JP5436209B2 - 転換増強方法及び生成物流を生産する生産方法 - Google Patents
転換増強方法及び生成物流を生産する生産方法 Download PDFInfo
- Publication number
- JP5436209B2 JP5436209B2 JP2009519539A JP2009519539A JP5436209B2 JP 5436209 B2 JP5436209 B2 JP 5436209B2 JP 2009519539 A JP2009519539 A JP 2009519539A JP 2009519539 A JP2009519539 A JP 2009519539A JP 5436209 B2 JP5436209 B2 JP 5436209B2
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- downflow reactor
- product stream
- stream
- reaction product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G51/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only
- C10G51/06—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only plural parallel stages only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
- C10G11/14—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
- C10G11/18—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/40—Characteristics of the process deviating from typical ways of processing
- C10G2300/4006—Temperature
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/40—Characteristics of the process deviating from typical ways of processing
- C10G2300/4093—Catalyst stripping
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/02—Gasoline
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/20—C2-C4 olefins
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/487,011 US20080011644A1 (en) | 2006-07-13 | 2006-07-13 | Ancillary cracking of heavy oils in conjuction with FCC unit operations |
| US11/487,011 | 2006-07-13 | ||
| PCT/US2007/015950 WO2008008470A2 (en) | 2006-07-13 | 2007-07-11 | Ancillary cracking of heavy oils in conjuction with fcc unit operations |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009543898A JP2009543898A (ja) | 2009-12-10 |
| JP2009543898A5 JP2009543898A5 (enExample) | 2013-05-09 |
| JP5436209B2 true JP5436209B2 (ja) | 2014-03-05 |
Family
ID=38923918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009519539A Expired - Fee Related JP5436209B2 (ja) | 2006-07-13 | 2007-07-11 | 転換増強方法及び生成物流を生産する生産方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (2) | US20080011644A1 (enExample) |
| EP (1) | EP2046919A4 (enExample) |
| JP (1) | JP5436209B2 (enExample) |
| KR (1) | KR101447299B1 (enExample) |
| CN (1) | CN101743292B (enExample) |
| BR (1) | BRPI0713238A2 (enExample) |
| CA (1) | CA2657615C (enExample) |
| EA (1) | EA014574B1 (enExample) |
| MX (1) | MX2009000383A (enExample) |
| NO (1) | NO20090153L (enExample) |
| WO (1) | WO2008008470A2 (enExample) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080011644A1 (en) * | 2006-07-13 | 2008-01-17 | Dean Christopher F | Ancillary cracking of heavy oils in conjuction with FCC unit operations |
| WO2012004809A1 (en) | 2010-07-08 | 2012-01-12 | Indian Oil Corporation Ltd. | Two stage fluid catalytic cracking process and apparatus |
| SG11201502991RA (en) * | 2012-10-19 | 2015-06-29 | Saudi Arabian Oil Co | Process for high severity catalytic cracking of crude oil |
| EA201691762A1 (ru) * | 2013-11-19 | 2016-12-30 | Шеврон Ю.Эс.Эй. Инк. | Способ получения средних дистиллятов и тяжелого вакуумного газойля, служащего сырьем флюид-каталитического крекинга |
| JP2017502110A (ja) * | 2013-12-02 | 2017-01-19 | サウジ アラビアン オイル カンパニー | 軽質オレフィンの製造のための溶剤脱瀝および流動接触分解の統合された方法 |
| CN106609146B (zh) * | 2015-10-21 | 2018-06-19 | 中国石油化工股份有限公司 | 一种调节费托合成油催化裂化热平衡的方法 |
| CN106609151B (zh) * | 2015-10-21 | 2018-05-18 | 中国石油化工股份有限公司 | 一种生产低碳烯烃的方法 |
| US10844296B2 (en) | 2017-01-04 | 2020-11-24 | Saudi Arabian Oil Company | Conversion of crude oil to aromatic and olefinic petrochemicals |
| US10851316B2 (en) | 2017-01-04 | 2020-12-01 | Saudi Arabian Oil Company | Conversion of crude oil to aromatic and olefinic petrochemicals |
| US10767117B2 (en) | 2017-04-25 | 2020-09-08 | Saudi Arabian Oil Company | Enhanced light olefin yield via steam catalytic downer pyrolysis of hydrocarbon feedstock |
| US10870802B2 (en) | 2017-05-31 | 2020-12-22 | Saudi Arabian Oil Company | High-severity fluidized catalytic cracking systems and processes having partial catalyst recycle |
| US10889768B2 (en) | 2018-01-25 | 2021-01-12 | Saudi Arabian Oil Company | High severity fluidized catalytic cracking systems and processes for producing olefins from petroleum feeds |
| CN108485704B (zh) * | 2018-04-17 | 2020-04-28 | 中国石油大学(华东) | 原油毫秒分级气相催化裂解和加氢组合最大化制取化工原料工艺 |
| US11680521B2 (en) | 2019-12-03 | 2023-06-20 | Saudi Arabian Oil Company | Integrated production of hydrogen, petrochemicals, and power |
| US11193072B2 (en) | 2019-12-03 | 2021-12-07 | Saudi Arabian Oil Company | Processing facility to form hydrogen and petrochemicals |
| US11572517B2 (en) | 2019-12-03 | 2023-02-07 | Saudi Arabian Oil Company | Processing facility to produce hydrogen and petrochemicals |
| US11426708B2 (en) | 2020-03-02 | 2022-08-30 | King Abdullah University Of Science And Technology | Potassium-promoted red mud as a catalyst for forming hydrocarbons from carbon dioxide |
| US11279891B2 (en) | 2020-03-05 | 2022-03-22 | Saudi Arabian Oil Company | Systems and processes for direct crude oil upgrading to hydrogen and chemicals |
| US11492255B2 (en) | 2020-04-03 | 2022-11-08 | Saudi Arabian Oil Company | Steam methane reforming with steam regeneration |
| US11420915B2 (en) | 2020-06-11 | 2022-08-23 | Saudi Arabian Oil Company | Red mud as a catalyst for the isomerization of olefins |
| US11495814B2 (en) | 2020-06-17 | 2022-11-08 | Saudi Arabian Oil Company | Utilizing black powder for electrolytes for flow batteries |
| US12000056B2 (en) | 2020-06-18 | 2024-06-04 | Saudi Arabian Oil Company | Tandem electrolysis cell |
| US11492254B2 (en) | 2020-06-18 | 2022-11-08 | Saudi Arabian Oil Company | Hydrogen production with membrane reformer |
| US11999619B2 (en) | 2020-06-18 | 2024-06-04 | Saudi Arabian Oil Company | Hydrogen production with membrane reactor |
| US11583824B2 (en) | 2020-06-18 | 2023-02-21 | Saudi Arabian Oil Company | Hydrogen production with membrane reformer |
| US11434432B2 (en) | 2020-09-01 | 2022-09-06 | Saudi Arabian Oil Company | Processes for producing petrochemical products that utilize fluid catalytic cracking of a greater boiling point fraction with steam |
| US11352575B2 (en) | 2020-09-01 | 2022-06-07 | Saudi Arabian Oil Company | Processes for producing petrochemical products that utilize hydrotreating of cycle oil |
| US11242493B1 (en) | 2020-09-01 | 2022-02-08 | Saudi Arabian Oil Company | Methods for processing crude oils to form light olefins |
| US11230672B1 (en) | 2020-09-01 | 2022-01-25 | Saudi Arabian Oil Company | Processes for producing petrochemical products that utilize fluid catalytic cracking |
| US11505754B2 (en) | 2020-09-01 | 2022-11-22 | Saudi Arabian Oil Company | Processes for producing petrochemical products from atmospheric residues |
| US11332680B2 (en) | 2020-09-01 | 2022-05-17 | Saudi Arabian Oil Company | Processes for producing petrochemical products that utilize fluid catalytic cracking of lesser and greater boiling point fractions with steam |
| US11230673B1 (en) | 2020-09-01 | 2022-01-25 | Saudi Arabian Oil Company | Processes for producing petrochemical products that utilize fluid catalytic cracking of a lesser boiling point fraction with steam |
| US11820658B2 (en) | 2021-01-04 | 2023-11-21 | Saudi Arabian Oil Company | Black powder catalyst for hydrogen production via autothermal reforming |
| US11814289B2 (en) | 2021-01-04 | 2023-11-14 | Saudi Arabian Oil Company | Black powder catalyst for hydrogen production via steam reforming |
| US11427519B2 (en) | 2021-01-04 | 2022-08-30 | Saudi Arabian Oil Company | Acid modified red mud as a catalyst for olefin isomerization |
| US11724943B2 (en) | 2021-01-04 | 2023-08-15 | Saudi Arabian Oil Company | Black powder catalyst for hydrogen production via dry reforming |
| US11718522B2 (en) | 2021-01-04 | 2023-08-08 | Saudi Arabian Oil Company | Black powder catalyst for hydrogen production via bi-reforming |
| US11718575B2 (en) | 2021-08-12 | 2023-08-08 | Saudi Arabian Oil Company | Methanol production via dry reforming and methanol synthesis in a vessel |
| US12258272B2 (en) | 2021-08-12 | 2025-03-25 | Saudi Arabian Oil Company | Dry reforming of methane using a nickel-based bi-metallic catalyst |
| US11787759B2 (en) | 2021-08-12 | 2023-10-17 | Saudi Arabian Oil Company | Dimethyl ether production via dry reforming and dimethyl ether synthesis in a vessel |
| US11578016B1 (en) | 2021-08-12 | 2023-02-14 | Saudi Arabian Oil Company | Olefin production via dry reforming and olefin synthesis in a vessel |
| US12018392B2 (en) | 2022-01-03 | 2024-06-25 | Saudi Arabian Oil Company | Methods for producing syngas from H2S and CO2 in an electrochemical cell |
| US11617981B1 (en) | 2022-01-03 | 2023-04-04 | Saudi Arabian Oil Company | Method for capturing CO2 with assisted vapor compression |
| US12227704B2 (en) | 2022-11-03 | 2025-02-18 | Saudi Arabian Oil Company | Processes for producing petrochemical products from crude oil |
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| US3424672A (en) * | 1967-01-09 | 1969-01-28 | Phillips Petroleum Co | Fluid catalytic stripping |
| US3542667A (en) * | 1968-03-21 | 1970-11-24 | Foster Wheeler Corp | Process for the production of aromatic and olefinic hydrocarbons |
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| US3784463A (en) * | 1970-10-02 | 1974-01-08 | Texaco Inc | Catalytic cracking of naphtha and gas oil |
| US3856659A (en) * | 1972-12-19 | 1974-12-24 | Mobil Oil Corp | Multiple reactor fcc system relying upon a dual cracking catalyst composition |
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| US4830728A (en) * | 1986-09-03 | 1989-05-16 | Mobil Oil Corporation | Upgrading naphtha in a multiple riser fluid catalytic cracking operation employing a catalyst mixture |
| US4814067A (en) * | 1987-08-11 | 1989-03-21 | Stone & Webster Engineering Corporation | Particulate solids cracking apparatus and process |
| US5049360A (en) * | 1988-01-19 | 1991-09-17 | Mobil Oil Corporation | Multi-stage conversion of alkanes to gasoline |
| US5053204A (en) * | 1988-12-30 | 1991-10-01 | Mobil Oil Corporation | Multiple feed point catalytic cracking apparatus using elutriable catalyst mixture |
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| FR2667609B1 (fr) * | 1990-10-03 | 1993-07-16 | Inst Francais Du Petrole | Procede et dispositif de craquage catalytique en lit fluide a courant descendant. |
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| US5584986A (en) * | 1993-03-19 | 1996-12-17 | Bar-Co Processes Joint Venture | Fluidized process for improved stripping and/or cooling of particulate spent solids, and reduction of sulfur oxide emissions |
| CN2205827Y (zh) * | 1993-07-30 | 1995-08-23 | 北京联合应用化学与化学工程研究所 | 下行催化裂化提升管两段再生装置 |
| US5582712A (en) * | 1994-04-29 | 1996-12-10 | Uop | Downflow FCC reaction arrangement with upflow regeneration |
| JPH08322377A (ja) * | 1995-05-31 | 1996-12-10 | Nisshoku Corp | 建造物等の壁面緑化基体 |
| JP3580518B2 (ja) * | 1996-06-05 | 2004-10-27 | 新日本石油株式会社 | 重質油の流動接触分解法 |
| FR2753454B1 (fr) * | 1996-09-18 | 1999-06-04 | Inst Francais Du Petrole | Procede et dispositif de craquage catalytique descendant mettant en oeuvre l'injection d'une charge sous un angle adequat sur un catalyseur conditionne |
| US5904837A (en) * | 1996-10-07 | 1999-05-18 | Nippon Oil Co., Ltd. | Process for fluid catalytic cracking of oils |
| US6045690A (en) * | 1996-11-15 | 2000-04-04 | Nippon Oil Co., Ltd. | Process for fluid catalytic cracking of heavy fraction oils |
| US5846403A (en) * | 1996-12-17 | 1998-12-08 | Exxon Research And Engineering Company | Recracking of cat naphtha for maximizing light olefins yields |
| US6187272B1 (en) * | 1997-03-13 | 2001-02-13 | Nippon Mitsubishi Oil Corporation | Recycling fluidization system |
| JP3933745B2 (ja) * | 1997-03-14 | 2007-06-20 | 新日本石油株式会社 | 気固分離器 |
| US5965012A (en) * | 1997-12-05 | 1999-10-12 | Uop Llc | FCC process with short primary contacting and controlled secondary contacting |
| US6113776A (en) * | 1998-06-08 | 2000-09-05 | Uop Llc | FCC process with high temperature cracking zone |
| FR2785907B1 (fr) * | 1998-11-13 | 2001-01-05 | Inst Francais Du Petrole | Procede et dispositif de craquage catalytique comprenant des reacteurs a ecoulements descendant et ascendant |
| FR2802211B1 (fr) * | 1999-12-14 | 2002-02-01 | Inst Francais Du Petrole | Procede et dispositif de craquage catalytique comprenant en parallele au moins un reacteur a ecoulement ascendant et au moins un reacteur a ecoulement descendant |
| US20010042702A1 (en) * | 2000-04-17 | 2001-11-22 | Stuntz Gordon F. | Cycle oil conversion process |
| FR2811327B1 (fr) * | 2000-07-05 | 2002-10-25 | Total Raffinage Distribution | Procede et dispositif de craquage d'hydrocarbures mettant en oeuvre deux chambres reactionnelles successives |
| US20020195373A1 (en) * | 2001-06-07 | 2002-12-26 | Takashi Ino | Heavy oil fluid catalytic cracking process |
| US6656346B2 (en) * | 2001-06-07 | 2003-12-02 | King Fahd University Of Petroleum And Minerals | Fluid catalytic cracking process for heavy oil |
| US6866771B2 (en) * | 2002-04-18 | 2005-03-15 | Uop Llc | Process and apparatus for upgrading FCC product with additional reactor with catalyst recycle |
| KR100939503B1 (ko) * | 2002-04-26 | 2010-01-29 | 차이나 페트로리움 앤드 케미컬 코포레이션 | 하향류 접촉분해 반응기 및 이의 용도 |
| EP1542796A1 (en) * | 2002-08-29 | 2005-06-22 | Albemarle Netherlands B.V. | Catalyst for the production of light olefins |
| US7087154B2 (en) * | 2002-12-30 | 2006-08-08 | Petroleo Brasileiro S.A. - Petrobras | Apparatus and process for downflow fluid catalytic cracking |
| US7144498B2 (en) * | 2004-01-30 | 2006-12-05 | Kellogg Brown & Root Llc | Supercritical hydrocarbon conversion process |
| CN100564486C (zh) * | 2004-02-10 | 2009-12-02 | 巴西石油公司 | 下流式流化催化裂化装置与方法 |
| WO2006020547A1 (en) | 2004-08-10 | 2006-02-23 | Shell Internationale Research Maatschappij B.V. | Method and apparatus for making a middle distillate product and lower olefins from a hydrocarbon feedstock |
| US20080011644A1 (en) * | 2006-07-13 | 2008-01-17 | Dean Christopher F | Ancillary cracking of heavy oils in conjuction with FCC unit operations |
-
2006
- 2006-07-13 US US11/487,011 patent/US20080011644A1/en not_active Abandoned
-
2007
- 2007-07-11 KR KR1020097002699A patent/KR101447299B1/ko not_active Expired - Fee Related
- 2007-07-11 EA EA200900186A patent/EA014574B1/ru not_active IP Right Cessation
- 2007-07-11 CA CA2657615A patent/CA2657615C/en not_active Expired - Fee Related
- 2007-07-11 WO PCT/US2007/015950 patent/WO2008008470A2/en not_active Ceased
- 2007-07-11 BR BRPI0713238-7A2A patent/BRPI0713238A2/pt not_active Application Discontinuation
- 2007-07-11 EP EP07796837A patent/EP2046919A4/en not_active Ceased
- 2007-07-11 CN CN200780026613.0A patent/CN101743292B/zh not_active Expired - Fee Related
- 2007-07-11 JP JP2009519539A patent/JP5436209B2/ja not_active Expired - Fee Related
- 2007-07-11 MX MX2009000383A patent/MX2009000383A/es active IP Right Grant
-
2009
- 2009-01-12 NO NO20090153A patent/NO20090153L/no not_active Application Discontinuation
-
2011
- 2011-05-19 US US13/111,437 patent/US8877042B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2008008470A2 (en) | 2008-01-17 |
| CA2657615C (en) | 2013-07-02 |
| US20080011644A1 (en) | 2008-01-17 |
| JP2009543898A (ja) | 2009-12-10 |
| WO2008008470A8 (en) | 2009-03-19 |
| CA2657615A1 (en) | 2008-01-17 |
| NO20090153L (no) | 2009-04-02 |
| US20110226668A1 (en) | 2011-09-22 |
| EP2046919A4 (en) | 2012-09-05 |
| WO2008008470A3 (en) | 2008-03-13 |
| EA200900186A1 (ru) | 2009-10-30 |
| EA014574B1 (ru) | 2010-12-30 |
| CN101743292A (zh) | 2010-06-16 |
| US8877042B2 (en) | 2014-11-04 |
| MX2009000383A (es) | 2009-08-18 |
| BRPI0713238A2 (pt) | 2014-10-29 |
| KR101447299B1 (ko) | 2014-10-06 |
| CN101743292B (zh) | 2014-12-03 |
| EP2046919A2 (en) | 2009-04-15 |
| KR20090069266A (ko) | 2009-06-30 |
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