JP3831415B2 - 乾燥器付噴霧室 - Google Patents
乾燥器付噴霧室 Download PDFInfo
- Publication number
- JP3831415B2 JP3831415B2 JP52951298A JP52951298A JP3831415B2 JP 3831415 B2 JP3831415 B2 JP 3831415B2 JP 52951298 A JP52951298 A JP 52951298A JP 52951298 A JP52951298 A JP 52951298A JP 3831415 B2 JP3831415 B2 JP 3831415B2
- Authority
- JP
- Japan
- Prior art keywords
- spray
- gas
- sheath gas
- spray chamber
- droplets
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000007921 spray Substances 0.000 title claims description 254
- 239000007789 gas Substances 0.000 claims description 193
- 239000007788 liquid Substances 0.000 claims description 46
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 34
- 238000000034 method Methods 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000002245 particle Substances 0.000 claims description 18
- 229910052786 argon Inorganic materials 0.000 claims description 17
- 238000002347 injection Methods 0.000 claims description 17
- 239000007924 injection Substances 0.000 claims description 17
- 239000007787 solid Substances 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 15
- 230000002776 aggregation Effects 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- 239000012528 membrane Substances 0.000 claims description 11
- 238000005054 agglomeration Methods 0.000 claims description 7
- 239000002131 composite material Substances 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 6
- 239000002699 waste material Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 230000002093 peripheral effect Effects 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- AUUAIQGEFIEHRO-UHFFFAOYSA-N 1,1,2,2-tetrafluoro-2-[1,1,1,2,3,3-hexafluoro-3-(1,2,2-trifluoroethenoxy)propan-2-yl]oxyethanesulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)OC(F)(C(F)(F)F)C(F)(F)OC(F)=C(F)F AUUAIQGEFIEHRO-UHFFFAOYSA-N 0.000 claims description 2
- 230000008878 coupling Effects 0.000 claims 1
- 238000010168 coupling process Methods 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 claims 1
- 239000000523 sample Substances 0.000 description 50
- 230000004044 response Effects 0.000 description 14
- 239000000443 aerosol Substances 0.000 description 13
- 238000009826 distribution Methods 0.000 description 12
- 230000003446 memory effect Effects 0.000 description 12
- 238000000889 atomisation Methods 0.000 description 8
- 238000010586 diagram Methods 0.000 description 8
- 238000010926 purge Methods 0.000 description 8
- 229920000557 Nafion® Polymers 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 239000011159 matrix material Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000004220 aggregation Methods 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 5
- 230000006872 improvement Effects 0.000 description 5
- 229910052703 rhodium Inorganic materials 0.000 description 5
- 239000010948 rhodium Substances 0.000 description 5
- 239000012491 analyte Substances 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 239000003595 mist Substances 0.000 description 4
- 239000006199 nebulizer Substances 0.000 description 4
- 230000003134 recirculating effect Effects 0.000 description 4
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 4
- 230000035945 sensitivity Effects 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 239000012488 sample solution Substances 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229920000544 Gore-Tex Polymers 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 229910000420 cerium oxide Inorganic materials 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 0 CC(*)CC(Cc1cccc(C*)c1)=C Chemical compound CC(*)CC(Cc1cccc(C*)c1)=C 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000004807 desolvation Methods 0.000 description 1
- 235000012489 doughnuts Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000003116 impacting effect Effects 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000009616 inductively coupled plasma Methods 0.000 description 1
- 238000005040 ion trap Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0468—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample
- H01J49/049—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample with means for applying heat to desorb the sample; Evaporation
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0431—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples
- H01J49/0445—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples with means for introducing as a spray, a jet or an aerosol
- H01J49/045—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for liquid samples with means for introducing as a spray, a jet or an aerosol with means for using a nebulising gas, i.e. pneumatically assisted
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/10—Ion sources; Ion guns
- H01J49/105—Ion sources; Ion guns using high-frequency excitation, e.g. microwave excitation, Inductively Coupled Plasma [ICP]
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
- Electron Tubes For Measurement (AREA)
- Sampling And Sample Adjustment (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77859397A | 1997-01-03 | 1997-01-03 | |
| US08/778,593 | 1997-01-03 | ||
| US08/974,957 US5969352A (en) | 1997-01-03 | 1997-11-20 | Spray chamber with dryer |
| US08/974,957 | 1997-11-20 | ||
| PCT/CA1997/001007 WO1998029896A1 (en) | 1997-01-03 | 1997-12-22 | Spray chamber with dryer |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2001507449A JP2001507449A (ja) | 2001-06-05 |
| JP2001507449A5 JP2001507449A5 (enExample) | 2005-08-11 |
| JP3831415B2 true JP3831415B2 (ja) | 2006-10-11 |
Family
ID=27119475
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP52951298A Expired - Lifetime JP3831415B2 (ja) | 1997-01-03 | 1997-12-22 | 乾燥器付噴霧室 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP1012871A1 (enExample) |
| JP (1) | JP3831415B2 (enExample) |
| AU (1) | AU5474598A (enExample) |
| CA (1) | CA2276018C (enExample) |
| WO (1) | WO1998029896A1 (enExample) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7045015B2 (en) | 1998-09-30 | 2006-05-16 | Optomec Design Company | Apparatuses and method for maskless mesoscale material deposition |
| JP3902380B2 (ja) * | 2000-05-19 | 2007-04-04 | エスアイアイ・ナノテクノロジー株式会社 | Icp分析装置 |
| WO2003005780A1 (en) * | 2001-07-03 | 2003-01-16 | Varian Australia Pty Ltd | Plasma torch |
| US7479630B2 (en) * | 2004-03-25 | 2009-01-20 | Bandura Dmitry R | Method and apparatus for flow cytometry linked with elemental analysis |
| DE202005001632U1 (de) * | 2004-02-06 | 2005-06-02 | Micromass Uk Ltd. | Massenspektrometer |
| US7265362B2 (en) | 2004-02-06 | 2007-09-04 | Micromass Uk Limited | Mass spectrometer |
| US7294841B2 (en) | 2004-02-06 | 2007-11-13 | Micromass Uk Limited | Mass spectrometer |
| US7938341B2 (en) | 2004-12-13 | 2011-05-10 | Optomec Design Company | Miniature aerosol jet and aerosol jet array |
| US7674671B2 (en) | 2004-12-13 | 2010-03-09 | Optomec Design Company | Aerodynamic jetting of aerosolized fluids for fabrication of passive structures |
| TWI482662B (zh) | 2007-08-30 | 2015-05-01 | Optomec Inc | 機械上一體式及緊密式耦合之列印頭以及噴霧源 |
| JP4982900B2 (ja) * | 2008-07-02 | 2012-07-25 | 独立行政法人産業技術総合研究所 | 脱溶媒機能付き誘導結合プラズマトーチ |
| KR200457166Y1 (ko) | 2008-12-16 | 2011-12-07 | 문무 주식회사 | 분말 건조 장치 |
| CN203325832U (zh) | 2010-02-26 | 2013-12-04 | 珀金埃尔默健康科技有限公司 | 允许单元在包括碰撞模式和反应模式的至少两种模式之间切换的系统和操作质谱仪的工具套件 |
| US9190253B2 (en) | 2010-02-26 | 2015-11-17 | Perkinelmer Health Sciences, Inc. | Systems and methods of suppressing unwanted ions |
| SG10201501031YA (en) | 2010-02-26 | 2015-04-29 | Perkinelmer Health Sci Inc | Fluid chromatography injectors and injector inserts |
| GB201216412D0 (en) * | 2012-09-14 | 2012-10-31 | Shimadzu Corp | Apparatus for providing gaseous sample ions/molecules and a corresponding method |
| JP2014211377A (ja) * | 2013-04-19 | 2014-11-13 | 株式会社堀場製作所 | 粒子分析装置 |
| US10994473B2 (en) | 2015-02-10 | 2021-05-04 | Optomec, Inc. | Fabrication of three dimensional structures by in-flight curing of aerosols |
| JP6048552B1 (ja) | 2015-08-21 | 2016-12-21 | 株式会社 イアス | オンライン移送した分析試料の分析システム |
| AU2017268310B8 (en) | 2016-05-18 | 2022-12-08 | Perkinelmer Health Sciences Canada, Inc. | Spray chambers and methods of using them |
| DE112018002448T5 (de) * | 2017-05-12 | 2020-02-20 | Sumco Corporation | Sprühkammer, Probenzerstäubungs- und -einführungsvorrichtung, Analysevorrichtung sowie Verfahren zur Analyse von Bestandteilen einer Probe |
| US10632746B2 (en) | 2017-11-13 | 2020-04-28 | Optomec, Inc. | Shuttering of aerosol streams |
| AU2020218788B2 (en) | 2019-02-04 | 2025-06-26 | Glass Expansion Pty. Limited | Analytic nebuliser |
| TW202247905A (zh) | 2021-04-29 | 2022-12-16 | 美商阿普托麥克股份有限公司 | 用於氣溶膠噴射裝置之高可靠性鞘護輸送路徑 |
| CN116726519A (zh) * | 2023-06-14 | 2023-09-12 | 广东省麦思科学仪器创新研究院 | 雾化气细胞干燥装置和质谱流式细胞仪 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4990740A (en) * | 1989-03-06 | 1991-02-05 | The Dow Chemical Company | Intra-microspray ICP torch |
| US4958529A (en) * | 1989-11-22 | 1990-09-25 | Vestec Corporation | Interface for coupling liquid chromatography to solid or gas phase detectors |
| US5122670A (en) * | 1991-05-17 | 1992-06-16 | Finnigan Corporation | Multilayer flow electrospray ion source using improved sheath liquid |
| CA2062629C (en) * | 1992-03-10 | 1999-06-15 | John Barry French | Apparatus and method for liquid sample introduction |
| EP0560537A1 (en) * | 1992-03-10 | 1993-09-15 | Mds Health Group Limited | Apparatus and method for liquid sample introduction |
-
1997
- 1997-12-22 CA CA002276018A patent/CA2276018C/en not_active Expired - Lifetime
- 1997-12-22 JP JP52951298A patent/JP3831415B2/ja not_active Expired - Lifetime
- 1997-12-22 EP EP97951050A patent/EP1012871A1/en not_active Withdrawn
- 1997-12-22 WO PCT/CA1997/001007 patent/WO1998029896A1/en not_active Ceased
- 1997-12-22 AU AU54745/98A patent/AU5474598A/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| JP2001507449A (ja) | 2001-06-05 |
| EP1012871A1 (en) | 2000-06-28 |
| AU5474598A (en) | 1998-07-31 |
| CA2276018A1 (en) | 1998-07-09 |
| WO1998029896A1 (en) | 1998-07-09 |
| CA2276018C (en) | 2004-11-23 |
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