JP3565373B2 - Cosmetics containing extracts of natural ingredients - Google Patents

Cosmetics containing extracts of natural ingredients Download PDF

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Publication number
JP3565373B2
JP3565373B2 JP09434995A JP9434995A JP3565373B2 JP 3565373 B2 JP3565373 B2 JP 3565373B2 JP 09434995 A JP09434995 A JP 09434995A JP 9434995 A JP9434995 A JP 9434995A JP 3565373 B2 JP3565373 B2 JP 3565373B2
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Japan
Prior art keywords
natural
extract
component
components
water
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Expired - Fee Related
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JP09434995A
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Japanese (ja)
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JPH08259989A (en
Inventor
彰宏 須藤
英一 苗代
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Sunstar Inc
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Sunstar Inc
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Priority to JP09434995A priority Critical patent/JP3565373B2/en
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Description

【0001】
【産業上の利用分野】
本発明は、香料植物から抽出して得た香気成分、色素成分などの天然成分の抽出物を配合した化粧品に関する。
【0002】
【従来の技術及び発明が解決しようとする課題】
化粧水等の化粧品に配合する天然成分の抽出物として、香料植物の子葉、茎、花弁などからの抽出物が使用されている。ここに、香料植物とは、専ら食品、化粧品等の着香又は着色のために用いられる成分を多量に含有し、天然香料や天然着色剤の採取が産業的に行われている植物をいう。
【0003】
例えば、特開昭61−289010号では、ウリ科植物の抽出物を配合した化粧品が、また特開平2−53717号では、ジュ、エイジツ、紅茶などの植物の抽出物を配合した歯磨及び洗口料が、それぞれ提案されている。
【0004】
香料植物から天然成分、主として香気成分及び色素成分を取り出すために、次に示す4つの方法が従来行われている。
【0005】
(1)蒸留法
植物を水蒸気蒸留して天然成分を取り出す方法であり、最も一般的な方法である。主に、ミント類等の天然香料の抽出に使用される。
(2)抽出法
植物を水又はアルコール等の抽出溶媒に浸漬して成分を溶媒抽出する方法である。不揮発性成分や蒸留法では成分が分解してしまう場合に使用される。色素成分を取り出すには、主としてこの方法が使用される。
(3)吸収法
植物中のオイル可溶性の香気成分をオイルに吸収・溶解させて取り出す方法である。蒸留法では成分が分解してしまう場合に使用される。
(4)圧搾法
植物の樹皮や、果皮を機械的に圧搾して成分を取り出す方法。
【0006】
特に、香料植物の花弁などから天然成分(特に香気成分)を取り出す方法としては、蒸留法が一般的である。
【0007】
しかしながら、この蒸留法には、収率が低い、加熱による成分の変性や色素成分を抽出することができない等の欠点がある。また、吸収法には、吸収体からの再抽出操作が煩雑で収率も悪いという欠点があり、圧搾法には、夾雑物の除去及び圧搾汁からの香気成分や色素成分の再抽出が必要であるという欠点がある。
【0008】
抽出法には上述の如き欠点は無いものの、蒸留水(精製水)を抽出溶媒として用いていた従来の抽出法では、香料植物から天然成分を収率良く、しかも破壊することなく抽出することが困難である。かかる抽出の際に破壊された天然成分を化粧品に配合しても、天然成分が発現する本来の色、香りを保持した化粧品を得ることは困難である。
【0009】
本発明は、以上の事情に鑑みなされたものであって、配合した天然成分の本来の色や香りが保持された化粧品を提供することを目的とする。
【0010】
【課題を解決するための手段】
上記目的を達成するための本発明に係る化粧品は、シソ科、バラ科、モクセイ科、キキョウ科、スミレ科、アヤメ科、ヒルガオ科、キク科、ツユクサ科、ウリ科、クワ科、アオイ科、キンポウゲ科、フジウツギ科、ナデシコ科、クマツヅラ科、スイカヅラ科又はユキノシタ科の各香料植物からpH2.0〜5.0の電解酸性水を抽出溶媒に使用して抽出して得た香気成分、色素成分などの天然成分の抽出物が配合されてなる。
【0011】
天然成分の抽出に用いる抽出溶媒は、水道水、ミネラルウォーター、井戸水、天然の湧き水などの通常の水を隔膜を配して電気分解することにより陽極側に得られるpH2.0〜5.0の電解酸性水である。かかる電解酸性水を用いることにより、蒸留水(精製水)を用いた場合に比べて、バラ等の香料植物に含まれる天然成分を破壊することなく抽出することができる。
【0012】
電解酸性水としては、pH2.0〜3.0のものを使用することが、抽出効率を上げるために好ましい。電解酸性水及び電解酸性水を使用して得た抽出物は、酸性領域にあるため、それ自体が抗菌、防腐作用を有する。このため、抽出中や保存中に腐敗変質等の問題が無く、好ましい。
【0013】
本発明に係る化粧品には、シソ科(ラベンダー、ローズマリーなど)、バラ科(バラ、ハマナス、ブラックベリーなど)、モクセイ科(キンモクセイなど)、キキョウ科(キキョウなど)、スミレ科(ニオイスミレ、バイオレットなど)、アヤメ科(アヤメ、サフランなど)、ヒルガオ科(アサガオなど)、キク科(キンセンカ、ベニバナ、ヒマワリ、カミツレなど)、ツユクサ科(ムラサキツユクサなど)、ウリ科(ヘチマなど)、クワ科(ホップなど)、アオイ科(ゼニアオイ)、キンポウゲ科(フクジュソウなど)、フジウツギ科(ジャスミンなど)、ナデシコ科(カーネーションなど)、クマツヅラ科(レモンバーベナなど)、スイカヅラ科(ニオイニンドウなど)又はユキノシタ科(アジサイなど)の各香料植物から抽出された天然成分が配合される。これらの香料植物のうち、バラ科、シソ科、ナデシコ科の各植物が特に好適であり、なかでもバラ科植物が最適である。
【0014】
天然成分の抽出物の化粧品への配合は、天然成分を含む抽出液をそのまま化粧品に配合してもよく、必要に応じて、濃縮した形態で配合してもよい。
【0015】
【作用】
抽出溶媒としてpH2.0〜5.0の電解酸性水を使用した場合、香料植物から天然成分が破壊されることなく収率良く抽出される。このため、このようにして得た天然成分の抽出物を配合した本発明に係る化粧品においては、天然成分が破壊されていないので本来の色や香りを発現する。
【0016】
【実施例】
以下、本発明を実施例に基づいてさらに詳しく説明するが、本発明は下記の実施例に何ら限定されるものではなく、その要旨を変更しない範囲において適宜変更して実施することが可能なものである。
【0017】
(参考例)
切花用として栽培されており、通常香りを採取することができないバラ(品種:ローテローゼ、花弁の色:赤)の花弁100gを、下記の条件で飲料用の水道水を電気分解して得た電解酸性水(pH=2.33)1200mlに常温で一昼夜浸漬した。また、比較のために、上記と同じバラの花弁100gを、精製水1200mlに常温で一昼夜浸漬した。
【0018】
〈電気分解の条件〉
原水:水道水(pH=6.50)
電解槽の電極:チタン・白金めっき電極
電解電圧:62V
電解酸性水流出速度:0.1リットル/分
【0019】
次いで、バラの花弁を取り除き、0.22ミクロンのミリポアフィルターで除菌ろ過を行い、抽出液を得た。得られた抽出液の性状及び抽出液の濃縮物の収率を表1に示す。
【0020】
【表1】

Figure 0003565373
【0021】
表1に示すように、電解酸性水を抽出溶媒に使用して得た抽出液は鮮やかなピンク色をしたバラの花の香がするものであったが、蒸留水を抽出溶媒に使用して得た抽出液は色も匂いも悪く、また抽出液の濃縮物の収率も、電解酸性水を使用した場合に比べて格段に低かった。
【0022】
(実施例)
参考例で得た電解酸性水によるバラの花弁の抽出物を使用して、下記(1)〜(3)に示す種々の化粧品を作製した。
【0023】
(1)化粧水
下記の(A)成分と下記の(B)成分とを混合して化粧水を作製した。配合割合を示す%は化粧水の総量に対する重量%である(後出する%も同義である)。
Figure 0003565373
【0024】
(2)美容液
下記の(A)成分と下記の(B)成分とを混合して美容液を作製した。
Figure 0003565373
【0025】
(3)クリーム
加熱混合した下記の(A)成分に下記の(B)成分を攪拌混合した後、冷却して、クリームを作製した。
Figure 0003565373
【0026】
【発明の効果】
本発明によれば、含有する天然成分の本来の色や香りを保持した化粧品が提供される。[0001]
[Industrial applications]
TECHNICAL FIELD The present invention relates to cosmetics containing an extract of a natural component such as an aroma component or a pigment component obtained by extracting from a perfume plant.
[0002]
Problems to be solved by the prior art and the invention
Extracts from cotyledons, stems, petals and the like of perfume plants have been used as extracts of natural ingredients to be incorporated into cosmetics such as lotions. Here, the fragrance plant refers to a plant that contains a large amount of components used exclusively for flavoring or coloring of foods, cosmetics, etc., and from which natural fragrances and natural coloring agents are collected industrially.
[0003]
For example, Japanese Patent Application Laid-Open No. 61-289010 discloses cosmetics containing an extract of a Cucurbitaceae plant, and Japanese Patent Application Laid-Open No. 2-53717 discloses a toothpaste and a mouthwash containing an extract of a plant such as ju, age and black tea. Fees have been proposed for each.
[0004]
In order to extract natural components, mainly fragrance components and pigment components from perfume plants, the following four methods have been conventionally performed.
[0005]
(1) Distillation method This is a method of extracting a natural component by steam distillation of a plant, and is the most common method. It is mainly used for extracting natural flavors such as mint.
(2) Extraction method This is a method of immersing a plant in an extraction solvent such as water or alcohol to extract the components by solvent. It is used when a nonvolatile component or a component is decomposed by a distillation method. This method is mainly used for removing the dye component.
(3) Absorption method This is a method in which an oil-soluble fragrance component in a plant is absorbed and dissolved in oil to be taken out. The distillation method is used when components are decomposed.
(4) Squeezing method A method of mechanically squeezing the bark or pericarp of a plant to extract components.
[0006]
In particular, a distillation method is generally used as a method for extracting a natural component (especially, an aroma component) from petals of a fragrance plant.
[0007]
However, this distillation method has disadvantages such as low yield, denaturation of components by heating, and inability to extract dye components. In addition, the absorption method has the drawback that the operation of re-extraction from the absorber is complicated and the yield is poor, and the compression method requires removal of contaminants and re-extraction of aroma components and pigment components from the compressed juice. There is a disadvantage that it is.
[0008]
Although the extraction method does not have the drawbacks described above, the conventional extraction method using distilled water (purified water) as an extraction solvent makes it possible to extract natural components from perfumery plants in good yield and without destruction. Have difficulty. Even if natural ingredients destroyed during such extraction are blended into cosmetics, it is difficult to obtain cosmetics that retain the original color and scent that the natural ingredients express.
[0009]
The present invention has been made in view of the above circumstances, and an object of the present invention is to provide a cosmetic product in which the original color and scent of the blended natural components are retained.
[0010]
[Means for Solving the Problems]
Cosmetics according to the present invention for achieving the above object, Lamiaceae, Rosaceae, Oleaceae, Fennelaceae, Violaceae, Iridaceae, Convolvulaceae, Asteraceae, Asteraceae, Cucurbitaceae, Mulberry family, Mallow family, Aroma component and pigment component obtained by extracting electrolytic acid water having a pH of 2.0 to 5.0 as an extraction solvent from each of the perfume plants of the buttercup family, Buddleiaceae, Papilionidae, Papilionidae, Watermelonaceae, or Saxifragaceae. An extract of a natural component such as a natural ingredient is blended.
[0011]
The extraction solvent used for the extraction of natural components has a pH of 2.0 to 5.0 obtained on the anode side by subjecting ordinary water such as tap water, mineral water, well water, natural spring water to electrolysis with a diaphragm. Electrolyzed acidic water. By using such electrolytic acidic water, it is possible to extract natural components contained in a fragrant plant such as rose without destroying it, as compared with the case of using distilled water (purified water).
[0012]
It is preferable to use an electrolyzed acidic water having a pH of 2.0 to 3.0 in order to increase the extraction efficiency. Electrolytic acidic water and the extract obtained using electrolytic acidic water are in the acidic region, and therefore have antibacterial and antiseptic effects themselves. For this reason, there is no problem such as spoilage alteration during extraction or storage, which is preferable.
[0013]
The cosmetics according to the present invention include Lamiaceae (lavender, rosemary, etc.), Rosaceae (roses, hamanas, blackberry, etc.), Moleaceae (Kinu-mokusei, etc.), Fenidae (Kekyo, etc.), and Violaceae (Numeis violet, Violet, etc., Iridaceae (Iris, Saffron, etc.), Convolvulaceae (Asagao, etc.), Asteraceae (Calendula, Safflower, Sunflower, Chamomile, etc.), Cyperaceae (Europea, etc.), Cucurbitaceae, etc., etc., Mulberry ( Hops), Malvaceae (Mallow), Ranunculaceae (Fukujusou, etc.), Buddleia family (Jasmine, etc.), Nadesicoceae (Carnation, etc.), Lilium spp. (Lemon verbena, etc.), Watermelonaceae (Smeltwood, etc.) or Saxifragaceae ( Hydrangea, etc.) Component is formulated. Among these fragrance plants, plants of the family Rosaceae, Lamiaceae, and Papilionidae are particularly suitable, and among them, the Rosaceae plant is most suitable.
[0014]
The natural component extract may be incorporated into cosmetics by using the extract containing the natural component in cosmetics as it is, or may be incorporated in a concentrated form as needed.
[0015]
[Action]
When electrolytic acidic water having a pH of 2.0 to 5.0 is used as the extraction solvent, natural components are extracted from perfume plants in good yield without being destroyed. For this reason, in the cosmetics according to the present invention in which the natural component extract thus obtained is blended, the natural color and fragrance are exhibited since the natural component is not destroyed.
[0016]
【Example】
Hereinafter, the present invention will be described in more detail with reference to Examples, but the present invention is not limited to the following Examples at all, and can be implemented by appropriately changing the scope without changing the gist thereof. It is.
[0017]
(Reference example)
Electrolysis obtained by electrolyzing 100 g of petals of roses (cultivar: rotherose, petal color: red), which are cultivated for cut flowers and cannot normally collect fragrance, under the following conditions with tap water for drinking It was immersed in 1200 ml of acidic water (pH = 2.33) at room temperature for 24 hours. Further, for comparison, 100 g of the same rose petal was immersed in 1200 ml of purified water at room temperature for 24 hours.
[0018]
<Electrolysis conditions>
Raw water: tap water (pH = 6.50)
Electrode of electrolytic cell: Titanium / platinum plating Electrode voltage: 62V
Electrolytic acid water outflow rate: 0.1 liter / min
Next, the petals of the rose were removed, and sterile filtration was performed with a 0.22 micron Millipore filter to obtain an extract. Table 1 shows the properties of the obtained extract and the yield of the concentrate of the extract.
[0020]
[Table 1]
Figure 0003565373
[0021]
As shown in Table 1, the extract obtained by using electrolytic acidic water as the extraction solvent had a bright pink rose flower scent. However, distilled water was used as the extraction solvent. The obtained extract had poor color and odor, and the yield of the extract concentrate was much lower than that in the case of using electrolytic acidic water.
[0022]
(Example)
Various cosmetics shown in the following (1) to (3) were produced using the extract of rose petals by the electrolytic acidic water obtained in the reference example.
[0023]
(1) Lotion A lotion was prepared by mixing the following components (A) and (B). % Indicating the blending ratio is% by weight with respect to the total amount of the lotion (the below-mentioned% has the same meaning).
Figure 0003565373
[0024]
(2) Beauty liquid A beauty liquid was prepared by mixing the following component (A) and the following component (B).
Figure 0003565373
[0025]
(3) The following component (B) was stirred and mixed with the following component (A) that had been heated and mixed, followed by cooling to prepare a cream.
Figure 0003565373
[0026]
【The invention's effect】
ADVANTAGE OF THE INVENTION According to this invention, the cosmetics which preserve | saved the original color and fragrance of the natural component contained are provided.

Claims (1)

シソ科、バラ科、モクセイ科、キキョウ科、スミレ科、アヤメ科、ヒルガオ科、キク科、ツユクサ科、ウリ科、クワ科、アオイ科、キンポウゲ科、フジウツギ科、ナデシコ科、クマツヅラ科、スイカヅラ科又はユキノシタ科の各香料植物からpH2.0〜5.0の電解酸性水を抽出溶媒に使用して抽出して得た香気成分、色素成分などの天然成分の抽出物を配合した化粧品。Labiatae, Rosaceae, Oleaceae, Fennelaceae, Violetaceae, Iridaceae, Convolvulaceae, Asteraceae, Asclepiaceae, Cucurbitaceae, Mulberry, Malvaceae, Ranunculaceae, Buddleiaceae, Papilionidae, Laceae, Honeysuckle Alternatively, cosmetics containing natural component extracts such as fragrance components and pigment components obtained by extracting electrolytic acid water having a pH of 2.0 to 5.0 as an extraction solvent from each fragrant plant of the family Saxifragaceae.
JP09434995A 1995-03-27 1995-03-27 Cosmetics containing extracts of natural ingredients Expired - Fee Related JP3565373B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP09434995A JP3565373B2 (en) 1995-03-27 1995-03-27 Cosmetics containing extracts of natural ingredients

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JP3565373B2 true JP3565373B2 (en) 2004-09-15

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106433974A (en) * 2016-11-17 2017-02-22 东莞波顿香料有限公司 Cleome viscosa extract and cut tobaccos containing cleome viscosa extract

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4441177B2 (en) * 2001-02-01 2010-03-31 明治製菓株式会社 Process for producing phenolic-containing Labiatae plant extract and use thereof
JP2006089543A (en) * 2004-09-22 2006-04-06 Shiseido Co Ltd Method for producing natural perfume
JP5859190B2 (en) * 2010-09-09 2016-02-10 八藤 眞 Method for producing fragrance composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106433974A (en) * 2016-11-17 2017-02-22 东莞波顿香料有限公司 Cleome viscosa extract and cut tobaccos containing cleome viscosa extract

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