JP5415448B2 - キラルイミンのジアステレオ選択的転化方法 - Google Patents

キラルイミンのジアステレオ選択的転化方法 Download PDF

Info

Publication number
JP5415448B2
JP5415448B2 JP2010538580A JP2010538580A JP5415448B2 JP 5415448 B2 JP5415448 B2 JP 5415448B2 JP 2010538580 A JP2010538580 A JP 2010538580A JP 2010538580 A JP2010538580 A JP 2010538580A JP 5415448 B2 JP5415448 B2 JP 5415448B2
Authority
JP
Japan
Prior art keywords
alkyl
formula
copper
catalyst
mass
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2010538580A
Other languages
English (en)
Japanese (ja)
Other versions
JP2011507814A (ja
JP2011507814A5 (https=
Inventor
ジーゲル ヴォルフガング
ハーン ティロ
シュテープ トビアス
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2011507814A publication Critical patent/JP2011507814A/ja
Publication of JP2011507814A5 publication Critical patent/JP2011507814A5/ja
Application granted granted Critical
Publication of JP5415448B2 publication Critical patent/JP5415448B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/52—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of imines or imino-ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2010538580A 2007-12-21 2008-12-10 キラルイミンのジアステレオ選択的転化方法 Expired - Fee Related JP5415448B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07150290.0 2007-12-21
EP07150290 2007-12-21
PCT/EP2008/067191 WO2009080511A1 (de) 2007-12-21 2008-12-10 Verfahren zur diastereoselektiven umsetzung von chiralen iminen

Publications (3)

Publication Number Publication Date
JP2011507814A JP2011507814A (ja) 2011-03-10
JP2011507814A5 JP2011507814A5 (https=) 2013-11-07
JP5415448B2 true JP5415448B2 (ja) 2014-02-12

Family

ID=40347974

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2010538580A Expired - Fee Related JP5415448B2 (ja) 2007-12-21 2008-12-10 キラルイミンのジアステレオ選択的転化方法

Country Status (7)

Country Link
US (1) US8354558B2 (https=)
EP (1) EP2234958B1 (https=)
JP (1) JP5415448B2 (https=)
KR (1) KR20100108393A (https=)
CN (1) CN101903329B (https=)
CA (1) CA2707813A1 (https=)
WO (1) WO2009080511A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0922984B1 (pt) 2008-12-19 2017-10-24 Basf Se Process for preparing pure triethanolamine
JP5847386B2 (ja) * 2010-09-15 2016-01-20 関東化學株式会社 アミン化合物の製造方法
US9259715B2 (en) 2012-10-17 2016-02-16 Archer Daniels Midland Company Hydrogenolysis catalysts and uses thereof
CN109942506B (zh) * 2019-03-27 2020-12-29 上海交通大学 不对称镍催化氢化n-磺酰亚胺制备手性胺的方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3717111C2 (de) 1986-05-22 1996-02-22 Basf Ag Kupferoxid, Zinkoxid und Aluminiumoxid enthaltender Katalysator zur Tieftemperaturkonvertierung
DE3904083A1 (de) 1989-02-11 1990-08-16 Basf Ag Kobaltkatalysatoren
JP2818958B2 (ja) * 1990-02-23 1998-10-30 塩野義製薬株式会社 ４―（４―アルコキシフェニル）―２―ブチルアミン誘導体およびその製造法
DE4428004A1 (de) 1994-08-08 1996-02-15 Basf Ag Verfahren zur Herstellung von Aminen
ES2217748T3 (es) * 1998-03-18 2004-11-01 Ciba Specialty Chemicals Holding Inc. Procedimiento para la hidrogenacin catalitica cis-selectiva de ciclohexilidenaminas.
DE19826396A1 (de) 1998-06-12 1999-12-16 Basf Ag Verfahren zur Herstellung von Aminen
ATE264831T1 (de) 1999-07-29 2004-05-15 Ciba Sc Holding Ag Verfahren zur cis-selektiven katalytischen hydrierung von cyclohexylidenaminen
JP3830727B2 (ja) * 2000-05-11 2006-10-11 セントラル硝子株式会社 光学活性α−メチル−ビス−３，５−（トリフルオロメチル）ベンジルアミンの製造方法
JP3982991B2 (ja) * 2000-12-04 2007-09-26 セントラル硝子株式会社 光学活性１−（トリフルオロメチルモノ置換フェニル）エチルアミンの製造方法
JP4287703B2 (ja) * 2003-06-11 2009-07-01 セントラル硝子株式会社 光学活性１−アルキル置換−２，２，２−トリフルオロエチルアミンの製造方法
JP4606041B2 (ja) * 2004-03-05 2011-01-05 セントラル硝子株式会社 光学活性１−アリール−２−フルオロ置換エチルアミン類およびその製造方法
CN1989097A (zh) * 2004-07-22 2007-06-27 帝斯曼知识产权资产管理有限公司 用于制备非对映异构体富集的化合物的方法
EP1640358A1 (en) 2004-09-15 2006-03-29 International University Bremen Gmbh Synthesis of amine stereoisomers

Also Published As

Publication number Publication date
US8354558B2 (en) 2013-01-15
CN101903329B (zh) 2014-11-05
JP2011507814A (ja) 2011-03-10
EP2234958A1 (de) 2010-10-06
CA2707813A1 (en) 2009-07-02
KR20100108393A (ko) 2010-10-06
US20100274053A1 (en) 2010-10-28
CN101903329A (zh) 2010-12-01
WO2009080511A1 (de) 2009-07-02
EP2234958B1 (de) 2013-09-18

Similar Documents

Publication Publication Date Title
KR102800555B1 (ko) 4-아미노-피리다진의 제조 방법
KR20090045920A (ko) 방향족 시클로프로판 에스테르 및 아미드의 화학적 제조 방법
JP5415448B2 (ja) キラルイミンのジアステレオ選択的転化方法
JPWO2014115801A1 (ja) α，α−ジフルオロアセトアルデヒドの製造方法
WO2013133208A1 (ja) テトラヒドロフラン化合物の製造方法
US11465977B2 (en) Process for the preparation of sphingosine-1-phosphate receptor agonist
WO2013018573A1 (ja) α－フルオロアルデヒド類の製造方法
EP2436665B1 (en) Process for producing vinyl ether
CN116768738B (zh) 一种烯丙基芳胺类化合物及其制备方法和应用
US8729320B2 (en) Method for producing difluorocyclopropane compound
CN110520403B (zh) α,α-二氟乙醛半缩醛的制造方法
JP7619730B2 (ja) アルキルシリルオキシ置換ベンジルアミン化合物の製造方法
JP7161275B2 (ja) ４－アミノ－ピリダジンを製造するための方法
JP5115762B2 (ja) ４−ホルミルピペリジンアセタール誘導体の製造方法
RU2778306C1 (ru) Способ получения 4-аминопиридазинов
JP4237565B2 (ja) 光学活性二級アルコール化合物の製造方法
JP4923698B2 (ja) ４−アミノテトラヒドロピラン化合物の製法
KR20190100913A (ko) 알코올 화합물의 제조법

Legal Events

Date Code Title Description
RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20101228

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20111207

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20111207

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20130509

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130520

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20130819

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130826

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20130920

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20131015

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20131113

LAPS Cancellation because of no payment of annual fees