JP4369515B2 - 酢酸セルローストウおよびその製造方法 - Google Patents
酢酸セルローストウおよびその製造方法 Download PDFInfo
- Publication number
- JP4369515B2 JP4369515B2 JP2007518049A JP2007518049A JP4369515B2 JP 4369515 B2 JP4369515 B2 JP 4369515B2 JP 2007518049 A JP2007518049 A JP 2007518049A JP 2007518049 A JP2007518049 A JP 2007518049A JP 4369515 B2 JP4369515 B2 JP 4369515B2
- Authority
- JP
- Japan
- Prior art keywords
- tow
- steam
- water
- cellulose acetate
- lubricant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G1/00—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
- D02G1/12—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics using stuffer boxes
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G1/00—Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
- D02G1/20—Combinations of two or more of the above-mentioned operations or devices; After-treatments for fixing crimp or curl
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M7/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made of other substances with subsequent freeing of the treated goods from the treating medium, e.g. swelling, e.g. polyolefins
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Lubricants (AREA)
- Paper (AREA)
Description
フライ(g/30分)=0.00009e0.0209UCE
同等のUCEにおいて、本発明のトウはフライが減少していることに注目されたい。曲線Cは、得られた実験結果(後述の方法)を示している。この実験結果は以下のように表すことができる:
フライ(g/30分)=0.00017UCE−0.0276
UCEが増加しても、フライはほとんど変化しないことに注目されたい。したがって、トウ製造元は、低フライを有する高UCEトウ(より低いCvのトウと言える)を製造することができる。さらに、本発明のトウは、高いUCEを有するにもかかわらず従来のトウと同様に開繊可能であった。
フライ(g/30分)<0.00009e(0.0209UCE)を有し、フライ値の最大値は0.06である。あるいは、トウは:平均UCE>280gcm/cmおよび平均フライ≦0.030g/30分、あるいは平均UCE>265および平均フライ≦0.023、あるいは平均UCE>250および平均フライ≦0.017を有している。さらに、これらのトウは、平均Cv<2.5または2.2または1.75を有している。これらのトウは、セルリアン(Cerulean)(以前はフィルトナ(Filtrona))QTM−7に基づいて80硬度単位以上の硬度も有している。これらのトウは、10,000〜100,000の範囲内の総デニール、および1.5〜4dpfの範囲内のdpfを有している。
UCE(gcm/cm)=(E×1000)/((D×2)+500)
さらに、本明細書において使用される値は平均UCEである。平均UCEとは、少なくとも35ベールのトウの平均を意味し、存在する変動性に対し95%の信頼性でサンプル間の10UCE差を検出できる能力を意味している。
フライ(g/30分)=(G−T)×3
G=テープ上のフライの総重量
T=テープの風袋重量。
さらに、本明細書において使用される値は平均フライである。平均フライは、少なくとも100ベールのトウの平均を意味し、存在する変動性に対し95%の信頼性でサンプル間の0.01g/30分の差を検出できる能力を意味している。
硬度%=(元の直径−減少量)/元の直径×100
本明細書において報告される硬度は、バージニア州リッチモンドのセルリアンのQTM−7を出荷時設定で使用して測定した。
Claims (9)
- 酢酸セルローストウの製造方法であって、
酢酸セルロースと溶媒との溶液を含むドープを紡糸するステップと、
紡糸したままの酢酸セルロースフィラメントを引き取るステップと、
3〜15%の水エマルジョンから成る繊維潤滑剤で前記酢酸セルロースフィラメントを潤滑させるステップであって、前記潤滑剤が、62.0〜65.0重量%の鉱油と、27.0〜28.0重量%の乳化剤であって、50.0〜52.0重量%のソルビタンモノラウレートおよび48.0〜50.0重量%のPOE(20)ソルビタンモノラウレートの混合物である乳化剤と、8.0〜10.0重量%の水とから成る、ステップと、
前記酢酸セルロースフィラメントからトウを形成するステップと、
前記トウを捲縮させるステップと、
前記捲縮したトウを乾燥させるステップと、
前記捲縮し乾燥させたトウをベール梱包するステップと
を含む方法。 - 前記水が、脱ミネラル水、脱イオン水、あるいはその他の適切に濾過および処理された水である請求項1に記載の方法。
- 前記鉱油が、80〜95SUSの粘度を有している請求項1に記載の方法。
- 前記潤滑剤が、63.5〜64.0重量%の鉱油と、27.5〜28.0重量%の乳化剤と、8.3〜8.5重量%の水とから成る、請求項1に記載の方法。
- 前記潤滑剤が、63.6重量%の鉱油と、28.0重量%の乳化剤と、8.4重量%の水とから成る、請求項4に記載の方法。
- 前記乳化剤が、50.0〜51.5重量%のソルビタンモノラウレートおよび48.5〜49.5重量%のPOE(20)ソルビタンモノラウレートの混合物である請求項1に記載の方法。
- 前記乳化剤が、50.9〜51.4重量%のソルビタンモノラウレートおよび49.6〜49.1重量%のPOE(20)ソルビタンモノラウレートの混合物である請求項1に記載の方法。
- 前記潤滑剤が、0.7〜1.8%FOYの範囲で、前記酢酸セルローストウに加えられている請求項1に記載の方法。
- 前記潤滑剤が、1.0%FOYで、前記酢酸セルローストウに加えられている請求項1に記載の方法。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/877,944 US20050287368A1 (en) | 2004-06-25 | 2004-06-25 | Cellulose acetate tow and method of making same |
PCT/US2005/014536 WO2006007018A2 (en) | 2004-06-25 | 2005-04-26 | Cellulose acetate tow and method of making same |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2008504454A JP2008504454A (ja) | 2008-02-14 |
JP4369515B2 true JP4369515B2 (ja) | 2009-11-25 |
Family
ID=35506173
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2007518049A Active JP4369515B2 (ja) | 2004-06-25 | 2005-04-26 | 酢酸セルローストウおよびその製造方法 |
Country Status (7)
Country | Link |
---|---|
US (1) | US20050287368A1 (ja) |
EP (1) | EP1766115A4 (ja) |
JP (1) | JP4369515B2 (ja) |
KR (1) | KR100837769B1 (ja) |
CN (1) | CN1973072B (ja) |
MX (1) | MXPA06014332A (ja) |
WO (1) | WO2006007018A2 (ja) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7585442B2 (en) * | 2004-06-25 | 2009-09-08 | Celanese Acetate, Llc | Process for making cellulose acetate tow |
DE102007061933A1 (de) * | 2007-12-21 | 2009-07-02 | Rhodia Acetow Gmbh | Filter Tow Ballen, Vorrichtung und Verfahren zur Herstellung eines Filter Tow Ballens sowie Filter Tow Streifen |
JP5744725B2 (ja) * | 2008-06-20 | 2015-07-08 | スリーエム イノベイティブ プロパティズ カンパニー | 医療用水性潤滑剤エマルション、又は洗浄装置及び方法 |
CN101487188B (zh) * | 2009-02-13 | 2010-11-10 | 南通醋酸纤维有限公司 | 在醋纤工业领域应用的纺丝油剂 |
US9149070B2 (en) | 2011-07-14 | 2015-10-06 | R.J. Reynolds Tobacco Company | Segmented cigarette filter for selective smoke filtration |
US8967155B2 (en) | 2011-11-03 | 2015-03-03 | Celanese Acetate Llc | Products of high denier per filament and low total denier tow bands |
US9212290B2 (en) | 2012-01-27 | 2015-12-15 | Celanese Acetate Llc | Substituted cellulose acetates and uses thereof |
US20130192613A1 (en) * | 2012-01-27 | 2013-08-01 | Celanese Acetate Llc | Substituted Cellulose Acetates and Uses Thereof |
US9167830B2 (en) | 2012-01-27 | 2015-10-27 | Celanese Acetate Llc | Substituted cellulose acetates and uses thereof |
US9023757B2 (en) | 2012-01-27 | 2015-05-05 | Celanese Acetate Llc | Substituted cellulose acetates and uses thereof |
KR101455002B1 (ko) * | 2013-06-28 | 2014-11-03 | 코오롱인더스트리 주식회사 | 담배필터용 라이오셀 소재 및 그 제조방법 |
EP3051011B1 (en) | 2013-09-26 | 2023-01-11 | Kolon Industries, Inc. | Lyocell material for cigarette filter and method for preparing same |
JP6415077B2 (ja) * | 2014-04-01 | 2018-10-31 | 株式会社ダイセル | 親水化されたセルロースアセテートトウバンド及びそれを用いた吸収体 |
KR102211219B1 (ko) | 2014-06-30 | 2021-02-03 | 코오롱인더스트리 주식회사 | 담배필터용 이형단면 라이오셀 소재 및 그 제조방법 |
KR102211186B1 (ko) | 2014-12-31 | 2021-02-03 | 코오롱인더스트리 주식회사 | 담배필터용 라이오셀 소재 및 그 제조방법 |
EP3258798B1 (en) * | 2015-02-18 | 2018-11-28 | JT International SA | Filters for smoking articles having high additive(s) loadings |
CN106723342A (zh) * | 2016-12-13 | 2017-05-31 | 云南中烟工业有限责任公司 | 一种聚乳酸纤维丝束滤棒成型装置 |
BR112019015258A2 (pt) * | 2017-02-28 | 2020-04-14 | Eastman Chem Co | fibra curta, trama não tecida, e, processo para produzir fibras curtas. |
EP3409829B1 (en) * | 2017-05-30 | 2020-08-12 | Rhodia Acetow GmbH | Composition comprising hydrocarbons, emulsifiers and water, its use and products comprising such composition |
JP6626948B2 (ja) * | 2018-10-02 | 2019-12-25 | 株式会社ダイセル | 親水化されたセルロースアセテートトウバンド及びそれを用いた吸収体 |
CN111227299B (zh) * | 2020-01-16 | 2022-05-31 | 浙江中烟工业有限责任公司 | 滤棒生产过程醋酸纤维和增塑剂在线连续检控系统和方法 |
CN113461996B (zh) * | 2021-07-23 | 2022-10-11 | 盈昌集团有限公司 | 眼镜用醋酸纤维板加硬处理方法 |
CA3242096A1 (en) * | 2021-12-28 | 2023-07-06 | Kolon Industries, Inc. | Lyocell material, smoking article filter, smoking article, and method for manufacturing same |
WO2023128523A1 (ko) * | 2021-12-28 | 2023-07-06 | 코오롱인더스트리 주식회사 | 이형단면 라이오셀 소재, 담배 필터 및 그 제조방법 |
Family Cites Families (17)
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US2593837A (en) * | 1949-10-10 | 1952-04-22 | Ernest Leitz G M B H | Motor and brake control |
CA639824A (en) * | 1952-12-05 | 1962-04-17 | B. Stevens Joel | Filter tow treated with sorbitan compounds |
NL6400844A (ja) * | 1964-02-01 | 1965-08-02 | ||
US3305897A (en) * | 1964-10-28 | 1967-02-28 | Du Pont | Crimping process |
US3756253A (en) * | 1970-12-18 | 1973-09-04 | Mitsubishi Acetate Co Ltd | Cellulose acetate fiber tobacco smoke filter and process of manufacturing the same |
KR910000805B1 (ko) * | 1988-12-17 | 1991-02-09 | 주식회사 선경인더스트리 | 아세테이트 토우 제조용 처리제 조성물 |
JP2947574B2 (ja) * | 1989-11-17 | 1999-09-13 | ダイセル化学工業株式会社 | 高捲縮弾性率アセテートトウおよびその製造方法 |
MY131648A (en) * | 1993-05-24 | 2007-08-30 | Courtaulds Fibres Holdings Ltd | Manufacture of crimped solvent-spun cellulose fibre |
EP1380684A1 (de) * | 2002-07-11 | 2004-01-14 | Zschimmer & Schwarz GmbH & Co KG Chemische Fabriken | Formulierung eines hochviskosen Mineralöls zur herstellung von Filtern für Tabakwaren |
US7323438B2 (en) * | 2003-06-13 | 2008-01-29 | Procter & Gamble | Cleansing article with improved handleability |
US20050136097A1 (en) * | 2003-12-19 | 2005-06-23 | Kimberly-Clark Worldwide, Inc. | Soft paper-based products |
US7585442B2 (en) * | 2004-06-25 | 2009-09-08 | Celanese Acetate, Llc | Process for making cellulose acetate tow |
US7445737B2 (en) * | 2004-06-25 | 2008-11-04 | Celanese Acetate, Llc | Cellulose acetate tow and method of making same |
US7534380B2 (en) * | 2004-06-25 | 2009-05-19 | Celanese Acetate Llc | Cellulose acetate tow and method of making same |
US7534379B2 (en) * | 2004-06-25 | 2009-05-19 | Celanese Acetate Llc | Process of making cellulose acetate tow |
US7585441B2 (en) * | 2004-06-25 | 2009-09-08 | Celanese Acetate, Llc | Process of making cellulose acetate tow |
US7425289B2 (en) * | 2004-06-25 | 2008-09-16 | Celanese Acetate Llc | Process of making cellulose acetate tow |
-
2004
- 2004-06-25 US US10/877,944 patent/US20050287368A1/en not_active Abandoned
-
2005
- 2005-04-26 KR KR1020077001126A patent/KR100837769B1/ko active IP Right Grant
- 2005-04-26 MX MXPA06014332A patent/MXPA06014332A/es active IP Right Grant
- 2005-04-26 JP JP2007518049A patent/JP4369515B2/ja active Active
- 2005-04-26 CN CN2005800211209A patent/CN1973072B/zh active Active
- 2005-04-26 EP EP05741728A patent/EP1766115A4/en not_active Ceased
- 2005-04-26 WO PCT/US2005/014536 patent/WO2006007018A2/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
EP1766115A4 (en) | 2009-07-15 |
MXPA06014332A (es) | 2007-03-12 |
CN1973072A (zh) | 2007-05-30 |
US20050287368A1 (en) | 2005-12-29 |
KR20070039547A (ko) | 2007-04-12 |
EP1766115A2 (en) | 2007-03-28 |
CN1973072B (zh) | 2012-10-31 |
KR100837769B1 (ko) | 2008-06-13 |
WO2006007018A3 (en) | 2006-09-28 |
JP2008504454A (ja) | 2008-02-14 |
WO2006007018A2 (en) | 2006-01-19 |
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