JP5662986B2 - 粉末皮膚洗浄料 - Google Patents
粉末皮膚洗浄料 Download PDFInfo
- Publication number
- JP5662986B2 JP5662986B2 JP2012239479A JP2012239479A JP5662986B2 JP 5662986 B2 JP5662986 B2 JP 5662986B2 JP 2012239479 A JP2012239479 A JP 2012239479A JP 2012239479 A JP2012239479 A JP 2012239479A JP 5662986 B2 JP5662986 B2 JP 5662986B2
- Authority
- JP
- Japan
- Prior art keywords
- powder
- fatty acid
- glutamate
- sodium
- skin cleanser
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000843 powder Substances 0.000 title claims description 27
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- 229930195712 glutamate Natural products 0.000 claims description 14
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- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
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- 235000015278 beef Nutrition 0.000 description 1
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- 229910000278 bentonite Inorganic materials 0.000 description 1
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- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 229960003180 glutathione Drugs 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
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- 239000008187 granular material Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
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- 235000010417 guar gum Nutrition 0.000 description 1
- 239000000665 guar gum Substances 0.000 description 1
- 229960002154 guar gum Drugs 0.000 description 1
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 1
- MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000000832 lactitol Substances 0.000 description 1
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- VQHSOMBJVWLPSR-JVCRWLNRSA-N lactitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@@H]1O[C@H](CO)[C@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-JVCRWLNRSA-N 0.000 description 1
- 229960003451 lactitol Drugs 0.000 description 1
- 239000008101 lactose Substances 0.000 description 1
- 229960001375 lactose Drugs 0.000 description 1
- 229940071085 lauroyl glutamate Drugs 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
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- 229960000274 lysozyme Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 229960002216 methylparaben Drugs 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 description 1
- 125000004365 octenyl group Chemical group C(=CCCCCCC)* 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
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- 229920001277 pectin Polymers 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229960000292 pectin Drugs 0.000 description 1
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 description 1
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- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- PYJBVGYZXWPIKK-UHFFFAOYSA-M potassium;tetradecanoate Chemical compound [K+].CCCCCCCCCCCCCC([O-])=O PYJBVGYZXWPIKK-UHFFFAOYSA-M 0.000 description 1
- 235000019423 pullulan Nutrition 0.000 description 1
- 229940109850 royal jelly Drugs 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- BTURAGWYSMTVOW-UHFFFAOYSA-M sodium dodecanoate Chemical compound [Na+].CCCCCCCCCCCC([O-])=O BTURAGWYSMTVOW-UHFFFAOYSA-M 0.000 description 1
- 229940037001 sodium edetate Drugs 0.000 description 1
- 229940082004 sodium laurate Drugs 0.000 description 1
- IEXXLSKKBWIDAC-ZOWNYOTGSA-M sodium;(3s)-3-(dodecanoylamino)-4-hydroxy-4-oxobutanoate Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CC(O)=O IEXXLSKKBWIDAC-ZOWNYOTGSA-M 0.000 description 1
- 229940071136 stearoyl glutamate Drugs 0.000 description 1
- 229960004793 sucrose Drugs 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 229940117986 sulfobetaine Drugs 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 235000015523 tannic acid Nutrition 0.000 description 1
- 229920002258 tannic acid Polymers 0.000 description 1
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
- 229940033123 tannic acid Drugs 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical class NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 1
- 229940098465 tincture Drugs 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960003487 xylose Drugs 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- OJYLAHXKWMRDGS-UHFFFAOYSA-N zingerone Chemical compound COC1=CC(CCC(C)=O)=CC=C1O OJYLAHXKWMRDGS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/267—Heterocyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
Description
本発明の構成は、次のとおりである。
N−アシルグルタミン酸塩と環状構造保有分岐状グルカン、ヒドロキシプロピルデンプンリン酸、ポリデキストロースからなる群から選ばれる一種以上を含有することを特徴とする粉末または顆粒状の皮膚洗浄料。
本発明に用いられる環状構造保有分岐状グルカンとして市販品を用いることが可能であり、例えば、日本食品化工(株)製「クラスターデキストリン」が挙げられる。
ヒドロキシアルキルデンプンリン酸は市販品を用いることができ、例えばアクゾノーベル(株)製ヒドロキシプロピルデンプンリン酸「STRUCTURE XL」が挙げられる。
ポリデキストロースとして市販品を用いることができ、例えば、ダニスコジャパン(株)製「ライテスウルトラ」が挙げられる。
本発明の皮膚洗浄料には界面活性剤として、N−アシルグルタミン酸塩以外のアニオン界面活性剤、両性界面活性剤、カチオン界面活性剤、ノニオン界面活性剤を配合することができる。
アニオン界面活性剤としては、高級脂肪酸塩、N−アシルアラニン塩、N−アシルメチルタウリン塩、N−アシルイセチオン酸塩、N−アシルグリシン塩、モノアルキルリン酸塩、エ−テルカルボン酸塩、アルキルスルホン酸塩、スルホコハク酸塩等が挙げられる。
両性界面活性剤としては、カルボベタイン型界面活性剤、スルホベタイン型界面活性剤、アミドベタイン型界面活性剤、イミダゾリン型界面活性剤等が挙げられる。
無機粉体としては、タルク、カオリン、シリカ、雲母、ゼオライト、ベントナイト、二酸化チタン等が挙げられる。
薬効成分としては、L−アスコルビン酸、L−アスコルビン酸リン酸エステル、L−アスコルビン酸モノパルミチン酸エステル、L−アスコルビン酸ジパルミチン酸エステル、L−アスコルビン酸−2−グルコシド等のビタミンC類等、グルタチオン、ユキノシタ抽出物等の美白剤、ローヤルゼリー、ぶなの木エキス等の皮膚賦活剤、カプサイシン、ジンゲロン、カンタリスチンキ、イクタモール、カフェイン、タンニン酸γ−オリザノール等の血行促進剤、グリチルリチン酸誘導体、グリチルレチン酸誘導体、アズレン等の消炎剤、常在菌コントロール剤のマルトースショ糖縮合物、塩化リゾチーム等を挙げることができる。
本発明の皮膚洗浄料は、洗顔や、身体の洗浄に使用することができる。
専門パネラー10名に、調製した試料0.6gを手のひらにとり、水道水約2〜3mLを加えて、両手をこすり合わせるように約30秒間泡立てさせ、その後泡に空気を巻き込むようにしっかりと泡立て動作をさせた。
(ヤシ脂肪酸/パーム脂肪酸/ヒマワリ脂肪酸)アシルグルタミン酸ナトリウム単独の粉末状皮膚洗浄料の泡質を標準として、以下の基準により評価させた。
4点:著しく弾力があり、キメが細かい。
3点:弾力があり、キメが細かい。
2点:変わらない。
1点:弾力が少なく、キメが粗い。
0点:著しく弾力が少なく、キメが粗い。
10名の評価点の平均値を表1に示す。
専門パネラー10名に、泡質の評価と同時に起泡性を評価させた。
(ヤシ脂肪酸/パーム脂肪酸/ヒマワリ脂肪酸)アシルグルタミン酸ナトリウム単独の粉末状皮膚洗浄料の起泡性を標準として、以下の基準により評価させた。
4点:著しく泡立ちが速い。
3点:泡立ちが速い。
2点:変わらない。
1点:泡立ちが遅い。
0点:著しく泡立ちが遅い。
10名の評価点の平均値を表1に示す。
泡質の評価の平均値と起泡性の評価の平均値を合計し、以下の基準により評価した。
◎:6点以上8点以下
○:5点以上6点未満
△:4点以上5点未満
×:4点未満
総合評価を表1に示す。
オクテニルコハク酸化デンプンを配合した比較例12の粉末状皮膚洗浄料は、0.5〜1質量%の配合量で優れた起泡性を示したが、配合濃度を増すにつれて泡質が顕著に低下する傾向にあった。
PEGを配合した比較例4、5については、1〜5質量%配合して泡立てた際に、不溶物の固まりが顕著に出現したため、評価しなかった。
成分 配合量(質量%)
N-ラウロイルグルタミン酸ナトリウム 40
ポリγグルタミン酸ナトリウム 0.02
L−セリン 0.02
マンニトール 30
ブドウ糖 10
環状構造保有分岐状グルカン 3
ヒドロキシプロピルデンプンリン酸 3
ポリデキストロース 3
タルク 残余
成分 配合量(質量%)
N-ヤシ油脂肪酸アシルグルタミン酸ナトリウム 30
ラウリン酸ナトリウム 10
N-ラウロイルアスパラギン酸ナトリウム 10
ポリγグルタミン酸ナトリウム 4
L−セリン 4
マンニトール 20
ブドウ糖 10
環状構造保有分岐状グルカン 1
ヒドロキシプロピルデンプンリン酸 1
ポリデキストロース 1
タルク 残余
成分 配合量(質量%)
N-ラウロイルグルタミン酸ナトリウム 10
N-ミリストイルグルタミン酸カリウム 18
ミリスチン酸カリウム 2
ポリγグルタミン酸ナトリウム 0.3
L−セリン 0.3
ヤシ油脂肪酸エチルエステルスルホン酸ナトリウム 10
マンニトール 10
マルチトール 10
塩化O-[2-ヒドロキシ-3-(トリメチルアンモニオ)プロピル]
デキストラン 0.1
寒天粉末 2
デキストリン末 2
環状構造保有分岐状グルカン 5
ヒドロキシプロピルデンプンリン酸 5
ポリデキストロース 5
タルク 残余
Claims (1)
- N−アシルグルタミン酸塩とポリデキストロースを含有することを特徴とする粉末または顆粒状の皮膚洗浄料。
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JP2012239479A JP5662986B2 (ja) | 2012-10-30 | 2012-10-30 | 粉末皮膚洗浄料 |
TW102129762A TW201416088A (zh) | 2012-10-30 | 2013-08-20 | 粉末皮膚洗淨料 |
CN201310487327.1A CN103784329A (zh) | 2012-10-30 | 2013-10-17 | 粉末皮肤清洗品 |
KR1020130129336A KR20140056061A (ko) | 2012-10-30 | 2013-10-29 | 분말 피부 세정료 |
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WO2016093089A1 (ja) * | 2014-12-12 | 2016-06-16 | ライオン株式会社 | 皮膚洗浄剤組成物 |
CN107184407B (zh) * | 2017-05-24 | 2020-10-20 | 云南贝泰妮生物科技集团股份有限公司 | 一种柔滑保湿造粒洁颜粉及其制备方法 |
JP7442991B2 (ja) | 2019-07-25 | 2024-03-05 | ポーラ化成工業株式会社 | 水中油乳化型化粧料 |
CN112608800A (zh) * | 2020-12-17 | 2021-04-06 | 江苏耐雀生物工程技术有限公司 | 一种具有抗敏功能的手工皂及其制备方法 |
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FR2663948B1 (fr) * | 1990-07-02 | 1994-06-03 | Rhone Poulenc Chimie | Composition detergente contenant un polysaccharide greffe biodegradable. |
CA2095776C (en) * | 1992-05-12 | 2007-07-10 | Richard C. Fuisz | Rapidly dispersable compositions containing polydextrose |
JP3107358B2 (ja) * | 1994-09-13 | 2000-11-06 | 江崎グリコ株式会社 | 環状構造を有するグルカンおよびその製造方法 |
JP2003238337A (ja) * | 2002-02-08 | 2003-08-27 | Kanebo Ltd | 粉末状化粧料 |
US6727209B2 (en) * | 2002-08-14 | 2004-04-27 | Unilever Home & Personal Care, Usa, Division Of Conopco, Inc. | Biphasic composition induced by polydextrose and sucrose |
JP4600030B2 (ja) * | 2003-12-19 | 2010-12-15 | 味の素株式会社 | N−長鎖アシルグルタミン酸及び/又はその塩の結晶 |
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JP4738749B2 (ja) * | 2004-02-18 | 2011-08-03 | アクゾノーベル株式会社 | 化粧品用組成物 |
JP4696507B2 (ja) * | 2004-09-13 | 2011-06-08 | 味の素株式会社 | 洗浄剤組成物 |
JP4257442B2 (ja) * | 2007-08-27 | 2009-04-22 | 株式会社ファンケル | 皮膚洗浄料及びこれに用いるn−アシルグルタミン酸塩 |
JP2010196042A (ja) * | 2009-01-28 | 2010-09-09 | Unitika Ltd | 高度に柔軟なゲル状組成物およびその用途 |
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