JP5586686B2 - １，６−ヘキサンジオールの製造方法 - Google Patents

１，６−ヘキサンジオールの製造方法 Download PDF

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Publication number
JP5586686B2
JP5586686B2 JP2012503955A JP2012503955A JP5586686B2 JP 5586686 B2 JP5586686 B2 JP 5586686B2 JP 2012503955 A JP2012503955 A JP 2012503955A JP 2012503955 A JP2012503955 A JP 2012503955A JP 5586686 B2 JP5586686 B2 JP 5586686B2
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Japan
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acid
hydrogenation
cyclohexanediol
catalyst
esterification
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Japanese (ja)
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JP2012522819A5 (https=
JP2012522819A (ja
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ピンコス ロルフ
ブロイニンガー ダニエル
テベン ゲアト−ディーター
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
    • C07C29/145—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP2012503955A 2009-04-07 2010-03-29 １，６−ヘキサンジオールの製造方法 Expired - Fee Related JP5586686B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09157511 2009-04-07
EP09157511.8 2009-04-07
PCT/EP2010/054053 WO2010115738A1 (de) 2009-04-07 2010-03-29 Verfahren zur herstellung von 1,6-hexandiol

Publications (3)

Publication Number Publication Date
JP2012522819A JP2012522819A (ja) 2012-09-27
JP2012522819A5 JP2012522819A5 (https=) 2013-05-16
JP5586686B2 true JP5586686B2 (ja) 2014-09-10

Family

ID=42668286

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012503955A Expired - Fee Related JP5586686B2 (ja) 2009-04-07 2010-03-29 １，６−ヘキサンジオールの製造方法

Country Status (9)

Country Link
US (1) US8629306B2 (https=)
EP (1) EP2417088B1 (https=)
JP (1) JP5586686B2 (https=)
KR (1) KR20120005018A (https=)
CN (1) CN102388009B (https=)
CA (1) CA2755696A1 (https=)
ES (1) ES2415156T3 (https=)
SG (1) SG174392A1 (https=)
WO (1) WO2010115738A1 (https=)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009047194A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Kunststoffen mit 1,6-Hexandiol mit einem Aldehydanteil von kleiner 500ppm
DE102009047193A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Diolen durch Hydrierung eines Carbonsäure enthaltenden Gemisches mittels Kobalt enthaltenden Katalysatoren
US8865940B2 (en) 2011-12-30 2014-10-21 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
US8889912B2 (en) 2011-12-30 2014-11-18 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
BR112014015994A2 (pt) 2011-12-30 2018-05-22 Du Pont processo.
US8884036B2 (en) 2011-12-30 2014-11-11 E I Du Pont De Nemours And Company Production of hydroxymethylfurfural from levoglucosenone
JP2015503569A (ja) 2011-12-30 2015-02-02 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ ヘキサンジオールを生成するための方法
EP2797866A4 (en) 2011-12-30 2015-08-05 Du Pont PROCESS FOR THE PREPARATION OF 1,6-HEXANEDIOL
US8859826B2 (en) 2012-04-27 2014-10-14 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US9018423B2 (en) 2012-04-27 2015-04-28 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US8846985B2 (en) 2012-04-27 2014-09-30 E I Du Pont De Nemours And Company Production of alpha, omega-diols
CN105727962B (zh) * 2016-02-02 2018-07-31 上海华峰新材料研发科技有限公司 用于己二酸二甲酯制己二醇的催化剂及其制备方法和应用
TWI905687B (zh) * 2023-04-13 2025-11-21 日商Ｄｉｃ股份有限公司 六亞甲基(甲基)丙烯酸酯組成物、活性能量線硬化型樹脂組成物、硬化物

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1235879B (de) 1964-03-17 1967-03-09 Basf Ag Verfahren zur Herstellung von Alkoholen durch katalytische Hydrierung von Carbonsaeuren
JPS4815314B1 (https=) * 1969-08-18 1973-05-14
DE2060548C3 (de) 1970-12-09 1979-10-11 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von sehr reinem 1,6-Hexandiol durch Kristallisation
DE2321101C2 (de) 1973-04-26 1982-07-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung im wesentlichen trägerfreier Kobaltkatalysatoren
US3933930A (en) * 1975-03-06 1976-01-20 Celanese Corporation Hexanediol from cyclohexane
DE4141199A1 (de) 1991-12-13 1993-06-17 Sued Chemie Ag Chromfreier katalysator fuer die hydrierung von organischen verbindungen, die die carbonylfunktionen enthalten
DE59703470D1 (de) * 1996-03-01 2001-06-07 Basf Ag Verfahren zur herstellung von 1,6-hexandiol mit einer reinheit über 99 %
MY118128A (en) * 1996-03-01 2004-09-30 Basf Ag The preparation of 1, 6-hexanediol and caprolactone
DE19607954A1 (de) 1996-03-01 1997-09-04 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol und Caprolacton
DE19730939A1 (de) 1997-07-18 1999-01-21 Basf Ag Verfahren zur Hydrierung von Carbonylverbindungen
DE19738464A1 (de) 1997-09-03 1999-03-04 Basf Ag Verwendung von Formkörpern als Katalysator zur Herstellung von Caprolactam
DE10128249A1 (de) * 2001-06-11 2002-12-12 Basf Ag Verfahren zur Entfernung von Ameisensäure aus wässrigen Lösungen
DE10313702A1 (de) 2003-03-27 2004-10-07 Basf Ag Katalysator und Verfahren zur Hydrierung von Carbonylverbindungen
DE102004033557A1 (de) * 2004-07-09 2006-02-16 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol in einer Reinheit von über 99,5%
DE102004054047A1 (de) * 2004-11-05 2006-05-11 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol
JP2010529159A (ja) * 2007-06-14 2010-08-26 ビーエーエスエフ ソシエタス・ヨーロピア ε−カプロラクトンの製造法
JP5453289B2 (ja) 2007-11-05 2014-03-26 ビーエーエスエフ ソシエタス・ヨーロピア ε−カプロラクトンの製造方法
MY148576A (en) 2007-12-21 2013-04-30 Basf Se Process for preparing epsilon-caprolactone
CA2714574A1 (en) 2008-02-15 2009-08-20 Basf Se Process for preparing 6-hydroxycaproic esters
SG174394A1 (en) * 2009-04-07 2011-10-28 Basf Se Method for producing 1,6-hexanediol and caprolactone
DE102009047194A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Kunststoffen mit 1,6-Hexandiol mit einem Aldehydanteil von kleiner 500ppm
DE102009047193A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Diolen durch Hydrierung eines Carbonsäure enthaltenden Gemisches mittels Kobalt enthaltenden Katalysatoren

Also Published As

Publication number Publication date
SG174392A1 (en) 2011-11-28
CA2755696A1 (en) 2010-10-14
US8629306B2 (en) 2014-01-14
CN102388009B (zh) 2014-11-05
EP2417088A1 (de) 2012-02-15
US20120022298A1 (en) 2012-01-26
KR20120005018A (ko) 2012-01-13
WO2010115738A1 (de) 2010-10-14
ES2415156T3 (es) 2013-07-24
CN102388009A (zh) 2012-03-21
JP2012522819A (ja) 2012-09-27
EP2417088B1 (de) 2013-05-29

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