JP5439177B2 - 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法 - Google Patents

共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法 Download PDF

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JP5439177B2
JP5439177B2 JP2009525655A JP2009525655A JP5439177B2 JP 5439177 B2 JP5439177 B2 JP 5439177B2 JP 2009525655 A JP2009525655 A JP 2009525655A JP 2009525655 A JP2009525655 A JP 2009525655A JP 5439177 B2 JP5439177 B2 JP 5439177B2
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hfc
fluoroolefin
distillate
mixture
composition
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JP2010501579A5 (enExample
JP2010501579A (ja
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ジェフリー・ピー・ナップ
バリー・アシャー・マーラー
ドナルド・ジェイ・トートン
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EIDP Inc
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification
    • C01B7/196—Separation; Purification by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2009525655A 2006-08-24 2007-08-24 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法 Active JP5439177B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US83973706P 2006-08-24 2006-08-24
US60/839,737 2006-08-24
PCT/US2007/018837 WO2008024508A1 (en) 2006-08-24 2007-08-24 Processes for separation of fluoroolefins from hydrogen fluoride by azeotropic distillation

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JP2010501579A JP2010501579A (ja) 2010-01-21
JP2010501579A5 JP2010501579A5 (enExample) 2010-09-30
JP5439177B2 true JP5439177B2 (ja) 2014-03-12

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US (2) US8273928B2 (enExample)
EP (2) EP2054361B1 (enExample)
JP (1) JP5439177B2 (enExample)
CN (1) CN101541715B (enExample)
ES (1) ES2450945T3 (enExample)
PL (1) PL2433921T3 (enExample)
RU (1) RU2466979C2 (enExample)
WO (1) WO2008024508A1 (enExample)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY145459A (en) * 2005-11-01 2012-02-15 Du Pont Solvent compositions comprising unsaturated fluorinated hydrocarbons
BRPI0619729A2 (pt) * 2005-12-14 2011-10-11 Sasol Tech Pty Ltd método e aparelho para produção de metil isobutil cetona purificada
EP1960339B1 (en) * 2005-12-14 2012-09-12 Sasol Technology (Pty) Ltd Method and apparatus for producing purified methyl isobutyl ketone
DE102006004870A1 (de) * 2006-02-02 2007-08-16 Siltronic Ag Halbleiterschichtstruktur und Verfahren zur Herstellung einer Halbleiterschichtstruktur
WO2008002500A1 (en) * 2006-06-27 2008-01-03 E. I. Du Pont De Nemours And Company Tetrafluoropropene production processes
RU2444508C2 (ru) * 2006-06-27 2012-03-10 Е. И. Дюпон Де Немур Энд Компани Способ производства тетрафторпропена
US7563384B2 (en) * 2006-07-28 2009-07-21 Honeywell International Inc. Essentially non-flammable low global warming compositions
US8273928B2 (en) 2006-08-24 2012-09-25 E I Du Pont De Nemours And Company Processes for separation of fluoroolefins from hydrogen fluoride by azeotropic distillation
WO2008030438A2 (en) * 2006-09-05 2008-03-13 E. I. Du Pont De Nemours And Company A process and methods of purification for the manufacture fluorocarbons
WO2008030615A2 (en) * 2006-09-08 2008-03-13 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,1,2,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7888539B2 (en) * 2007-02-23 2011-02-15 E.I. Du Pont De Nemours And Company Azeotrope compositions of octafluorocyclobutane and uses thereof
US7641808B2 (en) 2007-08-23 2010-01-05 E.I. Du Pont De Nemours And Company Azeotropic compositions comprising fluorinated olefins for cleaning applications
US8287579B2 (en) * 2007-09-17 2012-10-16 Thermage, Inc. Method of using cryogenic compositions for cooling heated skin
JP5136111B2 (ja) * 2008-02-19 2013-02-06 セントラル硝子株式会社 フルオロオレフィンとフッ化水素の分離方法
CA2712616A1 (en) * 2008-02-21 2009-08-27 E. I. Du Pont De Nemours And Company Processes for separation of 1,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation
WO2009105512A1 (en) * 2008-02-21 2009-08-27 E. I. Du Pont De Nemours And Company Processes for separation of 2,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation
ES2610615T3 (es) * 2008-02-21 2017-04-28 The Chemours Company Fc, Llc Composiciones de azeótropos que comprenden 3,3,3-trifluoropropeno y fluoruro de hidrógeno y procedimientos para la separación de los mismos
JP5176624B2 (ja) * 2008-03-18 2013-04-03 ダイキン工業株式会社 冷凍装置
KR102010208B1 (ko) 2008-05-07 2019-08-12 더 케무어스 컴퍼니 에프씨, 엘엘씨 2,3-다이클로로-1,1,1-트라이플루오로프로판, 2-클로로-1,1,1-트라이플루오로프로펜, 2-클로로-1,1,1,2-테트라플루오로프로판 또는 2,3,3,3-테트라플루오로프로펜을 포함하는 조성물
US8168837B2 (en) * 2008-05-15 2012-05-01 Honeywell International Inc. Process for separating hydrogen fluoride from organic feedstocks
JP5370479B2 (ja) 2008-08-26 2013-12-18 ダイキン工業株式会社 共沸又は共沸様組成物、及び2,3,3,3−テトラフルオロプロペンの製造方法
FR2937328B1 (fr) 2008-10-16 2010-11-12 Arkema France Procede de transfert de chaleur
US20100119460A1 (en) * 2008-11-11 2010-05-13 Honeywell International Inc. Azeotrope-Like Compositions Of 2,3,3,3-Tetrafluoropropene And 3,3,3-Trifluoropropene
US8871112B2 (en) 2008-11-19 2014-10-28 E I Du Pont De Nemours And Company Compositions comprising 2,3,3,3-tetrafluoropropene and hydrocarbons and uses thereof
US9061958B2 (en) 2009-03-24 2015-06-23 Arkema Inc. Separation of R-1233 from hydrogen fluoride
US8735636B2 (en) * 2009-03-24 2014-05-27 Arkema Inc. Separation of R-1233 from hydrogen fluoride
EP2499110B1 (en) * 2009-11-10 2020-02-26 Daikin Industries, Ltd. Method for purifying 2,3,3,3-tetrafluoropropene
HUE047698T2 (hu) 2009-12-22 2020-05-28 Chemours Co Fc Llc 2,3,3,3-tetrafluorpropént és 2,3-diklór-3,3-difluorpropént tartalmazó kompozíciók
US8747691B2 (en) * 2010-05-06 2014-06-10 Honeywell International Inc. Azeotrope-like compositions of tetrafluoropropene and water
US8951431B2 (en) 2010-05-06 2015-02-10 E I Du Pont De Nemours And Company Azeotrope-like compositions of pentafluoropropene and water
US8436218B2 (en) * 2010-05-27 2013-05-07 Honeywell International Inc. Azeotrope-like composition of hexafluoropropane, hexafluoropropene and hydrogen fluoride
ES2508616T3 (es) 2010-07-23 2014-10-16 Daikin Industries, Ltd. Procedimiento de purificación de 2,3,3,3-tetrafluoropropeno
US8518293B2 (en) 2010-09-03 2013-08-27 Honeywell International Inc. 1,3,3,3-tetrafluoropropene process azeotropes with HF
WO2012157764A1 (ja) * 2011-05-19 2012-11-22 旭硝子株式会社 作動媒体および熱サイクルシステム
FR2977584B1 (fr) * 2011-07-08 2014-12-05 Arkema France Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique
US9309116B2 (en) * 2011-09-26 2016-04-12 Honeywell International Inc. Method for producing high concentration aqueous HF solutions
US8592538B2 (en) * 2011-12-20 2013-11-26 Honeywell International Inc. Azeotropes of methyl chloride with fluorocarbons
US8519200B1 (en) * 2012-02-23 2013-08-27 Honeywell International Inc. Azeotropic compositions of 1,1,3,3-tetrachloro-1-fluoropropane and hydrogen fluoride
KR20150036220A (ko) * 2012-08-01 2015-04-07 이 아이 듀폰 디 네모아 앤드 캄파니 E-1,3,4,4,4-펜타플루오로-3-트라이플루오로메틸-1-부텐 및 z-1,1,1,4,4,4-헥사플루오로-2-부텐의 공비 및 공비-유사 조성물 및 그의 용도
US20150191576A1 (en) * 2012-08-01 2015-07-09 E I Du Pont De Nemours And Company Azeotropic and azeotrope-like compositions of e-1,3,4,4,4-pentafluoro-3-trifluoromethyl-1-butene and z-1,1,1,4,4,4-hexafluoro-2-butene and uses thereof
WO2014028697A1 (en) * 2012-08-15 2014-02-20 E. I. Du Pont De Nemours And Company Azeotropic and azeotrope-like compositions of 2,3,3,4,4,4-hexafluoro-1-butene and 1,1,1,2,3,3-hexafluoropropane and uses thereof
US8927666B2 (en) 2012-11-08 2015-01-06 Honeywell International Inc. Polymerization of monomers using fluorinated propylene solvents
US8987399B2 (en) * 2012-11-08 2015-03-24 Honeywell International Inc. Azeotropes of isobutylene with fluoro-olefins
FR3000093B1 (fr) * 2012-12-26 2015-07-17 Arkema France Composition azeotropique ou quasi-azeotropique de chloromethane
FR3003567B1 (fr) * 2013-03-20 2015-03-06 Arkema France Composition comprenant hf et 3,3,3-trifluoropropene
FR3003569B1 (fr) * 2013-03-20 2015-12-25 Arkema France Composition comprenant hf et 1,3,3,3-tetrafluoropropene
FR3003565B1 (fr) * 2013-03-20 2018-06-29 Arkema France Composition comprenant hf et 2,3,3,3-tetrafluoropropene
FR3003566B1 (fr) * 2013-03-20 2018-07-06 Arkema France Composition comprenant hf et e-3,3,3-trifluoro-1-chloropropene
CN110041163A (zh) * 2013-07-16 2019-07-23 Agc株式会社 三氟乙烯的保存方法
CN110184033A (zh) * 2013-10-08 2019-08-30 得凯莫斯公司弗罗里达有限公司 E-HFO-1438ez和E-1-氯-三氟丙烯的类共沸组合物及其用途
FR3015478B1 (fr) 2013-12-19 2015-12-25 Arkema France Compositions azeotropiques a base de fluorure d'hydrogene et de z-3,3,3-trifluoro-1-chloropropene
KR102354557B1 (ko) * 2014-04-29 2022-01-26 알케마 인코포레이티드 불화수소로부터 r-1233의 분리
CN107001919A (zh) * 2014-08-12 2017-08-01 科慕埃弗西有限公司 Hfo‑e‑1,3,4,4,4‑五氟‑3‑三氟甲基‑1‑丁烯的共沸组合物和类共沸组合物及它们的用途
EP3265508A1 (en) * 2015-03-02 2018-01-10 The Chemours Company FC, LLC Azeotropic and azeotrope-like compositions of z-1-chloro-3,3,3-trifluoropropene
CN105669363A (zh) * 2016-02-23 2016-06-15 常熟三爱富中昊化工新材料有限公司 一种含氟烯烃的纯化方法
US10399004B2 (en) * 2016-09-08 2019-09-03 Eastman Chemical Company Thermally integrated distillation systems and processes using the same
FR3056222B1 (fr) 2016-09-19 2020-01-10 Arkema France Composition a base de 1-chloro-3,3,3-trifluoropropene
FR3096984B1 (fr) * 2017-06-09 2023-07-14 Arkema France 1,1,1,2,3,3-hexafluoropropane de haute pureté, son procédé de fabrication et utilisation
FR3067347B1 (fr) * 2017-06-09 2020-07-24 Arkema France 1,1,1,2,3,3-hexafluoropropane de haute purete, son procede de fabrication et utilisation
US10851303B2 (en) 2017-07-27 2020-12-01 The Chemours Company Fc, Llc Azeotropic compositions comprising hydrogen fluoride and fluorocarbons
CN111094503B (zh) * 2017-09-11 2022-04-01 科慕埃弗西有限公司 包含氟化氢和含氟烃的共沸组合物
JPWO2019123898A1 (ja) * 2017-12-18 2020-12-10 ダイキン工業株式会社 冷媒用または冷媒組成物用の冷凍機油、冷凍機油の使用方法、および、冷凍機油としての使用
FR3077572B1 (fr) 2018-02-05 2021-10-08 Arkema France Composition azeotropique ou quasi-azeotropique ternaire comprenant hf, 2,3,3,3-tetrafluoropropene et 1,1,1,2,2,-pentafluoropropane.
US11767494B2 (en) * 2018-05-03 2023-09-26 The Chemours Company Fc, Llc Binary azeotrope and azeotrope-like compositions comprising perfluoroheptene
US10662135B2 (en) * 2018-10-15 2020-05-26 Honeywell International Inc. Azeotrope or azeotrope-like compositions of trifluoroiodomethane (CF3I) and hexafluoroacetone (HFA)
US11344761B2 (en) 2018-10-15 2022-05-31 Honeywell International Inc. Azeotrope or azeotrope-like compositions of trifluoroiodomethane (CF3I) and 1,1,1,2,2,3,3,-heptafluoropropane (HFC-227ca)
US11318338B2 (en) * 2018-10-15 2022-05-03 Honeywell International Inc. Azeotrope or azeotrope-like compositions of trifluoroidomethane (CF3I) and 1,1,1,3,3,3-hexafluoropropane (HFC-236fa)
EP3919467A4 (en) * 2019-01-28 2022-11-02 Daikin Industries, Ltd. AZEOTROPICAL COMPOSITION WITH 1,2-DIFLUORETHYLENE OR 1,1,2-TRIFLUORETHYLENE AND HYDROGEN FLUORIDE
MX2023004646A (es) * 2020-10-21 2023-05-18 Daikin Ind Ltd Metodo para producir una composicion que contiene un compuesto de eter que contiene fluor purificado.
CN112607707B (zh) * 2020-12-16 2022-05-20 浙江天采云集科技股份有限公司 一种工业级高浓度HF精制为电子级的FTrPSA分离与提纯方法
US20240018074A1 (en) * 2022-07-14 2024-01-18 Honeywell International Inc. METHOD FOR REDUCING CHLOROFLUOROCARBON IMPURITIES IN THE MANUFACTURE OF TRANS-1,3,3,3-TETRAFLUOROPROPENE (HFO-1234ze(E))
CN118459669B (zh) * 2024-07-09 2024-09-27 黄山熠能科技有限公司 一种乙炔与hf反应的固体催化剂的制备方法及应用

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2831902A (en) 1957-01-18 1958-04-22 Dow Chemical Co Separation of 2-fluoropropene
US3947558A (en) * 1973-08-16 1976-03-30 Dow Chemical (Nederland) B.V. Method of recovering HF from mixtures containing C1 -C3 halocarbon compounds
SU1706690A1 (ru) 1988-04-19 1992-01-23 Всесоюзный Научно-Исследовательский Институт Технического Углерода Пористый углеродный материал
JP3175286B2 (ja) * 1991-04-15 2001-06-11 ダイキン工業株式会社 フッ化水素と1,1,1−トリフルオロ−2−クロロエタンの共沸混合物および1,1,1−トリフルオロ−2−クロロエタンの精製方法
FR2675496B1 (fr) * 1991-04-17 1993-09-03 Atochem Procede de separation du fluorure d'hydrogene de ses melanges avec le 1,1,1-trifluoro-2-chloroethane.
BR9305484A (pt) * 1992-04-13 1995-04-11 Daikin Ind Ltd Processo para remoção de fluoreto de hidrogênio.
KR950701896A (ko) 1992-06-05 1995-05-17 이노우에 노리유키 1,1,1,2,3-펜타플루오로프로펜의 제조방법 및 1,1,1,2,3-펜타플루오로프로판의 제조방법
US5396000A (en) 1993-05-24 1995-03-07 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,1,1,2,3,-pentafluoropropane
EP0734368B1 (en) 1993-12-14 2001-08-29 E.I. Du Pont De Nemours And Company Process for perhalofluorinated butanes
DE69812901T2 (de) 1997-01-31 2003-11-06 E.I. Du Pont De Nemours And Co., Wilmington Katalytische herstellung von pentafluorpropenen
US6031141A (en) 1997-08-25 2000-02-29 E. I. Du Pont De Nemours And Company Fluoroolefin manufacturing process
EP1027313A1 (en) 1997-10-17 2000-08-16 E.I. Du Pont De Nemours And Company Separating 1,1,1,3,3-pentafluoropropane from hydrogen fluoride
US5918481A (en) 1997-11-20 1999-07-06 Alliedsignal Inc. Process for separating hydrogen fluoride from fluorocarbons
AU747117B2 (en) * 1997-11-25 2002-05-09 Ineos Fluor Holdings Limited Preparation of fluorine-containing organic compounds
US6013846A (en) 1998-03-05 2000-01-11 Elf Atochem North America, Inc. Azeotrope of HF and 1233zd
JP3518321B2 (ja) * 1998-03-23 2004-04-12 ダイキン工業株式会社 1,1,1,3,3−ペンタフルオロプロパンの製造方法
US20030028057A1 (en) 2001-07-20 2003-02-06 Stephen Owens Methods and materials for the preparation and purification of halogenated hydrocarbons
RU2265007C1 (ru) * 2004-05-31 2005-11-27 Орлов Александр Павлович Способ выделения 1-фтор-1,1-дихлорэтана, 1,1-дифтор-1-хлорэтана, 1,1,1-трифторэтана и хлористого водорода из газов синтеза
US20060094911A1 (en) * 2004-10-29 2006-05-04 Rao Velliyur N M Noncatalytic manufacture of 1,1,3,3,3-pentafluoropropene from 1,1,1,3,3,3-hexafluoropropane
US20060116538A1 (en) * 2004-10-29 2006-06-01 Ralph Newton Miller Azeotrope compositions comprising 1,1,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7388117B2 (en) 2005-11-01 2008-06-17 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7385094B2 (en) 2005-11-01 2008-06-10 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising tridecafluoro-3-heptene and hydrogen fluoride and uses thereof
US7423188B2 (en) 2005-11-01 2008-09-09 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising E-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7709438B2 (en) 2005-11-01 2010-05-04 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising nonafluoropentene and hydrogen fluoride and uses thereof
US7476771B2 (en) 2005-11-01 2009-01-13 E.I. Du Pont De Nemours + Company Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US8273928B2 (en) 2006-08-24 2012-09-25 E I Du Pont De Nemours And Company Processes for separation of fluoroolefins from hydrogen fluoride by azeotropic distillation
WO2008030615A2 (en) 2006-09-08 2008-03-13 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,1,1,2,3-pentafluoropropene and hydrogen fluoride and uses thereof
WO2009105512A1 (en) 2008-02-21 2009-08-27 E. I. Du Pont De Nemours And Company Processes for separation of 2,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation

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Publication number Publication date
PL2433921T3 (pl) 2014-06-30
EP2433921B1 (en) 2014-01-15
EP2054361A1 (en) 2009-05-06
RU2466979C2 (ru) 2012-11-20
EP2054361B1 (en) 2016-02-17
US8273928B2 (en) 2012-09-25
US9000238B2 (en) 2015-04-07
US20120305382A1 (en) 2012-12-06
CN101541715A (zh) 2009-09-23
EP2433921A1 (en) 2012-03-28
ES2450945T3 (es) 2014-03-25
US20080051612A1 (en) 2008-02-28
WO2008024508A1 (en) 2008-02-28
CN101541715B (zh) 2013-09-11
RU2009110481A (ru) 2010-09-27
JP2010501579A (ja) 2010-01-21

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