=C(Cl)C4=C21 KOTVVDDZWMCZBT-UHFFFAOYSA-N 0.000 description 1
- GFFQNEGBFFGLQG-UHFFFAOYSA-N vat yellow 2 Chemical compound S1C2=C3C(=O)C4=CC=C5N=C(C=6C=CC=CC=6)SC5=C4C(=O)C3=CC=C2N=C1C1=CC=CC=C1 GFFQNEGBFFGLQG-UHFFFAOYSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- UKRDPEFKFJNXQM-UHFFFAOYSA-N vinylsilane Chemical class [SiH3]C=C UKRDPEFKFJNXQM-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XOSXWYQMOYSSKB-LDKJGXKFSA-L water blue Chemical compound CC1=CC(/C(\C(C=C2)=CC=C2NC(C=C2)=CC=C2S([O-])(=O)=O)=C(\C=C2)/C=C/C\2=N\C(C=C2)=CC=C2S([O-])(=O)=O)=CC(S(O)(=O)=O)=C1N.[Na+].[Na+] XOSXWYQMOYSSKB-LDKJGXKFSA-L 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 229940074411 xylene Drugs 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- NDKWCCLKSWNDBG-UHFFFAOYSA-N zinc;dioxido(dioxo)chromium Chemical compound [Zn+2].[O-][Cr]([O-])(=O)=O NDKWCCLKSWNDBG-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Optical Filters (AREA)
- Electroluminescent Light Sources (AREA)
- Devices For Indicating Variable Information By Combining Individual Elements (AREA)
Description
前記緑色の画素を形成するために用いる緑色着色組成物が、少なくともC.I.Pigment Green7とC.I.Pigment Blue15:3とC.I.Pigment Yellow 150を含むとともに、
前記緑色の画素が、C光源で計算したCIE1931のXYZ表色系における(x、y)色度座標が(0.17、0.65)、(0.20、0.65)、(0.17、0.70)、(0.20、0.70)の4点に囲まれた範囲に入り、
前記赤色の画素を形成するために用いる赤色着色組成物が、C.I.Pigment Red 254と、C.I.Pigment Red 177を含み、
前記青色の画素を形成するために用いる青色着色組成物が、C.I.Pigment Blue 15:6を含むことを特徴とする有機EL表示装置用カラーフィルタである。
前記有機EL表示装置を点灯したときのNTSC規格の色再現域の包含率が、97.4〜99.9%の範囲に入ることを特徴とする有機EL表示装置である。
ウム赤、群青、紺青、酸化クロム緑、コバルト緑等の金属酸化物粉、金属硫化物粉、金属粉等が挙げられる。無機顔料は、彩度と明度のバランスを取りつつ良好な塗布性、感度、現像性等を確保するために、有機顔料と組み合わせて用いられる。
アンモニア、ナトリウムメチラートのジメチルホルムアミド溶液などの塩基性溶媒などが知られている。
ート、トリプロピレングリコールジ(メタ)アクリレート、トリメチロールプロパントリ(メタ)アクリレート、ペンタエリスリトールトリ(メタ)アクリレート、1,6-ヘキサンジオールジグリシジルエーテルジ(メタ)アクリレート、ビスフェノールAジグリシジルエーテルジ(メタ)アクリレート、ネオペンチルグリコールジグリシジルエーテルジ(メタ)アクリレート、ジペンタエリスリトールヘキサ(メタ)アクリレート、トリシクロデカニル(メタ)アクリレート、エステルアクリレート、メチロール化メラミンの(メタ)アクリル酸エステル、エポキシ(メタ)アクリレート、ウレタンアクリレートなどの各種アクリル酸エステル及びメタクリル酸エステル、(メタ)アクリル酸、スチレン、酢酸ビニル、ヒドロキシエチルビニルエーテル、エチレングリコールジビニルエーテル、ペンタエリスリトールトリビニルエーテル、(メタ)アクリルアミド、N-ヒドロキシメチル(メタ)アクリルアミド、N-ビニルホルムアミド、アクリロニトリルなどが挙げられる。これらは、単独または2種類以上混合して用いることができる。
好適である。より好ましくは5%乃至40%であり、さらに好ましくは10質量%乃至40質量%である。熱硬化性化合物が5質量%未満では熱硬化性化合物の量が少なすぎるため、有機EL表示装置用カラーフィルタ10の製造工程におけるポストベーク工程において十分に着色画素3が十分に硬化しないため、その後の透明導電層27の成膜工程における加熱(スパッタリング中の加熱やその後のアニールのための加熱)の際に着色画素3が熱により収縮し、透明導電層27との間で応力が発生してシワの発生やクラックの発生の原因となる。
コンベクションオーブン、IRオーブン、ホットプレートなどを使用してもよい。必要により乾燥された膜には、この膜と接触あるいは非接触状態で設けられた所定のパターンを有するパターン露光用フォトマスクを介して膜に紫外線露光を行う。
至700nmにおける最大透過率は40%以上であることが好ましい。より好ましくは50%以上であり、さらに好ましくは55%以上である。40%未満では光の利用効率が悪くなり表示装置の輝度が低くなる場合や、利用効率が悪い分、白色有機EL素子の発光を強くする必要があるため、その分、発光素子の寿命が短くなるため都合が悪い。また、この時の波長は500nm乃至550nmの範囲に入ることが好ましく、より好ましくは500nm乃至530nmである。550nm以上では、色味が黄色くなるため、表示装置の色再現域が狭まる。一方、500nm未満では色味が青くなり、輝度が低下する。
色や橙色など、緑色画素3Gと赤色画素3Rを用いて表示される色の再現性が悪化する。一方、xが上述の範囲よりも大きくなる場合、該有機EL表示装置用カラーフィルタ10からなる有機EL表示装置30の緑色表示が黄色味になってしまう上、シアン色のような緑色画素3Gと青色画素3Bを用いて表示される色の再現性が悪化する。yが上述の範囲より小さいと緑色の色再現性が悪化する。
を挙げることができる。
ン誘導体、トリス(8−キノリノール)アルミニウム等の8−キノリノール誘導体の金属錯体、フタロシアニン、金属フタロシアニン、並びにジスチリルピラジン誘導体等を例示することができる。
EL素子20が対向するように配置された態様である。
部、粉砕した食塩1000部、及びジエチレングリコール120部をステンレス製1ガロンニーダー(井上製作所製)に仕込み、60℃で10時間混練した。この混合物を温水2000部に投入し、約80℃に加熱しながらハイスピードミキサーで約1時間攪拌してスラリー状とし、濾過、水洗をくりかえして食塩および溶剤を除いた後、80℃で24時間乾燥し、微細化顔料(R-1)を得た。得られた顔料の平均粒子径は25nmであった。
実施例及び比較例で用いたアクリル樹脂溶液の調製について説明する。樹脂の分子量は、GPC(ゲルパーミエーションクロマトグラフィ)により測定したポリスチレン換算の重量平均分子量である。
保土ヶ谷化学社製「EAB−F」)
<カラーフィルタの作成方法>表3に示した緑レジストG1からG10までの10種類及び赤レジストR1、青レジストB1を用い、実施例1から実施例6までの6種類のカラーフィルタ、比較例1から比較例4までの4種類のカラーフィルタ作製した。まず、赤レジストであるR1として、赤色着色組成物を、硬化後の膜厚が3μmとなるように、スピンコート法によりブラックマトリクス(BM:2)を形成してあるガラス基板1に塗布し、乾燥した後、ネガ像を有するフォトマスクを介して超高圧水銀ランプを用いて紫外線で露光した。その後、23℃の炭酸ナトリウム水溶液を用いてスプレー現像した後、イオン交換水で洗浄し、風乾した。その後、クリーンオーブン中で、200℃で30分のポストベークを行い、赤色着色パターン3(R)を有するガラス基板を得た。その後、
青レジストであるB1として、青色着色組成物を用いて同様に青色着色パターン3(B)を得る。さらにG1からG10の緑色着色組成物を用いて緑色着色パターンを得た。着色材料の組み合わせを表4に示す。
るとはいえない。また、比較例3の表示装置は、カラーフィルタの緑色画素における475nmの透過率が本発明の範囲に入っていない例であり、緑色表示における色度はNTSC規格の緑色の色度からは大きく青色にずれている。比較例4の表示装置はカラーフィルタの緑色画素における595nmの透過率が本発明の範囲に入っていない例であり、緑色表示における色度はNTSC規格の緑色の色度からは大きく黄色にずれている。比較例3及び比較例4の表示装置におけるNTSC規格の色再現域の包含率は96%程度であり、本発明にかかる表示装置と比較するとその色再現性は劣る。
2・・・ブラックマトリクス
3・・・着色画素
3B・・・青色画素
3R・・・赤色画素
3G・・・緑色画素
4・・・陽極
5・・・有機層
6・・・陰極
7・・・保護層
8・・・電源
10・・・有機EL表示装置用カラーフィルタ
11・・・正孔輸送層
12・・・赤色発光層
13・・・発光層
13B・・・青色発光層
13R・・・赤色発光層
13G・・・緑色発光層
14・・・電子輸送層
15・・・接着層
16・・・着色層
17・・・TFT
18・・・平坦化層
20・・・有機EL素子
21・・・背面側電極層
22・・・有機EL層
23・・・発光光
23B・・・青色発光光
23R・・・赤色発光光
23G・・・緑色発光光
24・・・隔壁
25・・・シール剤
26・・・有機EL素子側基板
27・・・透明導電層
30・・・有機EL表示装置
Claims (3)
- 白色発光の有機EL素子と少なくとも赤色、緑色、青色の画素を持つカラーフィルタを組み合わせた有機EL表示装置に用いられるカラーフィルタであって、該カラーフィルタの緑色画素の475nmと595nmにおける透過率が2.0%以下であり、且つ400nm乃至700nmにおける最大透過率が40%以上であり、
前記緑色の画素を形成するために用いる緑色着色組成物が、少なくともC.I.Pigment Green7とC.I.Pigment Blue15:3とC.I.Pigment Yellow 150を含むとともに、
前記緑色の画素が、C光源で計算したCIE1931のXYZ表色系における(x、y)色度座標が(0.17、0.65)、(0.20、0.65)、(0.17、0.70)、(0.20、0.70)の4点に囲まれた範囲に入り、
前記赤色の画素を形成するために用いる赤色着色組成物が、C.I.Pigment Red 254と、C.I.Pigment Red 177を含み、
前記青色の画素を形成するために用いる青色着色組成物が、C.I.Pigment Blue 15:6を含むことを特徴とする有機EL表示装置用カラーフィルタ。 - 前記有機EL素子の発光スペクトルと、前記カラーフィルタの緑色画素の分光透過率スペクトルから算出したCIE1931表色系(XYZ表色系)における色度(x,y)が(0.20,0.65)、(0.22,0.69)、(0.20,0.72)、(0.22,0.72)の4点に囲まれる範囲に入ることを特徴とする請求項1に記載の有機EL表示装置用カラーフィルタ。
- 請求項1又は請求項2に記載の有機EL表示装置用カラーフィルタを具備した有機EL表示装置であって、
前記有機EL表示装置を点灯したときのNTSC規格の色再現域の包含率が、97.4〜99.9%の範囲に入ることを特徴とする有機EL表示装置。
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