JP5364100B2 - 温度制御装置 - Google Patents
温度制御装置 Download PDFInfo
- Publication number
- JP5364100B2 JP5364100B2 JP2010530392A JP2010530392A JP5364100B2 JP 5364100 B2 JP5364100 B2 JP 5364100B2 JP 2010530392 A JP2010530392 A JP 2010530392A JP 2010530392 A JP2010530392 A JP 2010530392A JP 5364100 B2 JP5364100 B2 JP 5364100B2
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- JP
- Japan
- Prior art keywords
- reactor
- temperature
- calorimeter
- coolant
- cooling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K17/00—Measuring quantity of heat
- G01K17/04—Calorimeters using compensation methods, i.e. where the absorbed or released quantity of heat to be measured is compensated by a measured quantity of heating or cooling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4806—Details not adapted to a particular type of sample
- G01N25/4826—Details not adapted to a particular type of sample concerning the heating or cooling arrangements
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4806—Details not adapted to a particular type of sample
- G01N25/4826—Details not adapted to a particular type of sample concerning the heating or cooling arrangements
- G01N25/4833—Details not adapted to a particular type of sample concerning the heating or cooling arrangements specially adapted for temperature scanning
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/11—Automated chemical analysis
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/11—Automated chemical analysis
- Y10T436/115831—Condition or time responsive
Description
101、301 試料
102、302、402 反応器加熱装置
103、303、403 熱電冷却素子
104、304、404 冷却剤
105、305、405 制御および/または調節ユニット
106 熱流
307、407 反応器
308、408 撹拌器
309、409 反応器ジャケット
310 温度制御媒体
311 連結器
312、412 撹拌器モータ
313 冷却器
314、414 導管、回路
315 連結器、連結器ポート
116、316、416 温度センサ
317 導管
319 冷却装置
320 回路
421 反応器の蓋
422 絶縁体
423 筺体
325、425 較正加熱器、加熱素子
526 熱量計
Claims (12)
- 試料(301)を受け入れるための少なくとも1つの反応器(307、407)と、前記反応器(307、407)を包囲する反応器ジャケット(309、409)と、温度制御装置とを備え、前記温度制御装置は、反応器加熱装置(302、402)および反応器冷却装置とを備えるとともに、反応器の内部温度を調節するように働き、前記反応器冷却装置が、冷却剤(304、404)に熱的に連結された熱電冷却素子(303、403)を含む、熱量計であって、前記反応器冷却装置および前記反応器加熱装置(302、402)が、個々のユニットであり、そのいずれもが、前記反応器ジャケット(309、409)を介して前記反応器(307、407)に熱的に連結され、前記冷却剤は、前記反応器の内部温度から独立したほぼ一定の入口温度を有することを特徴とする、熱量計。
- 制御ユニット(305、405)と、温度センサ(316、416)とをさらに備え、前記温度センサ(316、416)が、前記反応器(307、407)に配置され、実際の反応器温度を測定するように働き、前記制御ユニット(305、405)が、前記反応器加熱装置(302、402)および前記反応器冷却装置の能力を調節するための少なくとも1つの作動プログラムを含み、前記実際の反応器温度を所与の反応器設定温度に調整する少なくとも1つの温度制御プログラムをさらに含む、請求項1に記載の熱量計。
- 前記作動プログラムが、前記反応器設定温度の時間最適化されたおよび/または能力最適化された調整のために設計されることを特徴とする、請求項1または2に記載の熱量計。
- 前記熱電冷却素子(303、403)が、DC電圧で作動され熱を前記反応器(307、407)から前記冷却剤(304、404)に導く少なくとも1つのペルチェ素子を含むことを特徴とする、請求項1から3の一項に記載の熱量計。
- 前記熱電冷却素子(403)が、個々の単段ペルチェ素子であることを特徴とする、請求項4に記載の熱量計。
- さらに、前記冷却剤(304)を備えた冷却器(313)を備え、前記冷却剤(304)は、前記反応器の内部温度から独立したほぼ一定の入口温度を有し、前記反応器冷却装置と共働することを特徴とする、請求項1から5の一項に記載の熱量計。
- さらに、前記制御ユニット(305、405)によってその能力が調節される、前記反応器(207、307、407)内に配置された加熱素子(325、425)を含むことを特徴とする、請求項1から6の一項に記載の熱量計。
- 前記反応器加熱装置(302、402)が、前記反応器ジャケット(309、409)と前記反応器冷却装置の間に配置されることを特徴とする、請求項1から7の一項に記載の熱量計。
- 前記反応器ジャケット(409)が、実質的に、高い熱伝導率を有する材料ブロックであることを特徴とする、請求項1から8の一項に記載の熱量計。
- 前記反応器ジャケット(309)が2重壁の反応器ジャケットであり、前記2重壁の反応器ジャケットは、前記反応器(307)のための空洞を有し、温度制御媒体(310)が充填されることを特徴とする、請求項1から7の一項に記載の熱量計。
- 共用の制御ユニットを用いて反応器の内部温度が互いに独立して調節され得る少なくとも2つの反応器を備え、前記反応器の各々が、反応器加熱装置および反応器冷却装置に熱的に連結されていることを特徴とする、請求項1から10の一項に記載の熱量計。
- 請求項1から11の一項に記載の熱量計または反応熱量計を備えた熱分析機器のための温度制御装置であって、反応器加熱装置(102、302、402)と、反応器冷却装置と、制御ユニット(105、305、405)とを備え、前記反応器冷却装置が、冷却剤(104、304、404)に熱的に連結された少なくとも1つの熱電冷却素子(103、303、403)を含む温度制御装置であって、前記反応器冷却装置および前記反応器加熱装置(102、302、402)が、互いに分離された個々のユニットであり、前記冷却剤(104、304、404)が、前記反応器の内部温度から独立したほぼ一定の入口温度を有することを特徴とする、温度制御装置。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP07119294.2A EP2053371B1 (de) | 2007-10-25 | 2007-10-25 | Thermostat |
EP07119294.2 | 2007-10-25 | ||
PCT/EP2008/063364 WO2009053237A1 (de) | 2007-10-25 | 2008-10-07 | Einrichtung zur temperaturkontrolle |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2011504580A JP2011504580A (ja) | 2011-02-10 |
JP5364100B2 true JP5364100B2 (ja) | 2013-12-11 |
Family
ID=39217908
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2010530392A Active JP5364100B2 (ja) | 2007-10-25 | 2008-10-07 | 温度制御装置 |
Country Status (5)
Country | Link |
---|---|
US (1) | US8815601B2 (ja) |
EP (2) | EP2053371B1 (ja) |
JP (1) | JP5364100B2 (ja) |
CN (1) | CN101842679B (ja) |
WO (1) | WO2009053237A1 (ja) |
Families Citing this family (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102007057463B3 (de) * | 2007-11-29 | 2009-04-16 | Ika-Werke Gmbh & Co. Kg | Kalorimeter mit einem Aufschlussbehälter und mit einem Wassermantel |
EP2133676B1 (de) * | 2008-06-13 | 2013-03-13 | Mettler-Toledo AG | Kalorimetrisches Verfahren |
JP5585131B2 (ja) * | 2010-03-12 | 2014-09-10 | いすゞ自動車株式会社 | 発熱量測定容器 |
KR101228571B1 (ko) * | 2010-10-05 | 2013-02-01 | 조후갑 | 열전소자를 포함하는 가스하이드레이트 반응기 |
CN102156009B (zh) * | 2011-03-31 | 2012-08-08 | 中国科学院化学研究所 | 一种热功率测量装置 |
DE102011016956B3 (de) * | 2011-04-13 | 2012-08-09 | Ika-Werke Gmbh & Co. Kg | Verfahren und Vorrichtung zum Kühlen eines Aufschlussbehälters eines Kalorimeters nach einer Benutzung |
CN102435352B (zh) * | 2011-09-13 | 2013-05-29 | 中国航天科工集团第二研究院二〇三所 | 一种微波功率量热计的控制及采集装置 |
US9398640B2 (en) * | 2012-12-21 | 2016-07-19 | Halliburton Energy Services, Inc. | Digital multi-use thermo-cup |
KR101331210B1 (ko) * | 2013-02-28 | 2013-11-20 | 이익재 | 가열장치와 냉각장치를 구비한 전두부 제조시스템 및 전두부 제조방법 |
KR102068741B1 (ko) | 2013-06-04 | 2020-01-22 | 삼성디스플레이 주식회사 | 다결정 규소막의 검사 방법 |
FR3007133B1 (fr) | 2013-06-18 | 2016-06-10 | Centre Nat Rech Scient | Dispositif et procede d'analyse thermique et calorimetrique differentielle d'echantillons de volumes importants pour la caracterisation thermodynamique de materiaux a changement de phase |
US9593988B1 (en) | 2013-07-23 | 2017-03-14 | Calmetrix, Inc. | Systems and methods of thermal energy measurement |
FR3012880B1 (fr) * | 2013-11-07 | 2023-01-13 | Centre Nat Rech Scient | Calorimetre a temperature stabilisee. |
WO2015158170A1 (zh) * | 2014-04-14 | 2015-10-22 | 哈尔滨工业大学 | 一种基于原位解耦的气固反应分析装置及分析方法 |
CN104316221B (zh) * | 2014-11-14 | 2017-04-12 | 陕西电器研究所 | 接触式高温温度传感器校准装置 |
CN104964765B (zh) * | 2015-07-15 | 2017-08-15 | 青岛科技大学 | 一种低临界温度液体混合过量焓的变温补偿量热装置 |
DE102015112255A1 (de) * | 2015-07-28 | 2017-02-02 | SIKA Dr. Siebert & Kühn GmbH & Co. KG | Temperaturkalibrator und Verfahren zum Temperieren eines Temperaturkalibrators |
US20200182852A1 (en) * | 2017-07-06 | 2020-06-11 | M-I L.L.C. | Automated Analysis of Drilling Fluid |
CN108195722A (zh) * | 2017-11-21 | 2018-06-22 | 国家电网公司 | 基于绝缘油界面张力检测的自动温控装置 |
CN112601953A (zh) | 2018-08-23 | 2021-04-02 | 沃特世科技公司 | 多样品差示扫描量热仪 |
US11643898B2 (en) | 2018-10-17 | 2023-05-09 | Schlumberger Technology Corporation | Systems and methods for monitoring and/or predicting sagging tendencies of fluids |
CN109540960B (zh) * | 2018-10-22 | 2020-07-28 | 西安交通大学 | 一种用于测量物质比热容和相变潜热的装置及方法 |
RU2707665C1 (ru) * | 2018-11-26 | 2019-11-28 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский государственный университет имени М.В. Ломоносова" (МГУ) | Термостатирующее устройство для проведения нанокалориметрических измерений в контролируемой атмосфере |
US20210096092A1 (en) * | 2019-09-30 | 2021-04-01 | Saudi Arabian Oil Company | Systems and Methods for High Temperature, High Pressure Isothermal Calorimetry |
CN110987242B (zh) * | 2019-12-17 | 2021-02-02 | 厦门标安科技有限公司 | 一种反应量热器的端盖改进结构 |
EP4078161A1 (en) * | 2019-12-20 | 2022-10-26 | TA Instruments-Waters LLC | Heat flow rate determination for a single sample differential scanning calorimeter |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4178800A (en) * | 1976-09-22 | 1979-12-18 | Christoph Thomann | Method of and apparatus for the measuring of quantities of heat |
CH651392A5 (de) * | 1980-06-10 | 1985-09-13 | Ciba Geigy Ag | Waermeflusskalorimeter. |
US5813763A (en) * | 1996-10-11 | 1998-09-29 | Microcal Incorporated | Ultrasensitive differential microcalorimeter |
JP3620981B2 (ja) * | 1998-11-17 | 2005-02-16 | 株式会社リガク | 試料温度制御方法 |
DE10010291A1 (de) * | 2000-03-02 | 2001-09-06 | Reineke Mes Und Regeltechnik G | Verfahren und Kalorimeter zur kalorimetrischen Bestimmung des Brennwertes von Gasen |
EP1184649A1 (de) * | 2000-09-04 | 2002-03-06 | Eidgenössische Technische Hochschule Zürich | Kalorimeter |
WO2003025528A2 (en) * | 2001-09-18 | 2003-03-27 | Energetic Geonomics Corporation | A high throughput energy array |
-
2007
- 2007-10-25 EP EP07119294.2A patent/EP2053371B1/de active Active
-
2008
- 2008-10-07 CN CN2008801128931A patent/CN101842679B/zh active Active
- 2008-10-07 WO PCT/EP2008/063364 patent/WO2009053237A1/de active Application Filing
- 2008-10-07 JP JP2010530392A patent/JP5364100B2/ja active Active
- 2008-10-07 EP EP08841684A patent/EP2205954A1/de not_active Withdrawn
-
2010
- 2010-04-26 US US12/767,019 patent/US8815601B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
WO2009053237A4 (de) | 2009-06-25 |
CN101842679B (zh) | 2012-09-12 |
EP2205954A1 (de) | 2010-07-14 |
EP2053371A1 (de) | 2009-04-29 |
JP2011504580A (ja) | 2011-02-10 |
US8815601B2 (en) | 2014-08-26 |
WO2009053237A1 (de) | 2009-04-30 |
EP2053371B1 (de) | 2017-11-29 |
CN101842679A (zh) | 2010-09-22 |
US20100255588A1 (en) | 2010-10-07 |
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