JP4927527B2 - 沈降シリカ生成物、それらを含む歯磨き剤および方法 - Google Patents
沈降シリカ生成物、それらを含む歯磨き剤および方法 Download PDFInfo
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- JP4927527B2 JP4927527B2 JP2006503477A JP2006503477A JP4927527B2 JP 4927527 B2 JP4927527 B2 JP 4927527B2 JP 2006503477 A JP2006503477 A JP 2006503477A JP 2006503477 A JP2006503477 A JP 2006503477A JP 4927527 B2 JP4927527 B2 JP 4927527B2
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- 239000000551 dentifrice Substances 0.000 title claims description 64
- 238000000034 method Methods 0.000 title claims description 48
- 229960001927 cetylpyridinium chloride Drugs 0.000 claims description 76
- YMKDRGPMQRFJGP-UHFFFAOYSA-M cetylpyridinium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YMKDRGPMQRFJGP-UHFFFAOYSA-M 0.000 claims description 76
- 239000011148 porous material Substances 0.000 claims description 50
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- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 20
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Images
Classifications
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3045—Treatment with inorganic compounds
- C09C1/3054—Coating
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/16—Pore diameter
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Chemical & Material Sciences (AREA)
- Birds (AREA)
- Organic Chemistry (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
- Silicon Compounds (AREA)
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| US10/366,604 US6946119B2 (en) | 2003-02-14 | 2003-02-14 | Precipitated silica product with low surface area, dentifrices containing same, and processes |
| US10/366,604 | 2003-02-14 | ||
| US10/677,294 US7255852B2 (en) | 2003-02-14 | 2003-10-03 | Precipitated silica product, dentifrices containing same, and processes |
| US10/677,294 | 2003-10-03 | ||
| PCT/US2004/003955 WO2004073539A2 (en) | 2003-02-14 | 2004-02-09 | Precipitated silica product, dentrifices containing same, and processes |
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| JP2007524555A JP2007524555A (ja) | 2007-08-30 |
| JP2007524555A5 JP2007524555A5 (https=) | 2010-11-25 |
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| JP2006503570A Expired - Fee Related JP5025259B2 (ja) | 2003-02-14 | 2004-02-10 | 表面積が低い沈降シリカ生成物、それらを含む歯磨き剤および方法 |
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| EP (1) | EP1596817B1 (https=) |
| JP (2) | JP4927527B2 (https=) |
| WO (1) | WO2004073380A2 (https=) |
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| WO2004007366A1 (ja) * | 2002-07-10 | 2004-01-22 | Tokuyama Corporation | 易分散性沈降シリカのケーク及びその製造方法 |
| DE102004005411A1 (de) * | 2004-02-03 | 2005-08-18 | Degussa Ag | Hydrophobe Fällungskieselsäure für Entschäumerformulierungen |
| US7306788B2 (en) * | 2004-11-24 | 2007-12-11 | J.M. Huber Corporation | High-cleaning/moderate abrasive silica materials and dentifrice containing such materials |
| US7267814B2 (en) * | 2004-11-24 | 2007-09-11 | J.M. Huber Corporation | High-cleaning/low abrasive silica and materials and dentifrice containing such materials |
| US7303742B2 (en) * | 2004-11-24 | 2007-12-04 | J.M. Huber Corporation | Viscosity-modifying silica materials that exhibit low cleaning and abrasive levels and dentifrices thereof |
| US7731110B2 (en) * | 2005-06-29 | 2010-06-08 | J.M. Huber Corporation | Method for making precipitated silica compositions and products thereof |
| US20070014740A1 (en) | 2005-07-15 | 2007-01-18 | Colgate-Palmolive Company | Oral compositions having cationic active ingredients |
| ATE487458T1 (de) * | 2005-09-29 | 2010-11-15 | Dentsply Int Inc | Verfahren zur verwendung von dentalzusammensetzungen mit fluoreszierenden mitteln |
| US20080160053A1 (en) * | 2006-12-27 | 2008-07-03 | Mcgill Patrick | High electrolyte additions for precipitated silica material production |
| US7438895B2 (en) * | 2006-12-27 | 2008-10-21 | J.M. Huber Corporation | Precipitated silica materials exhibiting high compatibility with cetylpyridinium chloride |
| US20080314872A1 (en) * | 2007-06-19 | 2008-12-25 | Ferro Corporation | Chemical-Mechanical Polishing Compositions Containing Aspartame And Methods Of Making And Using The Same |
| FR2928363B1 (fr) * | 2008-03-10 | 2012-08-31 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, silices precipitees a morphologie, granulometrie et porosite particulieres et leurs utilisations, notamment pour le renforcement de polymeres |
| US20090297459A1 (en) * | 2008-06-03 | 2009-12-03 | Duen-Wu Hua | Transparent silica gel/precipitated silica composite materials for dentifrices |
| US8211407B2 (en) * | 2008-11-25 | 2012-07-03 | The Procter & Gamble Company | Method of making oral care compositions with fused silica slurries |
| US8551457B2 (en) | 2008-11-25 | 2013-10-08 | The Procter & Gamble Company | Oral care compositions comprising spherical fused silica |
| DE102009001512A1 (de) * | 2009-03-12 | 2010-09-16 | Evonik Degussa Gmbh | Herstellung von hochreinen Suspensionen enthaltend gefällte Kieselsäuren durch Elektrodialyse |
| AR079182A1 (es) * | 2009-06-16 | 2012-01-04 | Grace W R & Co | Oxidos metalicos cationico - compatibles y composiciones para cuidado bucodental que contienen los oxidos metalicos |
| US11052029B2 (en) * | 2009-06-16 | 2021-07-06 | W. R. Grace & Co.-Conn. | Cation compatible metal oxides and oral care compositions containing the metal oxides |
| US8609068B2 (en) | 2010-02-24 | 2013-12-17 | J.M. Huber Corporation | Continuous silica production process and silica product prepared from same |
| WO2011150004A2 (en) | 2010-05-25 | 2011-12-01 | The Procter & Gamble Company | Oral care compositions and methods of making oral care compositions comprising silica from plant materials |
| US9028605B2 (en) | 2011-02-25 | 2015-05-12 | J.M. Huber Corporation | Coating compositions comprising spheroid silica or silicate |
| US9155310B2 (en) | 2011-05-24 | 2015-10-13 | Agienic, Inc. | Antimicrobial compositions for use in products for petroleum extraction, personal care, wound care and other applications |
| EP2713747B1 (en) | 2011-05-24 | 2023-02-22 | Agienic, Inc. | Compositions and methods for antimicrobial metal nanoparticles |
| CN103930091B (zh) * | 2011-09-01 | 2016-03-02 | 宝洁公司 | 具有改善的流变特性的口腔护理组合物 |
| JP2015535262A (ja) | 2012-11-05 | 2015-12-10 | ザ プロクター アンド ギャンブルカンパニー | 熱処理沈殿シリカ |
| US10208241B2 (en) | 2012-11-26 | 2019-02-19 | Agienic, Inc. | Resin coated proppants with antimicrobial additives |
| US11352551B2 (en) | 2012-11-26 | 2022-06-07 | Agienic, Inc. | Proppant coatings containing antimicrobial agents |
| JP5868310B2 (ja) * | 2012-12-11 | 2016-02-24 | 合同会社地球環境・麦飯石研究所 | 歯垢除去剤 |
| US20140271900A1 (en) * | 2013-03-15 | 2014-09-18 | J.M. Huber Corporation | High Cleaning Silica with Low Abrasion and Method for Making Same |
| CN103274422B (zh) * | 2013-05-31 | 2016-03-30 | 肇庆金三江硅材料有限公司 | 核壳型沉淀二氧化硅、制备方法及含有该二氧化硅的牙膏 |
| CN111544320A (zh) * | 2013-06-24 | 2020-08-18 | 宝洁公司 | 指示正确牙齿清洁的口腔组合物 |
| CN104276577B (zh) * | 2014-09-22 | 2016-08-24 | 无锡恒诚硅业有限公司 | 一种具有颗粒均一性的沉淀二氧化硅、制备方法及其用途 |
| CA2999039C (en) * | 2015-09-28 | 2023-08-29 | Evonik Degussa Gmbh | Silica-based antimicrobial oral compositions |
| WO2017145142A1 (en) * | 2016-02-25 | 2017-08-31 | Nobio Ltd. | Micro and nanoparticulate compositions comprising anti-microbially active groups |
| EP3435957A1 (en) | 2016-04-01 | 2019-02-06 | The Procter and Gamble Company | Oral care compositions containing gel networks and potassium nitrate |
| AU2017240034B2 (en) | 2016-04-01 | 2020-02-06 | The Procter & Gamble Company | Oral care compositions containing a gel network phase |
| CA3018559A1 (en) | 2016-04-01 | 2017-10-05 | The Procter & Gamble Company | Oral care compositions with an effective flavor display |
| BR112018069874A2 (pt) | 2016-04-01 | 2019-02-05 | Procter & Gamble | composições para tratamento bucal contendo uma fase de rede de gel e nitrato de potássio |
| AU2017240683B2 (en) | 2016-04-01 | 2020-01-16 | The Procter & Gamble Company | Oral care compositions containing potassium nitrate and peroxide |
| US11173471B2 (en) * | 2016-11-24 | 2021-11-16 | Universidad De Los Andes | Oxygen-absorbent composition comprising a silica matrix that encapsulates fatty acids, unsaturated esters or compounds containing same, and method for producing said composition |
| US12037252B2 (en) | 2016-12-19 | 2024-07-16 | Evonik Operations Gmbh | Stannous compatible silica |
| ES3042132T3 (en) | 2016-12-19 | 2025-11-18 | Evonik Operations Gmbh | Dentifrice compositions containing stannous compatible silica particles |
| US11548788B2 (en) | 2017-08-28 | 2023-01-10 | Evonik Operations Gmbh | Spherical silica for tubule occlusion |
| MX2020002217A (es) | 2017-08-29 | 2020-08-20 | Evonik Operations Gmbh | Tamaño de partícula esférica de sílice para control de rda. |
| CN111447912B (zh) | 2017-12-15 | 2023-06-23 | 高露洁-棕榄公司 | 具有高氟化亚锡相容性的二氧化硅磨料 |
| CN108383130A (zh) * | 2018-05-04 | 2018-08-10 | 福建远翔新材料股份有限公司 | 一种沉淀水合二氧化硅的合成方法 |
| CA3102893A1 (en) | 2018-06-12 | 2019-12-19 | Evonik Operations Gmbh | Spherical stannous compatible silica particles for reduced rda |
| CN113164337A (zh) * | 2018-12-04 | 2021-07-23 | 宝洁公司 | 具有改善的锡相容性的口腔护理组合物 |
| US11041095B2 (en) * | 2019-05-22 | 2021-06-22 | Kraton Polymers Llc | Desulfurized tall oil and derivatives thereof |
| JP7316177B2 (ja) * | 2019-10-03 | 2023-07-27 | 東ソー・シリカ株式会社 | 含水ケイ酸スラリー及びその製造方法 |
| CN111017933B (zh) * | 2020-01-13 | 2021-09-03 | 福建省三明正元化工有限公司 | 一种高比表面积二氧化硅的制备方法 |
| US11279849B2 (en) | 2020-05-21 | 2022-03-22 | Kraton Polymers Llc | Deodorized rosin ester and methods for making |
| CA3138558C (en) | 2020-11-16 | 2024-01-30 | Church & Dwight Co., Inc. | Teeth cleaning composition comprising banana extract |
| KR20230138530A (ko) * | 2021-02-11 | 2023-10-05 | 에보니크 오퍼레이션즈 게엠베하 | 무정형 비-다공성 실리카 |
| US12589061B2 (en) | 2021-05-04 | 2026-03-31 | Momentive Performance Materials Japan Llc | Method for producing silica particles and their use in cosmetic compositions |
| FI4452848T3 (fi) | 2021-12-20 | 2025-12-18 | Evonik Operations Gmbh | Saostettu piidioksidi ja siihen liittyvät menetelmät |
| WO2024100081A1 (en) | 2022-11-08 | 2024-05-16 | Evonik Operations Gmbh | Precipitated silica and methods thereof |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2601235A (en) | 1949-06-15 | 1952-06-24 | Du Pont | Process for producing built-up silica particles |
| US2731326A (en) | 1951-08-31 | 1956-01-17 | Du Pont | Process of preparing dense amorphous silica aggregates and product |
| US2885366A (en) | 1956-06-28 | 1959-05-05 | Du Pont | Product comprising a skin of dense, hydrated amorphous silica bound upon a core of another solid material and process of making same |
| GB8604985D0 (en) | 1986-02-28 | 1986-04-09 | Unilever Plc | Precipitated silicas |
| FR2622439B1 (fr) * | 1987-11-04 | 1991-07-12 | Rhone Poulenc Chimie | Silice pour compositions dentifrices compatible notamment avec la chlorhexidine |
| US5286478A (en) | 1987-11-04 | 1994-02-15 | Rhone-Poulenc Chimie | Dentifrice-compatible silica particulates |
| FR2649089B1 (fr) * | 1989-07-03 | 1991-12-13 | Rhone Poulenc Chimie | Silice a porosite controlee et son procede d'obtention |
| JPH03127718A (ja) * | 1989-10-11 | 1991-05-30 | Beecham Group Plc | 組成物 |
| JPH0684294B2 (ja) | 1990-05-29 | 1994-10-26 | サンスター株式会社 | 口腔用組成物 |
| EP0641191A4 (en) * | 1992-05-19 | 1996-08-21 | Grace W R & Co | ORAL CARE COMPOSITIONS WITH IMPROVED COMPATIBILITY THAT CONTAIN MATERIALS BASED ON PEEL EARTH. |
| ATE142170T1 (de) | 1992-10-28 | 1996-09-15 | Crosfield Joseph & Sons | Kieselsäuren |
| US5647903A (en) * | 1995-10-03 | 1997-07-15 | Mcgill; Patrick D. | Microporous high structure precipitated silicas and methods |
| FR2751635B1 (fr) * | 1996-07-23 | 1998-10-02 | Rhone Poulenc Chimie | Silice compatible avec les aromes, son procede de preparation et compositions dentifrices la contenant |
| US5897849A (en) | 1996-12-30 | 1999-04-27 | Uop Llc | Unimodal, large-pore silicas by hydrothermal treatment of silicia powders |
| MY117802A (en) | 1997-06-13 | 2004-08-30 | Mizusawa Industrial Chem | Amorphous silica particles having a double structure, process for producing the same and use |
| NZ511080A (en) | 1998-10-21 | 2003-05-30 | W | Aqueous alkaline (pH 10.8) slurries prepared from slurries with a particle size from 0.1-0.5 microns heated or autoclaved to increase abrasivity |
| US6471948B1 (en) | 2000-03-22 | 2002-10-29 | Church & Dwight Co. Inc. | Toothpaste compositions containing cetylpyridinium chloride |
| US6366522B1 (en) * | 2000-11-20 | 2002-04-02 | Sigmatel, Inc | Method and apparatus for controlling power consumption of an integrated circuit |
-
2003
- 2003-02-14 US US10/366,604 patent/US6946119B2/en not_active Expired - Lifetime
- 2003-10-03 US US10/677,294 patent/US7255852B2/en not_active Expired - Lifetime
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2004
- 2004-02-09 JP JP2006503477A patent/JP4927527B2/ja not_active Expired - Fee Related
- 2004-02-10 WO PCT/US2004/004338 patent/WO2004073380A2/en not_active Ceased
- 2004-02-10 EP EP04709947.8A patent/EP1596817B1/en not_active Expired - Lifetime
- 2004-02-10 JP JP2006503570A patent/JP5025259B2/ja not_active Expired - Fee Related
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|---|---|
| US20040161390A1 (en) | 2004-08-19 |
| US7255852B2 (en) | 2007-08-14 |
| EP1596817A2 (en) | 2005-11-23 |
| US6946119B2 (en) | 2005-09-20 |
| JP5025259B2 (ja) | 2012-09-12 |
| EP1596817A4 (en) | 2008-11-19 |
| JP2006517903A (ja) | 2006-08-03 |
| WO2004073380A3 (en) | 2005-02-03 |
| WO2004073380A2 (en) | 2004-09-02 |
| EP1596817B1 (en) | 2017-03-15 |
| US20040161389A1 (en) | 2004-08-19 |
| JP2007524555A (ja) | 2007-08-30 |
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