JP3110624B2 - Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain - Google Patents

Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain

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Publication number
JP3110624B2
JP3110624B2 JP06243989A JP24398994A JP3110624B2 JP 3110624 B2 JP3110624 B2 JP 3110624B2 JP 06243989 A JP06243989 A JP 06243989A JP 24398994 A JP24398994 A JP 24398994A JP 3110624 B2 JP3110624 B2 JP 3110624B2
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JP
Japan
Prior art keywords
steel sheet
rolled steel
content
steel
cold
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP06243989A
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Japanese (ja)
Other versions
JPH08104926A (en
Inventor
輝昭 山田
昌彦 織田
康長 大滝
裕和 芳賀
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
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Nippon Steel Corp
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Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP06243989A priority Critical patent/JP3110624B2/en
Publication of JPH08104926A publication Critical patent/JPH08104926A/en
Application granted granted Critical
Publication of JP3110624B2 publication Critical patent/JP3110624B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、耐デント性の優れた深
絞り用高強度冷延鋼板の製造方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a high-strength cold-rolled steel sheet for deep drawing having excellent dent resistance.

【0002】[0002]

【従来の技術】従来、耐デント性の優れた高強度冷延鋼
板は、自動車の外板パネルに主として使われている。そ
の従来技術としては、これまで耐デント性の優れた高強
度冷延鋼板の製造方法として、特開昭60−17485
2号、特開昭57−76131号、特公昭60−170
04号公報、更に、Bを添加し二次加工性をも付与する
方法として、特開昭58−84928号公報がある。す
なわち、特開昭60−174852号公報は、連続焼鈍
温度をAc3 以上1000℃以下とし複合組織を造る方
法で、特開昭57−76131号公報は、連続焼鈍温度
を900℃〜Ac3 とする方法であり、何れも連続焼鈍
の焼鈍温度が極めて高いのが特徴であるが、そのため、
通常の連続焼鈍設備では、900℃を越えるような高温
の鋼帯が炉内のハースロールを通過すると鋼板が軟らか
過ぎて絞り込まれ皺が発生し良好な形状の板が製造でき
なくなると言う問題がある。
2. Description of the Related Art Conventionally, high-strength cold-rolled steel sheets having excellent dent resistance have been mainly used for outer panels of automobiles. As the prior art, a method for producing a high-strength cold-rolled steel sheet having excellent dent resistance has been disclosed in JP-A-60-17485.
No. 2, JP-A-57-76131, JP-B-60-170
JP-A-58-84928 discloses a method for imparting secondary workability by adding B to JP-A-58-84928. In other words, JP 60-174852 discloses is a method of making a continuous annealing temperature Ac 3 above 1000 ° C. or less and a composite structure, JP 57-76131 discloses includes a continuous annealing temperature 900 ° C. to Ac 3 Are characterized by the extremely high annealing temperature of continuous annealing.
In ordinary continuous annealing equipment, when a steel strip having a high temperature exceeding 900 ° C. passes through a hearth roll in a furnace, the steel sheet is too soft and squeezed to cause wrinkles, which makes it impossible to produce a sheet having a good shape. is there.

【0003】また、特公昭60−17004号公報は、
連続焼鈍時に均熱後の冷却において、少なくとも650
℃以上の温度域を10℃/s以上(好ましくは50℃/
s以上)の急速冷却で冷却することで、焼付硬化性の優
れた深絞り用冷延鋼板を製造する方法であるが、例え
ば、同公報で好ましい範囲とされているような50℃/
sのような急速冷却で均熱後の冷却を行えば、冷却速度
が著しく速いために、鋼帯がハースロールを通過する際
に、鋼帯の温度とハースロール温度を一致させることが
難しくなり、鋼帯がハースロールにより急速に加熱され
たり或いは冷却されたりするために鋼板形状が悪くな
り、安定して良好な形状の鋼板の製造が困難であると言
う問題を抱えている。
[0003] Japanese Patent Publication No. Sho 60-17004 discloses that
In cooling after soaking during continuous annealing, at least 650
Temperature range of 10 ° C / s or more (preferably 50 ° C /
s or more) to produce a cold-rolled steel sheet for deep drawing with excellent bake hardening properties, for example, 50 ° C. /
If the cooling after soaking is performed by rapid cooling such as s, it is difficult to make the temperature of the steel strip coincide with the hearth roll temperature when the steel strip passes through the hearth roll because the cooling rate is extremely high. In addition, since the steel strip is rapidly heated or cooled by the hearth roll, the shape of the steel sheet is deteriorated, and there is a problem that it is difficult to stably produce a steel sheet having a good shape.

【0004】更には、特開昭58−84928号公報
は、二次加工性の向上とNの悪影響を防止するために、
Bを重量比で0.8〜1.4添加する方法であるが、同
公報の補正後の第2表に示されているようにr値(以
下、ここでは深絞り特性の指標となるr値の面内平均値
を示す)は2.03と少し高い実施例もあるが1.6
3,1.65と云ったかなり低い深絞り性しか得られて
いない実施例をも含んでおり、更に厳しい深絞り性が要
求される最近の自動車のフェンダー用の高強度鋼板を安
定して製造することが困難であると言う問題がある。
Further, Japanese Patent Application Laid-Open No. 58-84928 discloses a method for improving the secondary workability and preventing the adverse effect of N.
In this method, B is added in a weight ratio of 0.8 to 1.4, and as shown in Table 2 after correction in the publication, the r value (hereinafter referred to as an index of the deep drawing characteristic here, r) In some examples, the in-plane average value of the values was slightly higher at 2.03, but 1.6.
Includes an example in which only a very low deep drawability, such as 3,1.65, is obtained, and stably manufactures a high-strength steel sheet for a fender of a recent automobile that requires a more severe deep drawability. There is a problem that it is difficult to do.

【0005】以上述べたように、最近の自動車のフェン
ダーのような、より厳しい深絞り加工にも耐えられる耐
デント性の優れた深絞り用高強度冷延鋼板を連続焼鈍法
で鋼板形状不良のトラブルもなく製造できる製造方法は
まだないのである。従って、この問題を解決するため
の、耐デント性の優れた深絞り用高強度冷延鋼板の製造
方法の提供が強く望まれている。
As described above, a high-strength cold-rolled steel sheet for deep drawing with excellent dent resistance, such as a recent automobile fender, which can withstand more severe deep drawing work, has a sheet shape defect by a continuous annealing method. There is not yet a manufacturing method that can be manufactured without trouble. Therefore, it is strongly desired to provide a method for producing a high-strength cold-rolled steel sheet for deep drawing with excellent dent resistance to solve this problem.

【0006】[0006]

【発明が解決しようとする課題】本発明で解決しようと
する課題は、フェンダーのように、より厳しい深絞り加
工にも耐えられる耐デント性の優れたストレッチャスト
レインの発生しない深絞り用高強度冷延鋼板の製造方法
を提供することである。
The problem to be solved by the present invention is to provide a high-strength cold drawing for deep drawing which does not generate a stretcher strain excellent in dent resistance that can withstand more severe deep drawing processing like a fender. An object of the present invention is to provide a method for manufacturing a rolled steel sheet.

【0007】[0007]

【課題を解決するための手段】本発明者等は、上記課題
を解決する方法に付いて、(1)連続焼鈍法で鋼板形状
不良のトラブルもなく製造できる製造条件の検討を行
い、その上で、より厳しい深絞り加工にも耐えられる耐
デント性の優れた深絞り用高強度冷延鋼板の製造方法を
検討し、請求項1記載の方法を見出したものである。ま
た、更に、一部用途には、鋼板の特性値を劣化させない
で且つ二次加工性をも付与できる製造法を検討し、請求
項2記載の方法を見出したものである。
Means for Solving the Problems In order to solve the above-mentioned problems, the present inventors have studied (1) the manufacturing conditions under which the steel sheet can be manufactured by the continuous annealing method without any trouble of defective shape of the steel sheet. The present inventors have studied a method for producing a high-strength cold-rolled steel sheet for deep drawing with excellent dent resistance that can withstand more severe deep drawing, and have found the method described in claim 1. Furthermore, for some applications, a production method capable of imparting secondary workability without deteriorating the characteristic value of the steel sheet was studied, and a method according to claim 2 was found.

【0008】その本発明の要旨は次の通りである。 (1)C:0.0010〜0.0030wt%,Si≦
0.50wt%,Mn:0.02〜0.23wt%
P:0.035〜0.150wt%,S≦0.030w
t%,sol.Al:0.025〜0.100wt%,
N:0.0005〜0.0100wt%,Nb:0.0
07〜0.020wt%で、且つ、C量とNb量の関係
が下記式の範囲を満たし残部不可避的不純物及び鉄より
なる鋳片を、Ar3 以上で仕上げ圧延を行い巻き取り熱
延鋼帯とし、冷間圧延を行い、連続焼鈍法で750〜8
90℃に加熱し再結晶焼鈍を行い、その後、冷却を行う
に当たり、少なくとも730℃までの間を、2℃/s以
上10℃/s未満の冷却速度で冷却し、焼鈍板を造り、
その後、0.5〜3%の調質圧延を行うことを特徴とす
る耐デント性に優れたストレッチャストレインの発生し
ない深絞り用高強度冷延鋼板の製造方法。 Nb:7.75 ×wt% C−0.013 ≦Nb(wt%)≦7.75 ×
wt% C+0.007 (2)(1)記載の方法に於いて、鋼の組成を、更に、
B(wt%)を0.004×wt%P以上、0.001
0wt%以下で、且つ、B/N≦0.7(wt%比)の
範囲とすることを特徴とする優れた二次加工性をも付与
する製造方法にある。
The gist of the present invention is as follows. (1) C: 0.0010 to 0.0030 wt%, Si ≦
0.50 wt%, Mn: 0.02 to 0.23 wt%,
P: 0.035 to 0.150 wt%, S ≦ 0.030 w
t%, sol. Al: 0.025 to 0.100 wt%,
N: 0.0005 to 0.0100 wt%, Nb: 0.0
07-0.020 wt%, and the relationship between the C amount and the Nb amount satisfies the range of the following formula, and the cast slab composed of the inevitable impurities and iron is rolled by finishing rolling with Ar 3 or more, and the rolled hot rolled steel strip. Cold rolling is performed, and 750 to 8
After heating to 90 ° C. for recrystallization annealing, and then cooling, at least to 730 ° C., at a cooling rate of 2 ° C./s or more and less than 10 ° C./s, to produce an annealed plate,
Thereafter, a method for producing a high-strength cold-rolled steel sheet for deep drawing, which does not generate stretcher strain and has excellent dent resistance, characterized by performing a temper rolling of 0.5 to 3%. Nb: 7.75 × wt% C−0.013 ≦ Nb (wt%) ≦ 7.75 ×
wt% C + 0.007 (2) In the method described in (1), the steel composition
B (wt%) is 0.004 × wt% P or more, 0.001
The present invention is also directed to a manufacturing method for imparting excellent secondary workability, characterized in that the content is 0 wt% or less and B / N ≦ 0.7 (wt% ratio).

【0009】以下、本発明について詳細に述べる。本発
明者等は、本発明が解決しようとする課題について、
(1)通常の連続焼鈍設備で安定して良好な形状の鋼帯
を得る製造条件、(2)極低炭素冷延鋼板で造った外板
パネルのデント性と鋼板特性の関係、(3)良好なデン
ト性が得られる材質特性の冷延鋼板の製造方法について
検討し、本発明の方法を見出したものである。その考え
方は、下記に示す概要の通りである。 (1)通常の連続焼鈍設備で安定して良好な形状の鋼帯
を得る製造条件 自動車外板用の冷延鋼板は、板厚が0.60〜0.80
mmで板幅が1400〜1700mm程度の薄手広幅材
が主であるが、これらの冷延鋼板を連続焼鈍設備で製造
する上で最も障害となるのは、加熱温度が高い場合や高
い温度域で急激な冷却を行うとハースロール部のロール
クラウン(凸)による幅方向の圧縮応力による板の絞り
や、板温とロール温度との不一致により発生する熱応力
による板形状不良である。本発明者等はこの件に関し、
種々検討した結果、自動車外板に適用できるような良好
な形状の鋼帯を安定して得るには、少なくとも、焼鈍温
度を890℃以下とし、且つ、730℃以上の温度域の
冷却速度を少なくとも20℃/s未満とする必要がある
ことがわかった。
Hereinafter, the present invention will be described in detail. The present inventors have solved the problem to be solved by the present invention,
(1) Manufacturing conditions to obtain a steel strip having a good shape stably with ordinary continuous annealing equipment; (2) Relationship between dent properties of outer panel made of extremely low carbon cold rolled steel sheet and steel sheet properties; (3) The present inventors have studied a method for producing a cold-rolled steel sheet having material properties that can provide good dent properties, and have found the method of the present invention. The concept is as outlined below. (1) Manufacturing conditions for obtaining a steel strip having a good shape stably with ordinary continuous annealing equipment A cold rolled steel sheet for an automobile outer panel has a thickness of 0.60 to 0.80.
mm and a sheet width of about 1400 to 1700 mm are mainly used. However, the most hindrance in producing these cold-rolled steel sheets by continuous annealing equipment is when the heating temperature is high or in a high temperature range. When rapid cooling is performed, the plate is narrowed due to the compressive stress in the width direction due to the roll crown (convex) of the hearth roll portion, and the plate shape is defective due to the thermal stress generated due to the mismatch between the plate temperature and the roll temperature. The present inventors have dealt with this matter,
As a result of various studies, in order to stably obtain a steel strip having a good shape that can be applied to an automobile outer panel, at least the annealing temperature is set to 890 ° C or lower, and the cooling rate in the temperature range of 730 ° C or higher is set to at least. It was found that the temperature had to be lower than 20 ° C./s.

【0010】(2)極低炭素冷延鋼板で造った外板パネ
ルのデント性と鋼板特性の関係一方、本発明者等は、極
低炭素冷延鋼板で造った外板パネルのデント性と鋼板特
性の関係についても種々検討した結果、完全非時効性の
極低炭素冷延鋼板で造った外板パネルは、箱焼鈍法(B
AF法)で製造した完全非時効性の低炭素Alキルド冷
延鋼板に比べて顕著にデント性が劣っているが、極低炭
素冷延鋼板でも固溶Cを存在せしめ、約1kgf/mm
2 以上のBH性を付与した冷延鋼板は顕著に耐デント性
が向上することを見出した。即ち、極低炭素冷延鋼板で
は、BAF法で製造した低炭素Al−K鋼の場合とは異
なり、完全非時効性の鋼板のデント性はY.P(0.2
%耐力)の値以上に大きく低下するが、BH量が1kg
f/mm2 以上あるとBH後のY.Pに対応した良好な
耐デント性が確保できることを知見したものであり、自
動車外板用の冷延鋼板としては必ずしも3kgf/mm
2 以上のBHを付与する必要がなく1kgf/mm2
上のBH量を付与してやればよいことが明らかになっ
た。尚、極低炭素冷延鋼板の耐デント性が、BH量が0
と1kgf/mm2 とでこの様に大きく異なるのは、必
ずしも明確になっているわけではないが、BH量が0の
場合の弾性限が、Y.Pの50〜60%程度しかないこ
とに起因しているものと推察される。
(2) Relationship between Dent Property of Outer Panel Made of Ultra-Low Carbon Cold Rolled Steel Sheet and Steel Sheet Properties On the other hand, the present inventors have studied the dent property of an outer panel made of extremely low carbon cold rolled steel sheet. As a result of various studies on the relationship between the properties of the steel sheets, the outer panel made of a completely non-ageable ultra-low carbon cold-rolled steel sheet was subjected to the box annealing method (B
AF method), the dent property is remarkably inferior to that of a completely non-aged low-carbon Al-killed cold-rolled steel sheet. However, even a very low-carbon cold-rolled steel sheet has solid solution C, and is about 1 kgf / mm.
It has been found that a cold-rolled steel sheet provided with a BH property of 2 or more has significantly improved dent resistance. That is, in the ultra-low carbon cold rolled steel sheet, unlike the case of the low carbon Al-K steel manufactured by the BAF method, the dent property of the completely non-aging steel sheet is Y. P (0.2
% Proof stress), but the BH amount is 1 kg.
If f / mm 2 or more, Y. It has been found that good dent resistance corresponding to P can be ensured, and it is not necessarily 3 kgf / mm as a cold rolled steel sheet for an automobile outer panel.
That may do it by applying a 1 kgf / mm 2 or more BH amount is not necessary to impart two or more BH revealed. The dent resistance of the ultra-low carbon cold-rolled steel sheet is 0, and the BH amount is 0.
Although it is not necessarily clear that such a large difference between 1 kgf / mm 2 and 1 kgf / mm 2 , the elastic limit when the BH amount is 0 is Y. It is presumed that it is caused by only about 50 to 60% of P.

【0011】(3)ストレッチャストレインの発生もな
く良好なデント性が得られる材質特性の冷延鋼板の製造
方法 より厳しい深絞り加工にも耐えられる耐デント性の優れ
た深絞り用高強度冷延鋼板の製造方法における重要な課
題は、の「より厳しい深絞り加工にも耐えられる優れ
たr値が得られること」、の「安定して1kgf/m
2 以上のBH量を得ることストレッチャストレインが
全く発生しないこと」、の上記(1)の「通常の連続
焼鈍設備で安定して良好な形状の鋼帯を得る製造条
件」、即ち、少なくとも、焼鈍温度を890℃以下と
し、且つ、730℃以上の温度域の冷却速度を少なくと
も20℃/s未満の条件で製造できることである。
(3) A method for producing a cold-rolled steel sheet having a material property capable of obtaining good dent properties without generation of stretch strain, and a high-strength deep-drawing cold-rolling sheet having excellent dent resistance to withstand more severe deep drawing. An important issue in the method for manufacturing a steel sheet is to “obtain an excellent r-value that can withstand stricter deep drawing” and “stable 1 kgf / m”.
(a) obtaining a BH amount of not less than m 2, that no stretcher strain is generated at all ”, and“ (1) “production conditions for stably obtaining a steel strip having a good shape with ordinary continuous annealing equipment”, ie, at least: That is, it can be manufactured under the condition that the annealing temperature is 890 ° C. or less and the cooling rate in the temperature range of 730 ° C. or more is at least less than 20 ° C./s.

【0012】本発明者等は、先ず、の「通常の連続焼
鈍設備で安定して良好な形状の鋼帯を得る製造条件」、
即ち、少なくとも、焼鈍温度を890℃以下とし、且
つ、730℃以上の温度域の冷却速度を少なくとも20
℃/s未満の条件内で、のより厳しい深絞り加工にも
耐えられる優れたr値が得られる製造方法について検討
した。本発明者等は、ラボ真空溶解炉を用い、種々の成
分の鋼を溶製し、熱間圧延、冷間圧延、連続焼鈍、調質
圧延を行い検討した結果、BH性も得られ且つr値の高
い冷延鋼板が得られるのは、請求項1に示すような成分
の鋼でなければならないことを見出した。中でも、r値
に大きく影響するのは、C含有量とNb含有量である。
[0012] The present inventors have firstly described "manufacturing conditions for obtaining a steel strip having a good shape stably with ordinary continuous annealing equipment".
That is, at least the annealing temperature is 890 ° C. or lower, and the cooling rate in the temperature range of 730 ° C. or higher is at least 20 ° C.
Under conditions of less than ° C./s, a manufacturing method that can obtain an excellent r-value that can withstand more severe deep drawing was studied. The inventors of the present invention smelted steels of various components using a laboratory vacuum melting furnace, and performed hot rolling, cold rolling, continuous annealing, and temper rolling. As a result, BH properties were obtained and r It has been found that a cold-rolled steel sheet having a high value must be obtained from a steel having the composition shown in claim 1. Among them, the C content and the Nb content greatly affect the r value.

【0013】C含有量が0.0030wt%超になった
り、Nb含有量が0.007wt%未満であったり、
0.020wt%超となった場合は、r値が低下し十分
な深絞り性が得られない。特に、C含有量が0.003
0wt%超となった場合のr値の劣化は大きいことがわ
かった。次に、本発明者等は上記のC,Nb含有量の範
囲内で、の安定して1kgf/mm2 以上のBH量を
得ることとストレッチャストレインが全く発生しないこ
とを両立させる方法について検討した。この課題が製鉄
所で実質的に解決されるには、前提条件として、鋳片を
製造するときのC含有量のバラツキ範囲を許容できる製
造方法でなければならない。即ち、安定して1kgf/
mm2 以上のBH量を得ることとストレッチャストレイ
ンが全く発生しないことを両立させるためには、これら
特性に最も大きく影響するC含有量が現在の製鋼の成分
のコントロール範囲内の鋳片で達成可能な製造方法でな
ければ工業的に意味の無い発明となるからである。従っ
て、現状の製鋼で極低炭素鋼の鋳片を造るときのC含有
量のバラツキ範囲であるC:±10ppmを前提とし、
且つ、r値を確保するためのC,Nb含有量の範囲、即
ち、C:0.0010〜0.0030wt%,Nb:
0.007〜0.020wt%の成分の鋼を前提として
検討した。
When the C content exceeds 0.0030 wt%, the Nb content is less than 0.007 wt%,
If the content exceeds 0.020 wt%, the r value decreases, and sufficient deep drawability cannot be obtained. In particular, the C content is 0.003.
It has been found that when the content exceeds 0 wt%, the deterioration of the r value is large. Next, the present inventors have studied a method for achieving a stable BH amount of 1 kgf / mm 2 or more and no stretcher strain at all within the above-mentioned ranges of C and Nb contents. . In order for this problem to be substantially solved in a steel mill, as a precondition, a manufacturing method must be able to tolerate a variation range of the C content when manufacturing a slab. That is, 1 kgf /
In order to achieve a BH amount of at least 2 mm2 and no stretcher strain at all, the C content, which has the greatest effect on these properties, can be achieved with a slab within the control range of the current steelmaking components. This is because an industrially meaningless invention is required unless the production method is appropriate. Therefore, assuming C: ± 10 ppm, which is a range of variation of the C content when producing a cast piece of ultra-low carbon steel in the current steelmaking,
And, the range of the C and Nb contents for securing the r value, that is, C: 0.0010 to 0.0030 wt%, Nb:
The study was conducted on the premise that the steel had a composition of 0.007 to 0.020 wt%.

【0014】図1は、本発明のポイントであるの安定
して1kgf/mm2 以上のBH量を得ることストレッ
チャストレインが全く発生しないこと、とが両立できる
ことを示すもので、(a)は、C:0.0030wt
%,Nb:0.011wt%の鋼(本発明の範囲内の成
分範囲で、最もYP−Elが発生し易い成分)の冷延鋼
板を850℃で60secの再結晶焼鈍し、その後、図
のX軸として示す冷却速度で650℃まで冷却し、その
後、30℃/sで室温まで冷却して焼鈍板を造り、1.
0%の調質圧延を施し、冷延鋼板とした後、100℃×
4Hrのフル時効処理を行い、JIS−♯5片で引張り
試験を行いYP−Elを測定し、プロットしたものであ
る。また、(b)は、C:0.0010wt%,Nb:
0.014wt%の鋼(本発明の範囲内の成分範囲で、
最もBH量が得難い成分)の冷延鋼板のBH量(2%予
歪を与え、除荷後、170℃×20min時効処理し、
再引張りを行ったときのΔY.P)をプロットしたもの
である。
FIG. 1 shows that the point of the present invention is to achieve both the stable BH amount of 1 kgf / mm 2 or more and the absence of stretcher strain at all. C: 0.0030wt
%, Nb: A cold-rolled steel sheet of steel of 0.011 wt% (the component in which YP-El is most likely to be generated in the component range within the range of the present invention) is recrystallized and annealed at 850 ° C. for 60 sec. It is cooled to 650 ° C. at a cooling rate shown as the X axis, and then cooled to room temperature at 30 ° C./s to produce an annealed plate.
0% temper rolling, cold rolled steel sheet, 100 ℃ ×
This is a plot obtained by performing a full aging treatment of 4Hr, performing a tensile test with JIS- # 5 pieces, measuring YP-El, and plotting. (B) shows C: 0.0010 wt%, Nb:
0.014 wt% steel (with a component range within the scope of the present invention,
The BH amount of the cold-rolled steel sheet of the component (the component with the least BH amount) is given (2% prestrain is given, after unloading, aging treatment at 170 ° C. × 20 min)
ΔY when re-tension was performed. P) is plotted.

【0015】図1の(a),(b)から明らかなよう
に、本発明の方法であれば、現状の製鋼で極低炭素鋼の
鋳片を造るときのC含有量のバラツキの範囲であるC:
±10ppmを前提とし、且つ、r値を確保するための
C,Nb含有量の範囲、即ち、C:0.0010〜0.
0030wt%,Nb:0.007〜0.020wt%
の成分の鋼を前提とした鋳片を用いても、の安定して
1kgf/mm2 以上のBH量を得ることストレッチャ
ストレインが全く発生しないこと、とが両立できること
明かであり、本発明の工業的、経済的価値は大きい。
尚、従来技術の中で連続焼鈍の均熱後の冷却速度を10
℃/s(好ましくは50℃/s)以上とすることによっ
てBH性を付与する特公昭60−17004号公報の方
法では、同公報の第1図には、3℃/sで650℃まで
冷却した場合(本発明の図1とほぼ同じ焼鈍条件)BH
量がほぼ0(同公報のBH量はWH+BHで示されてい
るため、通常BH量として表現される値に換算するには
3.5〜4kgf/mm2 を引かねばならないのでほぼ
0となる)となっており、本発明の図1の結果と異なっ
た結果となっている。これは、C量が0.005wt
%,Nb=0.03wt%とNb含有量が0.03wt
%と本発明の範囲を大幅に越えていることが影響してい
るのではないかと考えられる。
As is clear from FIGS. 1 (a) and 1 (b), according to the method of the present invention, the range of variation of the C content at the time of producing a slab of ultra-low carbon steel with the current steelmaking is within a range. Some C:
The range of the C and Nb contents for assuming ± 10 ppm and securing the r value, that is, C: 0.0010 to 0.
0030 wt%, Nb: 0.007 to 0.020 wt%
It is clear that the use of a slab premised on steel having the following composition can achieve both a stable BH amount of 1 kgf / mm 2 or more and no stretch strain at all. The economic and economic value is great.
In the prior art, the cooling rate after soaking in continuous annealing was set at 10
In the method disclosed in Japanese Patent Publication No. Sho 60-17004, in which the BH property is imparted by increasing the temperature to 650 ° C. at 3 ° C./s (preferably 50 ° C./s). BH (substantially the same annealing conditions as in FIG. 1 of the present invention)
The amount is almost 0 (the BH amount in the publication is represented by WH + BH, so that 3.5 to 4 kgf / mm 2 must be subtracted to convert it into a value normally expressed as a BH amount, which is almost 0) This is a result different from the result of FIG. 1 of the present invention. This is because the C content is 0.005wt
%, Nb = 0.03 wt% and Nb content is 0.03 wt%
It is considered that the fact that the percentage and the range significantly exceed the scope of the present invention may have an effect.

【0016】以下に鋼の化学成分条件について詳細に述
べる。Cは、優れた深絞り性や非ストレッチャストレイ
ン性と耐デント性を確保する上で重要な元素で、0.0
030wt%超になると、r値が低下しより厳しい深絞
り性が要求されるような用途への適用が出来なくなるの
で、0.0030wt%以下に規制する必要がある。ま
た、0.0010wt%未満になると安定して1kgf
/mm2 以上のBH量が確保できなくなるので、0.0
010wt%以上に規制する必要がある。
Hereinafter, the chemical composition conditions of steel will be described in detail. C is an important element for securing excellent deep drawability, non-stretch strainability and dent resistance.
If the content exceeds 030 wt%, the r value decreases and it becomes impossible to apply to applications that require stricter deep drawability, so it is necessary to regulate the content to 0.0030 wt% or less. Also, if the content is less than 0.0010 wt%, 1 kgf
/ Mm 2 or more, the BH amount cannot be secured.
It must be regulated to 010 wt% or more.

【0017】Si,Mn,Pは、何れも、鋼板の強度を
上昇させる元素で、強度を上昇させるために必要に応じ
添加すればよいが、Siは、0.50wt%超になると
塗装密着性が悪くなるため、Mnは、0.23wt%
になるとr値が劣化するので、そして、Pは、0.15
0wt%超になると鋳片のPの偏析が大きくなり、Pバ
ンド欠陥と称する表面欠陥が発生し、自動車外板として
使えなくなるので、それぞれ、上限値を0.50wt
%,0.80wt%,0.150wt%と規制する必要
がある。尚、Siは、少なくても何等障害にならないの
で特に規制する必要がないが、Mnは、熱延の耳あれ性
を防止するために少なくとも0.02wt%、Pは、高
強度鋼板としての強度を得るために0.035wt%は
必要であるので、それぞれ、下限値を0.02wt%,
0.035wt%と規制する必要がある。
Si, Mn, and P are all elements that increase the strength of the steel sheet, and may be added as needed to increase the strength. However, when the Si content exceeds 0.50 wt%, the coating adhesion is increased. Is deteriorated, so that when Mn exceeds 0.23 wt% , the r value deteriorates, and P becomes 0.15 wt%.
If the content exceeds 0 wt%, the segregation of P in the slab becomes large, and a surface defect called a P band defect occurs, which makes it unusable as an automobile outer plate.
%, 0.80 wt%, and 0.150 wt%. It should be noted that Si does not cause any hindrance at least, so there is no particular need to regulate it. However, Mn is at least 0.02 wt% in order to prevent hot rolling, and P is the strength as a high-strength steel sheet. Since 0.035 wt% is necessary to obtain, the lower limits are 0.02 wt% and 0.035 wt%, respectively.
It is necessary to regulate to 0.035 wt%.

【0018】Sは、0.030wt%超になると熱延の
耳あれ性が劣化するようになるので0.030wt%に
規制する必要がある。尚、下限値は、いくら少なくても
障害にならないので特に規制する必要がない。sol.
Alは、NをAlNとして固定しストレッチャストレイ
ンの発生を防止する必要があるので、0.025wt%
以上は必要である。又、0.100wt%超になると鋳
造時に溶鋼の空気酸化が起こり易くなり介在物量が増
え、加工性や、めっき品質をも劣化させるようになるの
で0.100wt%を上限値とした。Nは、Alによっ
てAlNとして固定され無害化が成されるが、0.01
00wt%超になるとAlNが多くなりすぎr値が劣化
するようになるので、上限値を0.0100wt%とし
た。尚、通常の製鋼向上では0.0005wt%未満に
することは困難であるので下限値を0.0005wt%
とした。
If the content of S exceeds 0.030 wt%, the reversibility of hot rolling deteriorates, so it is necessary to regulate S to 0.030 wt%. It should be noted that the lower limit value does not need to be particularly restricted because it does not cause any trouble even if it is small. sol.
Since it is necessary to fix N as AlN to prevent the occurrence of stretch strain, Al is 0.025 wt%.
The above is necessary. On the other hand, if the content exceeds 0.100 wt%, air oxidation of molten steel tends to occur at the time of casting, the amount of inclusions increases, and the workability and plating quality also deteriorate, so 0.100 wt% was made the upper limit. N is fixed as AlN by Al and detoxified, but 0.01%.
If it exceeds 00 wt%, AlN becomes too large and the r-value deteriorates. Therefore, the upper limit is set to 0.0100 wt%. In addition, it is difficult to reduce the content to less than 0.0005 wt% in ordinary steelmaking improvement, so the lower limit is 0.0005 wt%.
And

【0019】Nb含有量は、0.007wt%未満であ
ったり、0.020wt%超である場合は、優れたr値
が得られないので、0.007wt%〜0.0200w
t%に規制する必要がある。Nbが0.007wt%未
満の場合は、熱延板の結晶粒径を細粒化することが不十
分となるとともにCをNbCとして十分に固定できなく
なり、その結果として焼鈍板のr値が十分高くならなく
なる。また、0.020wt%超になると、固溶Nb量
が多くなり焼鈍時の結晶粒の成長が抑制されr値が十分
に高くならなくなる。また、Nb量は、非ストレッチャ
ストレイン性を確保するには、Nb(wt%):7.7
5×wt%C−0.013以上添加する必要がある。更
に、BH量を安定して1kgf/mm2 以上確保するに
は、Nb(wt%):7.75×wt%C+0.007
以下とする必要がある。
If the Nb content is less than 0.007 wt% or more than 0.020 wt%, an excellent r value cannot be obtained, so that 0.007 wt% to 0.0200 w
It is necessary to regulate to t%. If Nb is less than 0.007 wt%, it is not enough to reduce the crystal grain size of the hot-rolled sheet, and C cannot be sufficiently fixed as NbC. As a result, the r-value of the annealed sheet is not sufficient. It will not be higher. On the other hand, if the content exceeds 0.020 wt%, the amount of solute Nb increases, and the growth of crystal grains during annealing is suppressed, so that the r value does not become sufficiently high. Further, the Nb amount is set to Nb (wt%): 7.7 in order to secure the non-stretch strain property.
It is necessary to add 5 × wt% C−0.013 or more. Further, in order to stably secure the BH amount of 1 kgf / mm 2 or more, Nb (wt%): 7.75 × wt% C + 0.007
It is necessary to:

【0020】B含有量は、特に耐二次加工性が要求され
ない用途に用いる場合は添加する必要はないが、耐二次
加工性が要求される用途に用いる場合は、B(wt
%):0.004×wt%P以上、0.0010wt%
以下で且つ、B/N≦0.7(wt%比)の範囲で添加
すればよい。BはTi添加極低炭素鋼に微量添加するこ
とによって二次加工性が改善できることがよく知られて
いるが同時にr値も低下することもよく知られている。
本発明者等は、二次加工性と深絞り性とを両立させる方
法について種々検討し本発明の請求項(2)の製造方法
を見出した。B含有量が、0.0010wt%超或いは
B/Nが0.7(wt%比)超となるとBNが生成する
ようになり、その結果としてr値が低下するようになる
が、B含有量が本発明の範囲での添加ではr値の劣化は
殆ど生じないのである。一方、二次加工性は、B(wt
%):0.004×wt%P以上の添加で顕著に向上す
る。
The B content need not be added particularly when used in applications where secondary processing resistance is not required. However, when used in applications where secondary processing resistance is required, B (wt.
%): 0.004 × wt% P or more, 0.0010 wt%
It may be added below and in the range of B / N ≦ 0.7 (wt% ratio). It is well known that secondary workability can be improved by adding a small amount of B to a Ti-added ultra-low carbon steel, but it is also well known that the r-value is also reduced at the same time.
The present inventors have studied various methods for achieving both secondary workability and deep drawability, and have found a manufacturing method according to claim (2) of the present invention. When the B content exceeds 0.0010 wt% or the B / N exceeds 0.7 (wt% ratio), BN is generated, and as a result, the r value decreases. However, addition within the range of the present invention hardly causes deterioration of the r value. On the other hand, the secondary workability is B (wt
%): Notably improved by adding 0.004 × wt% P or more.

【0021】以下、鋼板の成分構成条件以外の製造条件
について詳細に述べる。鋳片の製造条件は、各請求項の
鋼の成分が得られる方法であればどのような方法でもよ
く、特に規制する必要はない。熱延条件は、特に規制す
る必要がなく、鋳片を、Ar3 以上で仕上げ圧延を行い
巻き取り熱延鋼帯とすればよい。尚、N含有量が多い場
合や加熱温度が高温の場合は680℃以上の巻き取り温
度を採用することでより良好なr値が得られ、必要に応
じて採用すればよい。冷間圧延は、特に規制する必要が
なく通常の方法でよい。連続焼鈍方法は、750〜89
0℃に加熱し再結晶焼鈍を行い、その後、冷却を行うに
当たり、少なくとも730℃までの間を、2℃/s以上
10℃/s未満の冷却速度で冷却し、焼鈍板を造る必要
がある。焼鈍温度が750℃未満では十分なr値が得ら
れず、890℃超では良好な形状の鋼板が得られない。
Hereinafter, the manufacturing conditions other than the constituent conditions of the steel sheet will be described in detail. The production conditions of the cast slab may be any method as long as the components of the steel of each claim can be obtained, and need not be particularly limited. There is no particular restriction on the hot rolling conditions, and the cast slab may be subjected to finish rolling with Ar 3 or more to form a rolled hot rolled steel strip. When the N content is large or when the heating temperature is high, a better r-value can be obtained by using a winding temperature of 680 ° C. or higher, and may be adopted as needed. The cold rolling does not need to be particularly restricted, and may be a usual method. The continuous annealing method is 750 to 89
After heating to 0 ° C. to perform recrystallization annealing, and then cooling, it is necessary to cool at least to 730 ° C. at a cooling rate of 2 ° C./s or more and less than 10 ° C./s to produce an annealed plate. . If the annealing temperature is lower than 750 ° C., a sufficient r value cannot be obtained, and if it exceeds 890 ° C., a steel sheet having a good shape cannot be obtained.

【0022】焼鈍後の冷却速度は、BH量とストレッチ
ャストレインの発生に大きく影響し、図1に示すよう
に、2℃/s以上10℃/s未満の冷却速度で冷却しな
ければならない。また、この効果は、少なくとも730
℃までを2℃/s以上10℃/s未満の冷却速度で冷却
することで得られる。尚、過時効処理については特に規
制する必要はない。調質圧延は、0.5%未満では如何
に耐ストレッチャストレインに優れた焼鈍板を製造した
としてもプレス時のストレッチャストレインの発生を防
止することが出来ないので0.5%以上を施さねばなら
ない。尚、3%超では延性の劣化が大きいので3%未満
に規制する必要がある。
The cooling rate after annealing greatly affects the amount of BH and the occurrence of stretch strain, and as shown in FIG. 1, cooling must be performed at a cooling rate of 2 ° C./s or more and less than 10 ° C./s. Also, this effect is at least 730
It is obtained by cooling at a cooling rate of not less than 2 ° C./s and less than 10 ° C./s. Note that there is no particular need to regulate the overaging treatment. If the temper rolling is less than 0.5%, no matter how much an annealed sheet having excellent stretch-strain resistance is produced, it is not possible to prevent the occurrence of stretch-strain at the time of pressing, so 0.5% or more must be applied. . If it exceeds 3%, the ductility is greatly deteriorated, so it is necessary to regulate it to less than 3%.

【0023】[0023]

【実施例】以下に本発明の効果を実施例により説明す
る。表1に示す成分の鋳片を造り、表2に示す連続熱延
条件で3.8mmの熱延板を製造し、酸洗後0.65m
mに冷間圧延を行い、連続焼鈍で850℃×60sec
の再結晶焼鈍を行い均熱後の冷却速度を表2に示す条件
で冷却した後400℃の過時効処理帯を通過させた後室
温まで冷却して焼鈍板を製造し、その後1.0%の調質
圧延を施して35〜38kgf/mm2 級の高強度冷延
鋼板を製造した。製造した高強度冷延鋼板の材質を調査
し、表2に示す。Y.P,T.S,El、r値は調質圧
延後の特性値、YP−Elは100℃×4Hrの時効処
理を施した後の値、BH量の測定条件は予歪量は2%,
塗装焼き付け相当熱処理条件を170℃×20minと
した時の値である。また、二次加工性は絞り比2.52
でカップを絞り−40℃でカップを押しつぶした時の脆
性破断の長さで評価し全く割れなかったものを◎5mm
以下のものを〇それ以上を×として評価した。
EXAMPLES The effects of the present invention will be described below with reference to examples. A slab of the components shown in Table 1 was produced, and a hot-rolled sheet of 3.8 mm was manufactured under the continuous hot-rolling conditions shown in Table 2, and 0.65 m after pickling.
m, cold-rolled to 850 ° C x 60sec by continuous annealing
And then cooled under the conditions shown in Table 2 after soaking, passed through an overage treatment zone at 400 ° C., and then cooled to room temperature to produce an annealed sheet. , To produce a 35-38 kgf / mm 2 class high-strength cold-rolled steel sheet. The materials of the manufactured high-strength cold-rolled steel sheets were investigated and are shown in Table 2. Y. P, T. The S, El, and r values are characteristic values after temper rolling, YP-El is a value after aging treatment at 100 ° C. × 4 hours, and the BH amount is measured under a pre-strain amount of 2%.
These values are obtained when the heat treatment conditions equivalent to paint baking are 170 ° C. × 20 min. The secondary workability was 2.52.
The cup was squeezed at −40 ° C., and the length of the brittle fracture when the cup was crushed was evaluated.
The following items were evaluated as 〇 and more as ×.

【0024】[0024]

【表1】 [Table 1]

【0025】[0025]

【表2】 [Table 2]

【0026】鋼A,B,C,Dは、何れも本発明の成分
範囲内の鋼で、鋼AはBを添加しない請求項1の成分の
鋼、鋼B,C,Dは、本発明の請求項2のB添加量のそ
れぞれの下限値の3.3,3.1,4.4ppm以上の
6,6,9ppm添加した鋼、その内D鋼はPを0.1
10wt%添加し38kgf/mm2 級の高強度冷延鋼
板を製造する成分の鋼である。鋼Eは、C含有量を0.
0040wt%,Nb含有量を0.040wt%と本発
明の範囲より高い例で、従来法の特公昭60−1700
4号公報に準ずる鋼成分の例である。鋼Fは、Nb含有
量が0.003wt%と本発明鋼の範囲を下回った比較
例である。鋼Gは、C含有量を0.0040wt%,B
含有量を0.0045wt%とBを本発明の範囲より多
量に添加した例で、従来法の特開昭58−84928号
公報に準ずる鋼成分の例である。鋼Hは、C含有量が
0.0011wt%,Nb含有量が0.019wt%と
請求項の(1)式のNb含有量の上限値(7.75×w
t%C(0.0011)=0.0155%)を外れた鋼
成分の例である。鋼Iは、B含有量を0.0038wt
%とBを本発明の範囲より多量に添加した鋼成分の例で
ある。
The steels A, B, C and D are all steels within the composition range of the present invention, and the steels A, B, C and D according to the present invention do not contain B. The steel added with 6, 6, 9 ppm of not less than 3.3, 3.1, 4.4 ppm of the lower limit of the amount of B added according to claim 2 in which D steel has P of 0.1.
10 wt% added steel to produce 38 kgf / mm 2 class high strength cold rolled steel sheet. Steel E has a C content of 0.1.
0040 wt% and Nb content of 0.040 wt% which are higher than the range of the present invention.
4 is an example of a steel component according to Japanese Patent Publication No. 4 (Kokai) No. 4; Steel F is a comparative example in which the Nb content was 0.003 wt%, which was below the range of the steel of the present invention. Steel G has a C content of 0.0040 wt%, B
This is an example in which the content is 0.0045 wt% and B is added in a larger amount than the range of the present invention, and is an example of a steel component according to the conventional method of Japanese Patent Application Laid-Open No. 58-84928. The steel H has a C content of 0.0011 wt% and an Nb content of 0.019 wt%, the upper limit of the Nb content (7.75 × w) in the formula (1).
It is an example of a steel component deviating from t% C (0.0011) = 0.0155%). Steel I has a B content of 0.0038 wt.
2 is an example of a steel component in which% and B are added in a larger amount than the range of the present invention.

【0027】試料1,2,3,5は、何れも本発明の実
施例で、試料4は連続焼鈍時の均熱後の冷却速度が1℃
/sと本発明の範囲を下回る比較例、試料7は成分が本
発明外の比較例、試料6,8の焼鈍条件は本発明の条件
であるが鋼成分が従来法の成分である比較例である。試
料1,2,3,5は、何れも時効後のYP−El,BH
量,r値の全てが優れた値になっており、本発明の方法
によって、耐デント性に優れたストレッチャストレイン
の発生しない深絞り用高強度冷延鋼板が製造できること
がわかる。また、得られた焼鈍板は何れも良好な形状が
得られており、本発明の冷却速度を10℃/s未満とす
る製造方法は良好な形状の鋼板を安定して得られると言
う点においても優れていることがわかる。
Samples 1, 2, 3, and 5 are all examples of the present invention. Sample 4 has a cooling rate of 1 ° C. after soaking during continuous annealing.
/ S, which is lower than the range of the present invention, sample 7 is a comparative example in which the components are out of the present invention, and samples 6 and 8 have annealing conditions of the present invention but steel components are conventional components. It is. Samples 1, 2, 3, and 5 were all YP-El, BH after aging.
The amounts and r values are all excellent values, and it is understood that the method of the present invention can produce a high-strength cold-rolled steel sheet for deep drawing with excellent dent resistance and free of stretcher strain. In addition, all the obtained annealed sheets have a good shape, and the manufacturing method of the present invention in which the cooling rate is less than 10 ° C./s can stably obtain a steel sheet having a good shape. It can be seen that is also excellent.

【0028】また、請求項2の実施例である試料2,
3,5は耐二次加工性をも優れており、本発明のB(w
t%)を0.004×wt%P以上、0.0010wt
%以下で、且つ、B/N≦0.7(wt%比)の範囲と
することで優れた二次加工性をも付与することができる
ことがわかる。一方、比較例の鋼4は、連続焼鈍の冷却
条件が1℃/sと本発明の範囲を下回った条件のもの
で、BH量が0.5kgf/mm2 と低い値しか得られ
ておらず、本発明の実施例である試料3と比較すると、
連続焼鈍の冷却条件を2〜10℃/sとする本発明の製
造方法が優れているかがよくわかる。また、鋼6,7,
8,9,10は何れも比較例で、鋼6はC量が0.00
40wt%,及びNb量が0.040wt%と、鋼7は
Nb量が0.003wt%と、鋼8はB量が0.004
5wt%と、鋼9はNb量が請求項に記載の式の上限値
を超えて0.019wt%と、鋼10はB量が0.00
38wt%と、本発明の鋼成分範囲を外れた比較例で、
鋼6はBH量とr値が、鋼7,8,10はr値が、鋼9
はBH量が、劣悪な特性値となっている。
The sample 2 according to the embodiment of claim 2
Nos. 3 and 5 also have excellent secondary workability, and the B (w) of the present invention
t%) is 0.004 x wt% P or more, 0.0010 wt%
% Or less and B / N ≦ 0.7 (wt% ratio), it can be seen that excellent secondary workability can also be imparted. On the other hand, in the steel 4 of the comparative example, the cooling condition of the continuous annealing was 1 ° C./s, which was lower than the range of the present invention, and the BH amount was as low as 0.5 kgf / mm 2. In comparison with Sample 3 which is an example of the present invention,
It is clear that the manufacturing method of the present invention in which the cooling conditions for continuous annealing are 2 to 10 ° C./s is excellent. In addition, steel 6,7,
8, 9, and 10 are all comparative examples, and steel 6 has a C content of 0.00.
40 wt%, Nb content is 0.040 wt%, Steel 7 has Nb content of 0.003 wt%, and Steel 8 has B content of 0.004 wt%.
5 wt%, steel 9 has an Nb content of 0.019 wt% exceeding the upper limit of the expression according to the claim, and steel 10 has a B content of 0.00.
38 wt%, a comparative example out of the steel component range of the present invention,
Steel 6 has a BH content and r value, steels 7, 8, and 10 have an r value, and steel 9
Indicates that the BH amount is an inferior characteristic value.

【0029】以上の実施例の結果から明らかなように、
本発明の請求項1の製造方法によって、耐デント性に優
れたストレッチャストレインの発生しない深絞り用高強
度冷延鋼板が、請求項2の方法によって、耐二次加工性
に優れた特性をも付与することが出来、工業的価値が極
めて高いことがわかる。尚、本発明の製造方法は、電気
亜鉛メッキ等の各種の表面処理鋼板の原板の製造方法と
しても、また、溶融亜鉛メッキ鋼板の製造に於いても同
じ効果が得られる。
As is clear from the results of the above embodiments,
According to the production method of claim 1 of the present invention, a high-strength cold-rolled steel sheet for deep drawing that does not generate a stretcher strain and has excellent dent resistance can also have characteristics with excellent secondary workability by the method of claim 2. It can be given, and it is understood that the industrial value is extremely high. The same effect can be obtained by the production method of the present invention as a method for producing an original sheet of various surface-treated steel sheets such as electrogalvanizing, and also in producing a hot-dip galvanized steel sheet.

【0030】[0030]

【発明の効果】以上、本発明について詳細に説明した
が、本発明の製造方法によって、耐デント性に優れたス
トレッチャストレインの発生しない深絞り用高強度冷延
鋼板を製造することができる優れた効果が発揮出来、そ
の工業的価値は大である。
As described above, the present invention has been described in detail. According to the manufacturing method of the present invention, it is possible to manufacture a high-strength cold-rolled steel sheet for deep drawing with excellent dent resistance and free of stretcher strain. The effect can be demonstrated and its industrial value is great.

【図面の簡単な説明】[Brief description of the drawings]

【図1】連続焼鈍の冷却速度と時効後のYP−El、B
H量との関係を示す図である。
FIG. 1: Cooling rate of continuous annealing and YP-El, B after aging
It is a figure which shows the relationship with H amount.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 芳賀 裕和 兵庫県姫路市広畑区富士町1番地 新日 本製鐵株式会社 広畑製鐵所内 (56)参考文献 特開 平6−108153(JP,A) 特開 昭63−241122(JP,A) 特開 平6−116651(JP,A) 特開 平2−232316(JP,A) (58)調査した分野(Int.Cl.7,DB名) C21D 9/46 - 9/48 C21D 8/02 - 8/04 C22C 38/00 - 38/60 ────────────────────────────────────────────────── ─── Continuing on the front page (72) Inventor Hirokazu Haga 1-Fuji-cho, Hirohata-ku, Himeji-shi, Hyogo Nippon Steel Corporation Hirohata Works (56) References JP-A-6-108153 (JP, A JP-A-63-241122 (JP, A) JP-A-6-116651 (JP, A) JP-A-2-232316 (JP, A) (58) Fields investigated (Int. Cl. 7 , DB name) C21D 9/46-9/48 C21D 8/02-8/04 C22C 38/00-38/60

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 C:0.0010〜0.0030wt
%,Si≦0.50wt%,Mn:0.02〜0.23
wt%,P:0.035〜0.150wt%,S≦0.
030wt%,sol.Al:0.025〜0.100
wt%,N:0.0005〜0.0100wt%,N
b:0.007〜0.020wt%で、且つ、C量とN
b量の関係が下記式の範囲を満たし残部不可避的不純物
及び鉄よりなる鋳片を、Ar3 以上で仕上げ圧延を行い
巻き取り熱延鋼帯とし、冷間圧延を行い、連続焼鈍法で
750〜890℃に加熱し再結晶焼鈍を行い、その後、
冷却を行うに当たり、少なくとも730℃までの間を、
2℃/s以上10℃/s未満の冷却速度で冷却し、焼鈍
板を造り、その後、0.5〜3%の調質圧延を行うこと
を特徴とする耐デント性に優れたストレッチャストレイ
ンの発生しない深絞り用高強度冷延鋼板の製造方法。 Nb:7.75 ×wt% C−0.013 ≦Nb(wt%)≦7.75 ×
wt% C+0.007
1. C: 0.0010 to 0.0030 wt.
%, Si ≦ 0.50 wt%, Mn: 0.02 to 0.23
wt% , P: 0.035 to 0.150 wt% , S ≦ 0.
030 wt%, sol. Al: 0.025 to 0.100
wt%, N: 0.0005 to 0.0100 wt%, N
b: 0.007 to 0.020 wt%, C content and N
A slab having the relationship of the amount of b satisfying the range of the following formula and the balance consisting of unavoidable impurities and iron is subjected to finish rolling with Ar 3 or more to form a rolled hot-rolled steel strip, cold-rolled, and 750 by a continuous annealing method. To 890 ° C to perform recrystallization annealing, and then
When performing cooling, at least up to 730 ° C.
A stretcher strain having excellent dent resistance, characterized in that it is cooled at a cooling rate of 2 ° C./s or more and less than 10 ° C./s to produce an annealed plate, and then to perform a temper rolling of 0.5 to 3%. A method for producing high-strength cold-rolled steel sheets for deep drawing that does not occur. Nb: 7.75 × wt% C−0.013 ≦ Nb (wt%) ≦ 7.75 ×
wt% C + 0.007
【請求項2】 請求項1記載の方法に於いて、鋼の組成
を、更に、B(wt%)を0.004×wt%P以上、
0.0010wt%以下で、且つ、B/N≦0.7(w
t%比)の範囲とすることを特徴とする優れた二次加工
性をも付与する製造方法。
2. The method according to claim 1, wherein the composition of the steel and the content of B (wt%) are 0.004 × wt% P or more.
0.0010 wt% or less, and B / N ≦ 0.7 (w
(t% ratio) in a range that also provides excellent secondary workability.
JP06243989A 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain Expired - Fee Related JP3110624B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP06243989A JP3110624B2 (en) 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP06243989A JP3110624B2 (en) 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain

Publications (2)

Publication Number Publication Date
JPH08104926A JPH08104926A (en) 1996-04-23
JP3110624B2 true JP3110624B2 (en) 2000-11-20

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JP5556483B2 (en) * 2010-08-03 2014-07-23 新日鐵住金株式会社 Continuous annealing method for steel sheet using continuous annealing furnace
JPWO2020003986A1 (en) * 2018-06-27 2020-07-02 Jfeスチール株式会社 Cold rolled steel sheet, hot dip galvanized steel sheet, and method for manufacturing alloyed hot dip galvanized steel sheet
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