JP4705709B2 - 透明な固体シンチレータ材料 - Google Patents

透明な固体シンチレータ材料 Download PDF

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Publication number
JP4705709B2
JP4705709B2 JP2000133934A JP2000133934A JP4705709B2 JP 4705709 B2 JP4705709 B2 JP 4705709B2 JP 2000133934 A JP2000133934 A JP 2000133934A JP 2000133934 A JP2000133934 A JP 2000133934A JP 4705709 B2 JP4705709 B2 JP 4705709B2
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Japan
Prior art keywords
garnet
cubic
host material
gadolinium
scintillator material
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JP2000133934A
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Japanese (ja)
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JP2001072968A (ja
JP2001072968A5 (https=
Inventor
スティーブン・ジュード・ダクロス
オロク・マニー・スリバスタバ
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General Electric Co
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General Electric Co
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent materials, e.g. electroluminescent or chemiluminescent
    • C09K11/08—Luminescent materials, e.g. electroluminescent or chemiluminescent containing inorganic luminescent materials
    • C09K11/77—Luminescent materials, e.g. electroluminescent or chemiluminescent containing inorganic luminescent materials containing rare earth metals
    • C09K11/7766—Luminescent materials, e.g. electroluminescent or chemiluminescent containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
    • C09K11/7767—Chalcogenides
    • C09K11/7769—Oxides
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C04B35/645—Pressure sintering
    • C04B35/6455—Hot isostatic pressing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01T—MEASUREMENT OF NUCLEAR OR X-RADIATION
    • G01T1/00—Measuring X-radiation, gamma radiation, corpuscular radiation, or cosmic radiation
    • G01T1/16—Measuring radiation intensity
    • G01T1/20—Measuring radiation intensity with scintillation detectors
    • G01T1/202—Measuring radiation intensity with scintillation detectors the detector being a crystal
    • G01T1/2023—Selection of materials
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3286—Gallium oxides, gallates, indium oxides, indates, thallium oxides, thallates or oxide forming salts thereof, e.g. zinc gallate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/76—Crystal structural characteristics, e.g. symmetry
    • C04B2235/762—Cubic symmetry, e.g. beta-SiC
    • C04B2235/764—Garnet structure A3B2(CO4)3
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/77—Density
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9646—Optical properties
    • C04B2235/9653—Translucent or transparent ceramics other than alumina
    • G—PHYSICS
    • G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21K—HANDLING OF PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
    • G21K4/00—Conversion screens for the conversion of the spatial distribution of X-rays or particle radiation into visible images, e.g. fluoroscopic screens
    • G21K2004/06—Conversion screens for the conversion of the spatial distribution of X-rays or particle radiation into visible images, e.g. fluoroscopic screens with a phosphor layer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/91—Sintering to produce translucent inorganic article

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Molecular Biology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Luminescent Compositions (AREA)
  • Measurement Of Radiation (AREA)
JP2000133934A 1999-05-06 2000-05-02 透明な固体シンチレータ材料 Expired - Fee Related JP4705709B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/306025 1999-05-06
US09/306,025 US6246744B1 (en) 1999-05-06 1999-05-06 Cubic garnet host with PR activator as a scintillator material

Publications (3)

Publication Number Publication Date
JP2001072968A JP2001072968A (ja) 2001-03-21
JP2001072968A5 JP2001072968A5 (https=) 2007-06-14
JP4705709B2 true JP4705709B2 (ja) 2011-06-22

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Family Applications (1)

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JP2000133934A Expired - Fee Related JP4705709B2 (ja) 1999-05-06 2000-05-02 透明な固体シンチレータ材料

Country Status (3)

Country Link
US (2) US6246744B1 (https=)
JP (1) JP4705709B2 (https=)
DE (1) DE10022018A1 (https=)

Families Citing this family (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6490081B1 (en) 2000-07-28 2002-12-03 The Board Of Trustees Of The Leland Stanford Junior University Method of amplifying optical signals using doped materials with extremely broad bandwidths
JP4683719B2 (ja) * 2000-12-21 2011-05-18 株式会社日立メディコ 酸化物蛍光体及びそれを用いた放射線検出器、並びにｘ線ｃｔ装置
US6630077B2 (en) * 2001-10-11 2003-10-07 General Electric Company Terbium- or lutetium - containing garnet phosphors and scintillators for detection of high-energy radiation
US7008558B2 (en) * 2001-10-11 2006-03-07 General Electric Company Terbium or lutetium containing scintillator compositions having increased resistance to radiation damage
US6661867B2 (en) * 2001-10-19 2003-12-09 Control Screening, Llc Tomographic scanning X-ray inspection system using transmitted and compton scattered radiation
JP2003277191A (ja) * 2002-03-26 2003-10-02 Japan Science & Technology Corp Ｙｂ混晶酸化物単結晶からなるシンチレータ用発光材料
DE10238398A1 (de) * 2002-08-22 2004-02-26 Philips Intellectual Property & Standards Gmbh Vorrichtung zur Erzeugung von Bildern und/oder Projektionen
DE10308351A1 (de) * 2003-02-27 2004-11-25 Aventis Pharma Deutschland Gmbh 1,3-substituierte Cycloalkylderivate mit sauren, meist heterocyclischen Gruppen, Verfahren zu ihrer Herstellung und ihre Verwendung als Arzneimittel
US7088038B2 (en) * 2003-07-02 2006-08-08 Gelcore Llc Green phosphor for general illumination applications
US7019284B2 (en) * 2003-07-11 2006-03-28 General Electric Company Ultraviolet emitting scintillators for oil detection
US7279120B2 (en) 2003-09-04 2007-10-09 Intematix Corporation Doped cadmium tungstate scintillator with improved radiation hardness
US7576329B2 (en) * 2003-10-17 2009-08-18 General Electric Company Scintillator compositions, and related processes and articles of manufacture
US7180068B1 (en) 2004-06-09 2007-02-20 Radiation Monitoring Devices, Inc. Scintillation materials with reduced afterglow and method of preparation
JP4702767B2 (ja) * 2004-07-01 2011-06-15 シンジーテック株式会社 放射線検出用Ｌｕ３Ａｌ５Ｏ１２結晶材料の製造方法及び放射線検出用（ＺｘＬｕ１−ｘ）３Ａｌ５Ｏ１２結晶材料の製造方法
JP2006015050A (ja) * 2004-07-05 2006-01-19 Ge Medical Systems Global Technology Co Llc Ｘ線ｃｔ装置
CN102888652B (zh) * 2004-11-08 2016-09-21 东北泰克诺亚奇股份有限公司 含Pr的闪烁体用单晶及其制造方法和放射线检测器以及检查装置
US7358542B2 (en) * 2005-02-02 2008-04-15 Lumination Llc Red emitting phosphor materials for use in LED and LCD applications
US20070114562A1 (en) * 2005-11-22 2007-05-24 Gelcore, Llc Red and yellow phosphor-converted LEDs for signal applications
US7497973B2 (en) * 2005-02-02 2009-03-03 Lumination Llc Red line emitting phosphor materials for use in LED applications
US7648649B2 (en) * 2005-02-02 2010-01-19 Lumination Llc Red line emitting phosphors for use in led applications
US7879258B2 (en) * 2005-03-14 2011-02-01 Koninklijke Philips Electronics N.V. Phosphor in polycrystalline ceramic structure and a light-emitting element comprising same
US7274045B2 (en) * 2005-03-17 2007-09-25 Lumination Llc Borate phosphor materials for use in lighting applications
DE102005018329B4 (de) * 2005-04-20 2008-10-30 Siemens Ag Detektormodul für Röntgen- oder Gammastrahlung auf Basis von Wellenleitern
JP5415666B2 (ja) * 2005-12-15 2014-02-12 富士フイルム株式会社 Ｐｒドープ無機化合物及びこれを含む発光性組成物と発光体、発光装置、固体レーザ装置、電離放射線検出装置
US7560046B2 (en) * 2005-12-22 2009-07-14 General Electric Company Scintillator material and radiation detectors containing same
US20100243918A1 (en) * 2006-06-02 2010-09-30 The Regents Of The University Of California Garnet UV phosphor and scintillator materials preparation and use in radiation detection
JP5587601B2 (ja) * 2006-06-21 2014-09-10 コーニンクレッカ フィリップス エヌ ヴェ 少なくとも一つのセラミック球状色変換材料を有する光放出デバイス
US20110150735A1 (en) * 2006-11-01 2011-06-23 Lawrence Livermore National Security, Llc. Fabrication of Transparent Ceramics Using Nanoparticles Synthesized Via Flame Spray Pyrolysis
US8333907B2 (en) * 2007-01-17 2012-12-18 Utc Fire & Security Corporation Articles using persistent phosphors
US7959827B2 (en) * 2007-12-12 2011-06-14 General Electric Company Persistent phosphor
JP4993284B2 (ja) * 2007-03-23 2012-08-08 国立大学法人東北大学 シンチレータ用単結晶の製造方法およびシンチレータ用単結晶
US7608829B2 (en) * 2007-03-26 2009-10-27 General Electric Company Polymeric composite scintillators and method for making same
US7625502B2 (en) * 2007-03-26 2009-12-01 General Electric Company Nano-scale metal halide scintillation materials and methods for making same
US7708968B2 (en) 2007-03-26 2010-05-04 General Electric Company Nano-scale metal oxide, oxyhalide and oxysulfide scintillation materials and methods for making same
TWI429731B (zh) * 2007-07-16 2014-03-11 路明納森公司 由４價錳離子活化之發紅光錯合氟化磷光體
US8545723B2 (en) * 2007-12-12 2013-10-01 General Electric Company Persistent phosphor
WO2010078221A2 (en) * 2008-12-30 2010-07-08 Saint-Gobain Ceramics & Plastics, Inc. Scintillation device and method of producing a ceramic scintillator body
US8877093B2 (en) 2008-12-30 2014-11-04 Saint-Gobain Ceramics & Plastics, Inc. Ceramic scintillator body and scintillation device
WO2010078224A2 (en) 2008-12-30 2010-07-08 Saint-Gobain Ceramics & Plastics, Inc. Ceramic scintillator body and scintillation device
CN102326097B (zh) 2008-12-30 2014-03-12 圣戈本陶瓷及塑料股份有限公司 闪烁装置以及用于生产陶瓷闪烁体本体的方法
US8187089B2 (en) * 2009-03-03 2012-05-29 Wms Gaming Inc. Wagering game providing player options for time-based special event
US8431885B2 (en) 2010-05-19 2013-04-30 Schlumberger Technology Corporation Gamma-ray detectors for downhole applications
JP5342648B2 (ja) 2009-09-18 2013-11-13 三井金属鉱業株式会社 シンチレータ用蛍光体
JP5674385B2 (ja) * 2010-08-27 2015-02-25 古河機械金属株式会社 シンチレータ用ガーネット型結晶およびこれを用いる放射線検出器
CZ2015711A3 (cs) * 2015-10-09 2016-10-19 Crytur Spol S R O Způsob zkrácení scintilační odezvy zářivých center scintilátoru a materiál scintilátoru se zkrácenou scintilační odezvou
US10961452B2 (en) * 2015-12-01 2021-03-30 Siemens Medical Solutions Usa, Inc. Method for controlling gallium content in gadolinium-gallium garnet scintillators
US10197685B2 (en) * 2015-12-01 2019-02-05 Siemens Medical Solutions Usa, Inc. Method for controlling gallium content in gadolinium-gallium garnet scintillators
FR3090830B1 (fr) * 2018-12-20 2022-03-11 Commissariat Energie Atomique Dispositif de refroidissement comprenant une ceramique de grenat paramagnetique
US11994646B2 (en) 2021-03-12 2024-05-28 Baker Hughes Oilfield Operations Llc Garnet scintillator compositions for downhole oil and gas explorations

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL181063C (nl) * 1976-05-13 1987-06-01 Philips Nv Luminescerend scherm; lagedrukkwikdampontladingslamp; werkwijze voor de bereiding van een luminescerend materiaal.
US5391876A (en) * 1990-06-29 1995-02-21 General Electric Company Hole-trap-compensated scintillator material and computed tomography machine containing the same
CA2042263A1 (en) * 1990-06-29 1991-12-30 Charles D. Greskovich Transparent polycrystalline garnets
CA2042147A1 (en) * 1990-06-29 1991-12-30 Veneta G. Tsoukala Hole-trap-compensated scintillator material
US5100598A (en) * 1991-02-19 1992-03-31 General Electric Company Method of forming yttria-gadolinia ceramic scintillator from ammonium dispersed oxalate precipitates
US5116560A (en) * 1991-03-22 1992-05-26 General Electric Company Method of forming rare earth oxide ceramic scintillator with ammonium dispersion of oxalate precipitates
US5057642A (en) * 1991-04-18 1991-10-15 Phillips Petroleum Company Removal of basic impurities from olefin streams

Also Published As

Publication number Publication date
US6358441B2 (en) 2002-03-19
DE10022018A1 (de) 2001-12-20
JP2001072968A (ja) 2001-03-21
US6246744B1 (en) 2001-06-12
US20010028700A1 (en) 2001-10-11

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