JPH08104926A - Production of high strength cold rolled steel sheet for deep drawing excellent in dent resistance and free from generation of stretcher strain - Google Patents

Production of high strength cold rolled steel sheet for deep drawing excellent in dent resistance and free from generation of stretcher strain

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Publication number
JPH08104926A
JPH08104926A JP24398994A JP24398994A JPH08104926A JP H08104926 A JPH08104926 A JP H08104926A JP 24398994 A JP24398994 A JP 24398994A JP 24398994 A JP24398994 A JP 24398994A JP H08104926 A JPH08104926 A JP H08104926A
Authority
JP
Japan
Prior art keywords
steel sheet
rolled steel
steel
deep drawing
present
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP24398994A
Other languages
Japanese (ja)
Other versions
JP3110624B2 (en
Inventor
Teruaki Yamada
輝昭 山田
Masahiko Oda
昌彦 織田
Yasunaga Ootaki
康長 大滝
Hirokazu Haga
裕和 芳賀
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP06243989A priority Critical patent/JP3110624B2/en
Publication of JPH08104926A publication Critical patent/JPH08104926A/en
Application granted granted Critical
Publication of JP3110624B2 publication Critical patent/JP3110624B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Heat Treatment Of Sheet Steel (AREA)

Abstract

PURPOSE: To produce a high strength cold rolled steel sheet capable of producing without troubles such as deterioration in the shape of the steel sheet by a contin uous annealing method and capable of withstanding severer deep drawing such as fender. CONSTITUTION: A slab having a compsn. contg., by weight, 0.0010 to 0.0030% C, <=0.50% Si, 0.02 to 0.80% Mn, 0.035 to 0.150% P, <=0.030% S, 0.025 to 0.100% sol.Al, 0.0005 to 0.0100% N and 0.007 to 0.020% Nb, furthermore satisfying 7.75×C-0.013<=Nb<=7.75×C+0.007, and the balance iron with inevitable impurities is subjected to finish rolling at the Ar3 or above and is coiled to form into a hot rolled steel strip, which is subjected to cold rolling and is subjected to recrystallization annealing under heating to 750 to 890 deg.C by a continuous annealing method. Next, at the time of executing cooling, it is cooled at least to 730 deg.C at 2 to <10 deg.C/s cooling rate to make an annealed sheet, and after that, it is subjected to skin-pass rolling of 0.5 to 3%.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、耐デント性の優れた深
絞り用高強度冷延鋼板の製造方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a high strength cold rolled steel sheet for deep drawing which is excellent in dent resistance.

【0002】[0002]

【従来の技術】従来、耐デント性の優れた高強度冷延鋼
板は、自動車の外板パネルに主として使われている。そ
の従来技術としては、これまで耐デント性の優れた高強
度冷延鋼板の製造方法として、特開昭60−17485
2号、特開昭57−76131号、特公昭60−170
04号公報、更に、Bを添加し二次加工性をも付与する
方法として、特開昭58−84928号公報がある。す
なわち、特開昭60−174852号公報は、連続焼鈍
温度をAc3 以上1000℃以下とし複合組織を造る方
法で、特開昭57−76131号公報は、連続焼鈍温度
を900℃〜Ac3 とする方法であり、何れも連続焼鈍
の焼鈍温度が極めて高いのが特徴であるが、そのため、
通常の連続焼鈍設備では、900℃を越えるような高温
の鋼帯が炉内のハースロールを通過すると鋼板が軟らか
過ぎて絞り込まれ皺が発生し良好な形状の板が製造でき
なくなると言う問題がある。
2. Description of the Related Art Conventionally, high-strength cold-rolled steel sheets having excellent dent resistance have been mainly used for outer panel of automobiles. As the conventional technique, there has been disclosed a method for producing a high strength cold rolled steel sheet having excellent dent resistance, which has been disclosed in JP-A-60-17485.
No. 2, JP-A-57-76131, JP-B-60-170.
No. 04, and JP-A No. 58-84928 discloses a method of adding B to impart secondary workability. That is, JP-A-60-174852 is a method for producing a composite structure with a continuous annealing temperature of Ac 3 to 1000 ° C., and JP-A-57-76131 discloses a continuous annealing temperature of 900 ° C. to Ac 3 . It is a feature that the annealing temperature of continuous annealing is extremely high in both methods.
In a normal continuous annealing facility, when a steel strip having a high temperature exceeding 900 ° C. passes through a hearth roll in the furnace, the steel sheet is too soft and is narrowed down to cause wrinkles, which makes it impossible to produce a well-shaped sheet. is there.

【0003】また、特公昭60−17004号公報は、
連続焼鈍時に均熱後の冷却において、少なくとも650
℃以上の温度域を10℃/s以上(好ましくは50℃/
s以上)の急速冷却で冷却することで、焼付硬化性の優
れた深絞り用冷延鋼板を製造する方法であるが、例え
ば、同公報で好ましい範囲とされているような50℃/
sのような急速冷却で均熱後の冷却を行えば、冷却速度
が著しく速いために、鋼帯がハースロールを通過する際
に、鋼帯の温度とハースロール温度を一致させることが
難しくなり、鋼帯がハースロールにより急速に加熱され
たり或いは冷却されたりするために鋼板形状が悪くな
り、安定して良好な形状の鋼板の製造が困難であると言
う問題を抱えている。
Further, Japanese Patent Publication No. 60-17004 discloses
At least 650 in cooling after soaking during continuous annealing
Temperature range above ℃ 10 ℃ / s or more (preferably 50 ℃ /
It is a method of producing a cold-rolled steel sheet for deep drawing having excellent bake hardenability by cooling by rapid cooling of s or more), for example, 50 ° C. /
If the cooling is performed after soaking by rapid cooling such as s, the cooling rate is extremely high, and it becomes difficult to match the temperature of the steel strip and the hearth roll temperature when the steel strip passes through the hearth roll. However, since the steel strip is rapidly heated or cooled by the hearth roll, the shape of the steel sheet is deteriorated, and it is difficult to stably produce a steel sheet having a good shape.

【0004】更には、特開昭58−84928号公報
は、二次加工性の向上とNの悪影響を防止するために、
Bを重量比で0.8〜1.4添加する方法であるが、同
公報の補正後の第2表に示されているようにr値(以
下、ここでは深絞り特性の指標となるr値の面内平均値
を示す)は2.03と少し高い実施例もあるが1.6
3,1.65と云ったかなり低い深絞り性しか得られて
いない実施例をも含んでおり、更に厳しい深絞り性が要
求される最近の自動車のフェンダー用の高強度鋼板を安
定して製造することが困難であると言う問題がある。
Further, JP-A-58-84928 discloses that in order to improve the secondary workability and prevent the adverse effect of N,
This is a method of adding 0.8 to 1.4 by weight ratio of B, but as shown in the corrected Table 2 of the publication, the r value (hereinafter, r which is an index of the deep drawing characteristic is used. The average value of the values is 2.03, which is slightly higher than 2.03, but is 1.6.
It also includes examples in which a very low deep drawability such as 31.65 is obtained, and stably manufactures high-strength steel sheets for recent automobile fenders that require more severe deep drawability. There is a problem that it is difficult to do.

【0005】以上述べたように、最近の自動車のフェン
ダーのような、より厳しい深絞り加工にも耐えられる耐
デント性の優れた深絞り用高強度冷延鋼板を連続焼鈍法
で鋼板形状不良のトラブルもなく製造できる製造方法は
まだないのである。従って、この問題を解決するため
の、耐デント性の優れた深絞り用高強度冷延鋼板の製造
方法の提供が強く望まれている。
As described above, a high strength cold rolled steel sheet for deep drawing having excellent dent resistance, which can withstand even more severe deep drawing work, such as a recent automobile fender, has been produced by the continuous annealing method in the form of a defective steel sheet shape. There is still no manufacturing method that can be manufactured without trouble. Therefore, it has been strongly desired to provide a method for manufacturing a high strength cold rolled steel sheet for deep drawing, which is excellent in dent resistance and solves this problem.

【0006】[0006]

【発明が解決しようとする課題】本発明で解決しようと
する課題は、フェンダーのように、より厳しい深絞り加
工にも耐えられる耐デント性の優れたストレッチャスト
レインの発生しない深絞り用高強度冷延鋼板の製造方法
を提供することである。
SUMMARY OF THE INVENTION The problem to be solved by the present invention is to provide a high-strength cold drawing for deep drawing which does not cause stretcher strain with excellent dent resistance, which can withstand even deeper deep drawing like a fender. It is to provide a method for manufacturing a rolled steel sheet.

【0007】[0007]

【課題を解決するための手段】本発明者等は、上記課題
を解決する方法に付いて、(1)連続焼鈍法で鋼板形状
不良のトラブルもなく製造できる製造条件の検討を行
い、その上で、より厳しい深絞り加工にも耐えられる耐
デント性の優れた深絞り用高強度冷延鋼板の製造方法を
検討し、請求項1記載の方法を見出したものである。ま
た、更に、一部用途には、鋼板の特性値を劣化させない
で且つ二次加工性をも付与できる製造法を検討し、請求
項2記載の方法を見出したものである。
Means for Solving the Problems Regarding the method for solving the above-mentioned problems, the inventors of the present invention have studied (1) manufacturing conditions by which continuous annealing can be carried out without troubles such as defective steel sheet shape, and Then, a method for producing a high-strength cold-rolled steel sheet for deep drawing, which has excellent dent resistance and can withstand even more severe deep drawing, was studied, and the method according to claim 1 was found. Furthermore, for some uses, a manufacturing method that can impart secondary workability without deteriorating the characteristic values of the steel sheet was examined, and the method according to claim 2 was found.

【0008】その本発明の要旨は次の通りである。 (1)C:0.0010〜0.0030wt%,Si≦
0.50wt%,Mn:0.02〜0.80wt%,
P:0.035〜0.150wt%,S≦0.030w
t%,sol.Al:0.025〜0.100wt%,
N:0.0005〜0.0100wt%,Nb:0.0
07〜0.020wt%で、且つ、C量とNb量の関係
が下記式の範囲を満たし残部不可避的不純物及び鉄より
なる鋳片を、Ar3 以上で仕上げ圧延を行い巻き取り熱
延鋼帯とし、冷間圧延を行い、連続焼鈍法で750〜8
90℃に加熱し再結晶焼鈍を行い、その後、冷却を行う
に当たり、少なくとも730℃までの間を、2℃/s以
上10℃/s未満の冷却速度で冷却し、焼鈍板を造り、
その後、0.5〜3%の調質圧延を行うことを特徴とす
る耐デント性に優れたストレッチャストレインの発生し
ない深絞り用高強度冷延鋼板の製造方法。 Nb:7.75 ×wt% C−0.013 ≦Nb(wt%)≦7.75 ×
wt% C+0.007 (2)(1)記載の方法に於いて、鋼の組成を、更に、
B(wt%)を0.004×wt%P以上、0.001
0wt%以下で、且つ、B/N≦0.7(wt%比)の
範囲とすることを特徴とする優れた二次加工性をも付与
する製造方法にある。
The gist of the present invention is as follows. (1) C: 0.0010 to 0.0030 wt%, Si ≦
0.50 wt%, Mn: 0.02-0.80 wt%,
P: 0.035 to 0.150 wt%, S ≦ 0.030w
t%, sol. Al: 0.025 to 0.100 wt%,
N: 0.0005 to 0.0100 wt%, Nb: 0.0
A cast slab containing 07 to 0.020 wt% and having a relationship between the amount of C and the amount of Nb satisfying the range of the following formula and comprising the balance unavoidable impurities and iron is subjected to finish rolling with Ar 3 or more and rolled into a hot rolled steel strip. And cold rolling is performed, and it is 750-8 by the continuous annealing method.
Recrystallization annealing is performed by heating to 90 ° C., and then cooling is performed at least up to 730 ° C. at a cooling rate of 2 ° C./s or more and less than 10 ° C./s to form an annealed plate,
Then, 0.5-3% temper rolling is performed, and a method for producing a high-strength cold-rolled steel sheet for deep drawing, which is excellent in dent resistance and does not cause stretcher strain. Nb: 7.75 x wt% C-0.013 ≤ Nb (wt%) ≤ 7.75 x
wt% C + 0.007 (2) In the method described in (1), the composition of steel is further
B (wt%) 0.004 x wt% P or more, 0.001
It is a manufacturing method for imparting excellent secondary workability, which is characterized in that it is 0 wt% or less and B / N ≦ 0.7 (wt% ratio).

【0009】以下、本発明について詳細に述べる。本発
明者等は、本発明が解決しようとする課題について、
(1)通常の連続焼鈍設備で安定して良好な形状の鋼帯
を得る製造条件、(2)極低炭素冷延鋼板で造った外板
パネルのデント性と鋼板特性の関係、(3)良好なデン
ト性が得られる材質特性の冷延鋼板の製造方法について
検討し、本発明の方法を見出したものである。その考え
方は、下記に示す概要の通りである。 (1)通常の連続焼鈍設備で安定して良好な形状の鋼帯
を得る製造条件 自動車外板用の冷延鋼板は、板厚が0.60〜0.80
mmで板幅が1400〜1700mm程度の薄手広幅材
が主であるが、これらの冷延鋼板を連続焼鈍設備で製造
する上で最も障害となるのは、加熱温度が高い場合や高
い温度域で急激な冷却を行うとハースロール部のロール
クラウン(凸)による幅方向の圧縮応力による板の絞り
や、板温とロール温度との不一致により発生する熱応力
による板形状不良である。本発明者等はこの件に関し、
種々検討した結果、自動車外板に適用できるような良好
な形状の鋼帯を安定して得るには、少なくとも、焼鈍温
度を890℃以下とし、且つ、730℃以上の温度域の
冷却速度を少なくとも20℃/s未満とする必要がある
ことがわかった。
Hereinafter, the present invention will be described in detail. The present inventors, regarding the problems to be solved by the present invention,
(1) Manufacturing conditions for obtaining a steel strip having a stable and good shape by a normal continuous annealing equipment, (2) Relationship between dent property of outer panel made of ultra low carbon cold rolled steel sheet and steel sheet characteristics, (3) The method of the present invention was found by studying a method for producing a cold-rolled steel sheet having material characteristics capable of obtaining good dent property. The idea is as outlined below. (1) Manufacturing conditions for stably obtaining a good-shaped steel strip by a normal continuous annealing equipment Cold-rolled steel sheets for automobile outer plates have a sheet thickness of 0.60 to 0.80.
Although thin and wide materials with a width of 1 mm and a width of 1400 to 1700 mm are mainly used, the biggest obstacle in producing these cold-rolled steel sheets with continuous annealing equipment is when the heating temperature is high or in a high temperature range. When abrupt cooling is performed, the plate shape is narrowed due to compressive stress in the width direction due to the roll crown (convex) of the hearth roll portion, and the plate shape is defective due to thermal stress caused by the mismatch between the plate temperature and the roll temperature. The present inventors are concerned with this matter,
As a result of various studies, in order to stably obtain a steel strip having a good shape that can be applied to an automobile outer plate, at least an annealing temperature of 890 ° C. or lower and a cooling rate of at least 730 ° C. in a temperature range of at least It was found that it was necessary to set it to less than 20 ° C / s.

【0010】(2)極低炭素冷延鋼板で造った外板パネ
ルのデント性と鋼板特性の関係 一方、本発明者等は、極低炭素冷延鋼板で造った外板パ
ネルのデント性と鋼板特性の関係についても種々検討し
た結果、完全非時効性の極低炭素冷延鋼板で造った外板
パネルは、箱焼鈍法(BAF法)で製造した完全非時効
性の低炭素Alキルド冷延鋼板に比べて顕著にデント性
が劣っているが、極低炭素冷延鋼板でも固溶Cを存在せ
しめ、約1kgf/mm2 以上のBH性を付与した冷延
鋼板は顕著に耐デント性が向上することを見出した。即
ち、極低炭素冷延鋼板では、BAF法で製造した極低炭
素Al−K鋼の場合とは異なり、完全非時効性の鋼板の
デント性はY.P(0.2%耐力)の値以上に大きく低
下するが、BH量が1kgf/mm2 以上あるとBH後
のY.Pに対応した良好な耐デント性が確保できること
を知見したものであり、自動車外板用の冷延鋼板として
は必ずしも3kgf/mm2 以上のBHを付与する必要
がなく1kgf/mm2 以上のBH量を付与してやれば
よいことが明らかになった。尚、極低炭素冷延鋼板の耐
デント性が、BH量が0と1kgf/mm2 とでこの様
に大きく異なるのは、必ずしも明確になっているわけで
はないが、BH量が0の場合の弾性限が、Y.Pの50
〜60%程度しかないことに起因しているものと推察さ
れる。
(2) Relationship between Dentness of Outer Panel Made of Ultra-Low Carbon Cold Rolled Steel Sheet and Steel Sheet Properties On the other hand, the present inventors As a result of various studies on the relationship between steel sheet properties, an outer panel made of a completely non-aging ultra-low carbon cold-rolled steel sheet was found to be a completely non-aging low carbon Al-killed cold box produced by the box annealing method (BAF method). Although the dent property is remarkably inferior to that of the rolled steel plate, the cold rolled steel plate with BH property of about 1 kgf / mm 2 or more is remarkably dent resistant even if the ultra-low carbon cold rolled steel plate contains solid solution C. Have been found to improve. That is, in the ultra low carbon cold rolled steel sheet, unlike the case of the ultra low carbon Al-K steel manufactured by the BAF method, the dent property of the completely non-aging steel sheet is Y. P. (Powder strength 0.2%) is greatly reduced, but when the amount of BH is 1 kgf / mm 2 or more, Y.O. It was found that good dent resistance corresponding to P can be secured, and it is not always necessary to provide BH of 3 kgf / mm 2 or more as a cold-rolled steel sheet for automobile outer panels, and BH of 1 kgf / mm 2 or more is required. It became clear that the amount should be given. Incidentally, it is not always clear that the dent resistance of the ultra low carbon cold-rolled steel sheet differs greatly between BH amounts of 0 and 1 kgf / mm 2 , but it is not clear that the BH amount is 0. The elastic limit of Y. 50 of P
It is presumed that this is due to the fact that it is only about 60%.

【0011】(3)ストレッチャストレインの発生もな
く良好なデント性が得られる材質特性の冷延鋼板の製造
方法 より厳しい深絞り加工にも耐えられる耐デント性の優れ
た深絞り用高強度冷延鋼板の製造方法における重要な課
題は、の「より厳しい深絞り加工にも耐えられる優れ
たr値が得られること」、の「安定して1kgf/m
2 以上のBH量を得ることストレッチャストレインが
全く発生しないこと」、の上記(1)の「通常の連続
焼鈍設備で安定して良好な形状の鋼帯を得る製造条
件」、即ち、少なくとも、焼鈍温度を890℃以下と
し、且つ、730℃以上の温度域の冷却速度を少なくと
も20℃/s未満の条件で製造できることである。
(3) Method of manufacturing cold-rolled steel sheet having material characteristics capable of obtaining good dentability without occurrence of stretcher strain. High-strength cold-rolling for deep drawing excellent in dent resistance capable of withstanding more severe deep drawing. An important issue in the method of manufacturing a steel sheet is “to obtain an excellent r value that can withstand even deeper deep drawing”, and “stably 1 kgf / m.
"To obtain a BH amount of m 2 or more, no stretcher strain is generated at all", "(Conditions for producing a steel strip having a stable and good shape by a normal continuous annealing equipment", that is, at least, The annealing temperature is 890 ° C. or lower, and the cooling rate in the temperature range of 730 ° C. or higher can be manufactured under the condition of at least less than 20 ° C./s.

【0012】本発明者等は、先ず、の「通常の連続焼
鈍設備で安定して良好な形状の鋼帯を得る製造条件」、
即ち、少なくとも、焼鈍温度を890℃以下とし、且
つ、730℃以上の温度域の冷却速度を少なくとも20
℃/s未満の条件内で、のより厳しい深絞り加工にも
耐えられる優れたr値が得られる製造方法について検討
した。本発明者等は、ラボ真空溶解炉を用い、種々の成
分の鋼を溶製し、熱間圧延、冷間圧延、連続焼鈍、調質
圧延を行い検討した結果、BH性も得られ且つr値の高
い冷延鋼板が得られるのは、請求項1に示すような成分
の鋼でなければならないことを見出した。中でも、r値
に大きく影響するのは、C含有量とNb含有量である。
The inventors of the present invention firstly referred to “the manufacturing conditions for stably obtaining a steel strip having a good shape with a normal continuous annealing equipment”,
That is, at least the annealing temperature is 890 ° C. or lower, and the cooling rate in the temperature range of 730 ° C. or higher is at least 20.
Under the condition of less than ° C / s, a manufacturing method that can obtain an excellent r value that can withstand more severe deep drawing of was investigated. The inventors of the present invention conducted a study by performing melting of steels of various components using a laboratory vacuum melting furnace and performing hot rolling, cold rolling, continuous annealing and temper rolling, and as a result, BH property was also obtained and r It has been found that the cold rolled steel sheet having a high value must be obtained from the steel having the composition as set forth in claim 1. Among them, the C content and the Nb content have a great influence on the r value.

【0013】C含有量が0.0030wt%超になった
り、Nb含有量が0.007wt%未満であったり、
0.020wt%超となった場合は、r値が低下し十分
な深絞り性が得られない。特に、C含有量が0.003
0wt%超となった場合のr値の劣化は大きいことがわ
かった。次に、本発明者等は上記のC,Nb含有量の範
囲内で、の安定して1kgf/mm2 以上のBH量を
得ることとストレッチャストレインが全く発生しないこ
とを両立させる方法について検討した。この課題が製鉄
所で実質的に解決されるには、前提条件として、鋳片を
製造するときのC含有量のバラツキ範囲を許容できる製
造方法でなければならない。即ち、安定して1kgf/
mm2 以上のBH量を得ることとストレッチャストレイ
ンが全く発生しないことを両立させるためには、これら
特性に最も大きく影響するC含有量が現在の製鋼の成分
のコントロール範囲内の鋳片で達成可能な製造方法でな
ければ工業的に意味の無い発明となるからである。従っ
て、現状の製鋼で極低炭素鋼の鋳片を造るときのC含有
量のバラツキ範囲であるC:±10ppmを前提とし、
且つ、r値を確保するためのC,Nb含有量の範囲、即
ち、C:0.0010〜0.0030wt%,Nb:
0.007〜0.020wt%の成分の鋼を前提として
検討した。
If the C content exceeds 0.0030 wt% or the Nb content is less than 0.007 wt%,
If it exceeds 0.020 wt%, the r value decreases and sufficient deep drawability cannot be obtained. In particular, the C content is 0.003
It was found that the deterioration of the r value when the content was more than 0 wt% was large. Next, the inventors of the present invention examined a method for achieving both a stable BH amount of 1 kgf / mm 2 or more and no stretcher strain at all within the above C and Nb content ranges. . In order for this problem to be practically solved in a steel mill, as a precondition, it must be a manufacturing method that allows a variation range of the C content when manufacturing a cast slab. That is, 1 kgf /
In order to achieve both a BH amount of mm 2 or more and no stretcher strain at all, the C content that has the greatest effect on these properties can be achieved with a slab within the current steelmaking composition control range. This is because unless the manufacturing method is a proper manufacturing method, the invention is industrially meaningless. Therefore, assuming that C: ± 10 ppm, which is the variation range of the C content when producing an extremely low carbon steel slab with the current steelmaking,
In addition, the range of C and Nb contents for securing the r value, that is, C: 0.0010 to 0.0030 wt%, Nb:
The study was conducted on the premise of a steel having a composition of 0.007 to 0.020 wt%.

【0014】図1は、本発明のポイントであるの安定
して1kgf/mm2 以上のBH量を得ることストレッ
チャストレインが全く発生しないこと、とが両立できる
ことを示すもので、(a)は、C:0.0030wt
%,Nb:0.011wt%の鋼(本発明の範囲内の成
分範囲で、最もYP−Elが発生し易い成分)の冷延鋼
板を850℃で60secの再結晶焼鈍し、その後、図
のX軸として示す冷却速度で650℃まで冷却し、その
後、30℃/sで室温まで冷却して焼鈍板を造り、1.
0%の調質圧延を施し、冷延鋼板とした後、100℃×
4Hrのフル時効処理を行い、JIS−♯5片で引張り
試験を行いYP−Elを測定し、プロットしたものであ
る。また、(b)は、C:0.0010wt%,Nb:
0.014wt%の鋼(本発明の範囲内の成分範囲で、
最もBH量が得難い成分)の冷延鋼板のBH量(2%予
歪を与え、除荷後、170℃×20min時効処理し、
再引張りを行ったときのΔY.P)をプロットしたもの
である。
FIG. 1 shows that the point of the present invention is that it is possible to achieve a stable BH amount of 1 kgf / mm 2 or more and no stretcher strain at all, and (a) is C: 0.0030 wt
%, Nb: 0.011 wt% steel (in the composition range within the scope of the present invention, the component that is most prone to YP-El) cold-rolled steel sheet is recrystallized and annealed at 850 ° C. for 60 sec. Cool to 650 ° C. at the cooling rate shown as the X-axis, and then cool to room temperature at 30 ° C./s to make an annealed plate.
After subjecting to 0% temper rolling to make a cold rolled steel sheet, 100 ° C x
This is a plot obtained by performing a full aging treatment for 4 hours and performing a tensile test on a JIS- # 5 piece to measure YP-El. Further, (b) shows C: 0.0010 wt%, Nb:
0.014 wt% steel (within the composition range within the scope of the present invention,
BH amount (2% pre-strain is given to the cold rolled steel sheet with the most difficult component to obtain BH amount), after unloading, 170 ° C. × 20 min aging treatment,
ΔY when re-pulling was performed. P) is plotted.

【0015】図1の(a),(b)から明らかなよう
に、本発明の方法であれば、現状の製鋼で極低炭素鋼の
鋳片を造るときのC含有量のバラツキの範囲であるC:
±10ppmを前提とし、且つ、r値を確保するための
C,Nb含有量の範囲、即ち、C:0.0010〜0.
0030wt%,Nb:0.007〜0.020wt%
の成分の鋼を前提とした鋳片を用いても、の安定して
1kgf/mm2 以上のBH量を得ることストレッチャ
ストレインが全く発生しないこと、とが両立できること
明かであり、本発明の工業的、経済的価値は大きい。
尚、従来技術の中で連続焼鈍の均熱後の冷却速度を10
℃/s(好ましくは50℃/s)以上とすることによっ
てBH性を付与する特公昭60−17004号公報の方
法では、同公報の第1図には、3℃/sで650℃まで
冷却した場合(本発明の図1とほぼ同じ焼鈍条件)BH
量がほぼ0(同公報のBH量はWH+BHで示されてい
るため、通常BH量として表現される値に換算するには
3.5〜4kgf/mm2 を引かねばならないのでほぼ
0となる)となっており、本発明の図1の結果と異なっ
た結果となっている。これは、C量が0.005wt
%,Nb=0.03wt%とNb含有量が0.03wt
%と本発明の範囲を大幅に越えていることが影響してい
るのではないかと考えられる。
As is apparent from FIGS. 1 (a) and 1 (b), according to the method of the present invention, in the range of variation in the C content when producing a cast slab of ultra-low carbon steel by the current steelmaking. C:
The range of C and Nb contents for ensuring the r value, that is, C: 0.0010 to 0.
0030 wt%, Nb: 0.007 to 0.020 wt%
It is clear that even when using a cast slab premised on the steel of component (1), it is possible to obtain both a stable BH amount of 1 kgf / mm 2 or more, no stretcher strain at all, and the present invention. Has great economic and economic value.
In the prior art, the cooling rate after soaking in continuous annealing was 10
According to the method of Japanese Examined Patent Publication No. 60-17004, which imparts the BH property by setting the temperature to be not less than C / s (preferably 50 [deg.] C / s), in FIG. (Heat conditions similar to those of FIG. 1 of the present invention) BH
The amount is almost 0 (because the BH amount in the same publication is indicated by WH + BH, 3.5 to 4 kgf / mm 2 must be subtracted in order to convert it into a value normally expressed as the BH amount, which is almost 0). The result is different from the result of FIG. 1 of the present invention. This has a C content of 0.005 wt.
%, Nb = 0.03 wt% and Nb content is 0.03 wt
%, And it is considered that the influence greatly exceeds the range of the present invention.

【0016】以下に鋼の化学成分条件について詳細に述
べる。Cは、優れた深絞り性や非ストレッチャストレイ
ン性と耐デント性を確保する上で重要な元素で、0.0
030wt%超になると、r値が低下しより厳しい深絞
り性が要求されるような用途への適用が出来なくなるの
で、0.0030wt%以下に規制する必要がある。ま
た、0.0010wt%未満になると安定して1kgf
/mm2 以上のBH量が確保できなくなるので、0.0
010wt%以上に規制する必要がある。
The chemical composition conditions of steel will be described in detail below. C is an important element for ensuring excellent deep drawability, non-stretcher strain resistance and dent resistance.
If it exceeds 030 wt%, the r value decreases and it cannot be applied to applications requiring more stringent deep drawability. Therefore, it is necessary to regulate the content to 0.0030 wt% or less. Also, when the amount is less than 0.0010 wt%, it is stable at 1 kgf.
Since it is not possible to secure a BH amount of / mm 2 or more, 0.0
It is necessary to regulate it to 010 wt% or more.

【0017】Si,Mn,Pは、何れも、鋼板の強度を
上昇させる元素で、強度を上昇させるために必要に応じ
添加すればよいが、Siは、0.50wt%超になると
塗装密着性が悪くなるため、Mnは、0.80wt%超
になるとr値が劣化するので、そして、Pは、0.15
0wt%超になると鋳片のPの偏析が大きくなり、Pバ
ンド欠陥と称する表面欠陥が発生し、自動車外板として
使えなくなるので、それぞれ、上限値を0.50wt
%,0.80wt%,0.150wt%と規制する必要
がある。尚、Siは、少なくても何等障害にならないの
で特に規制する必要がないが、Mnは、熱延の耳あれ性
を防止するために少なくとも0.02wt%、Pは、高
強度鋼板としての強度を得るために0.035wt%は
必要であるので、それぞれ、下限値を0.02wt%,
0.035wt%と規制する必要がある。
Si, Mn, and P are all elements that increase the strength of the steel sheet, and may be added as necessary to increase the strength. However, if Si is more than 0.50 wt%, coating adhesion Is deteriorated, the r value is deteriorated when Mn exceeds 0.80 wt%, and P is 0.15
If it exceeds 0 wt%, the segregation of P in the slab becomes large, and surface defects called P band defects occur, and it cannot be used as an automobile outer plate. Therefore, the upper limit of each is 0.50 wt%.
%, 0.80 wt%, 0.150 wt% must be regulated. It should be noted that Si does not need to be restricted because it does not cause any hindrance at least, but Mn is at least 0.02 wt% to prevent ear rolling of hot rolling, and P is strength as a high strength steel plate. 0.035 wt% is necessary to obtain
It is necessary to regulate it to 0.035 wt%.

【0018】Sは、0.030wt%超になると熱延の
耳あれ性が劣化するようになるので0.030wt%に
規制する必要がある。尚、下限値は、いくら少なくても
障害にならないので特に規制する必要がない。sol.
Alは、NをAlNとして固定しストレッチャストレイ
ンの発生を防止する必要があるので、0.025wt%
以上は必要である。又、0.100wt%超になると鋳
造時に溶鋼の空気酸化が起こり易くなり介在物量が増
え、加工性や、めっき品質をも劣化させるようになるの
で0.100wt%を上限値とした。Nは、Alによっ
てAlNとして固定され無害化が成されるが、0.01
00wt%超になるとAlNが多くなりすぎr値が劣化
するようになるので、上限値を0.0100wt%とし
た。尚、通常の製鋼向上では0.0005wt%未満に
することは困難であるので下限値を0.0005wt%
とした。
If the content of S exceeds 0.030 wt%, the ear roll property of hot rolling deteriorates, so it is necessary to regulate S to 0.030 wt%. It should be noted that there is no need to restrict the lower limit value because it does not become an obstacle no matter how small. sol.
For Al, it is necessary to fix N as AlN to prevent the occurrence of stretcher strain, so 0.025 wt%
The above is necessary. On the other hand, if it exceeds 0.100 wt%, air oxidation of the molten steel is likely to occur during casting, the amount of inclusions increases, and the workability and plating quality also deteriorate, so 0.100 wt% was made the upper limit value. N is detoxified by being fixed as AlN by Al, but 0.01
If it exceeds 00 wt%, the amount of AlN becomes too large and the r value deteriorates, so the upper limit value was made 0.0100 wt%. Since it is difficult to reduce the amount to less than 0.0005 wt% by improving ordinary steelmaking, the lower limit is set to 0.0005 wt%.
And

【0019】Nb含有量は、0.007wt%未満であ
ったり、0.020wt%超である場合は、優れたr値
が得られないので、0.007wt%〜0.0200w
t%に規制する必要がある。Nbが0.007wt%未
満の場合は、熱延板の結晶粒径を細粒化することが不十
分となるとともにCをNbCとして十分に固定できなく
なり、その結果として焼鈍板のr値が十分高くならなく
なる。また、0.020wt%超になると、固溶Nb量
が多くなり焼鈍時の結晶粒の成長が抑制されr値が十分
に高くならなくなる。また、Nb量は、非ストレッチャ
ストレイン性を確保するには、Nb(wt%):7.7
5×wt%C−0.013以上添加する必要がある。更
に、BH量を安定して1kgf/mm2 以上確保するに
は、Nb(wt%):7.75×wt%C+0.007
以下とする必要がある。
If the Nb content is less than 0.007 wt% or more than 0.020 wt%, an excellent r value cannot be obtained, so 0.007 wt% to 0.0200 w
It is necessary to regulate t%. When Nb is less than 0.007 wt%, it becomes insufficient to reduce the crystal grain size of the hot rolled sheet and C cannot be sufficiently fixed as NbC, resulting in a sufficient r value of the annealed sheet. It won't get higher. On the other hand, if it exceeds 0.020 wt%, the amount of solute Nb increases, the growth of crystal grains during annealing is suppressed, and the r value cannot be sufficiently high. Further, the amount of Nb is Nb (wt%): 7.7 in order to secure non-stretchable strain.
It is necessary to add 5 × wt% C-0.013 or more. Further, in order to stably secure the BH amount of 1 kgf / mm 2 or more, Nb (wt%): 7.75 × wt% C + 0.007
It is necessary to:

【0020】B含有量は、特に耐二次加工性が要求され
ない用途に用いる場合は添加する必要はないが、耐二次
加工性が要求される用途に用いる場合は、B(wt
%):0.004×wt%P以上、0.0010wt%
以下で且つ、B/N≦0.7(wt%比)の範囲で添加
すればよい。BはTi添加極低炭素鋼に微量添加するこ
とによって二次加工性が改善できることがよく知られて
いるが同時にr値も低下することもよく知られている。
本発明者等は、二次加工性と深絞り性とを両立させる方
法について種々検討し本発明の請求項(2)の製造方法
を見出した。B含有量が、0.0010wt%超或いは
B/Nが0.7(wt%比)超となるとBNが生成する
ようになり、その結果としてr値が低下するようになる
が、B含有量が本発明の範囲での添加ではr値の劣化は
殆ど生じないのである。一方、二次加工性は、B(wt
%):0.004×wt%P以上の添加で顕著に向上す
る。
The B content does not need to be added particularly when it is used in applications where secondary workability is not required, but when it is used in applications where secondary workability is required, it is B (wt).
%): 0.004 x wt% P or more, 0.0010 wt%
It may be added below, within the range of B / N ≦ 0.7 (wt% ratio). It is well known that the secondary workability can be improved by adding a trace amount of B to the Ti-added ultra-low carbon steel, but it is also well known that the r value is lowered at the same time.
The present inventors have conducted various studies on a method for achieving both the secondary workability and the deep drawability, and have found the manufacturing method of claim (2) of the present invention. When the B content exceeds 0.0010 wt% or B / N exceeds 0.7 (wt% ratio), BN starts to be generated, and as a result, the r value decreases, but the B content However, the addition within the range of the present invention causes almost no deterioration of the r value. On the other hand, the secondary workability is B (wt
%): Addition of 0.004 × wt% P or more significantly improves.

【0021】以下、鋼板の成分構成条件以外の製造条件
について詳細に述べる。鋳片の製造条件は、各請求項の
鋼の成分が得られる方法であればどのような方法でもよ
く、特に規制する必要はない。熱延条件は、特に規制す
る必要がなく、鋳片を、Ar3 以上で仕上げ圧延を行い
巻き取り熱延鋼帯とすればよい。尚、N含有量が多い場
合や加熱温度が高温の場合は680℃以上の巻き取り温
度を採用することでより良好なr値が得られ、必要に応
じて採用すればよい。冷間圧延は、特に規制する必要が
なく通常の方法でよい。連続焼鈍方法は、750〜89
0℃に加熱し再結晶焼鈍を行い、その後、冷却を行うに
当たり、少なくとも730℃までの間を、2℃/s以上
10℃/s未満の冷却速度で冷却し、焼鈍板を造る必要
がある。焼鈍温度が750℃未満では十分なr値が得ら
れず、890℃超では良好な形状の鋼板が得られない。
The production conditions other than the compositional conditions of the steel sheet will be described in detail below. The production conditions of the cast slab may be any method as long as the components of the steel of each claim are obtained, and it is not particularly limited. The hot rolling conditions do not have to be particularly limited, and the slab may be finished rolled with Ar 3 or more to obtain a rolled hot rolled steel strip. When the N content is high or the heating temperature is high, a better r value can be obtained by adopting a coiling temperature of 680 ° C. or higher, and it may be adopted if necessary. Cold rolling does not need to be particularly restricted and may be a usual method. The continuous annealing method is 750-89.
When heating to 0 ° C. to perform recrystallization annealing, and then cooling, it is necessary to cool at least 730 ° C. at a cooling rate of 2 ° C./s or more and less than 10 ° C./s to produce an annealed plate. . If the annealing temperature is lower than 750 ° C, a sufficient r value cannot be obtained, and if it exceeds 890 ° C, a steel sheet having a good shape cannot be obtained.

【0022】焼鈍後の冷却速度は、BH量とストレッチ
ャストレインの発生に大きく影響し、図1に示すよう
に、2℃/s以上10℃/s未満の冷却速度で冷却しな
ければならない。また、この効果は、少なくとも730
℃までを2℃/s以上10℃/s未満の冷却速度で冷却
することで得られる。尚、過時効処理については特に規
制する必要はない。調質圧延は、0.5%未満では如何
に耐ストレッチャストレインに優れた焼鈍板を製造した
としてもプレス時のストレッチャストレインの発生を防
止することが出来ないので0.5%以上を施さねばなら
ない。尚、3%超では延性の劣化が大きいので3%未満
に規制する必要がある。
The cooling rate after annealing has a great influence on the amount of BH and the generation of stretcher strain, and as shown in FIG. 1, the cooling rate must be 2 ° C./s or more and less than 10 ° C./s. Also, this effect is at least 730
It can be obtained by cooling up to ° C at a cooling rate of 2 ° C / s or more and less than 10 ° C / s. Note that there is no particular need to regulate overaging treatment. If the temper rolling is less than 0.5%, no matter how excellent annealed sheet having excellent stretcher strain resistance can be produced, it is not possible to prevent the occurrence of stretcher strain during pressing, so 0.5% or more must be applied. . If it exceeds 3%, the ductility deteriorates greatly, so it is necessary to regulate it to less than 3%.

【0023】[0023]

【実施例】以下に本発明の効果を実施例により説明す
る。表1に示す成分の鋳片を造り、表2に示す連続熱延
条件で3.8mmの熱延板を製造し、酸洗後0.65m
mに冷間圧延を行い、連続焼鈍で850℃×60sec
の再結晶焼鈍を行い均熱後の冷却速度を表2に示す条件
で冷却した後400℃の過時効処理帯を通過させた後室
温まで冷却して焼鈍板を製造し、その後1.0%の調質
圧延を施して35〜38kgf/mm2 級の高強度冷延
鋼板を製造した。製造した高強度冷延鋼板の材質を調査
し、表2に示す。Y.P,T.S,El、r値は調質圧
延後の特性値、YP−Elは100℃×4Hrの時効処
理を施した後の値、BH量の測定条件は予歪量は2%,
塗装焼き付け相当熱処理条件を170℃×20minと
した時の値である。また、二次加工性は絞り比2.52
でカップを絞り−40℃でカップを押しつぶした時の脆
性破断の長さで評価し全く割れなかったものを◎5mm
以下のものを〇それ以上を×として評価した。
EXAMPLES The effects of the present invention will be described below with reference to examples. A slab of the components shown in Table 1 is made, a 3.8 mm hot rolled sheet is manufactured under the continuous hot rolling conditions shown in Table 2, and 0.65 m after pickling
m by cold rolling and continuous annealing at 850 ° C x 60 sec
Recrystallization annealing was performed and the cooling rate after soaking was cooled under the conditions shown in Table 2, then passed through an overaging zone of 400 ° C., and then cooled to room temperature to produce an annealed plate, and then 1.0% Was subjected to temper rolling to produce a high strength cold rolled steel sheet of 35 to 38 kgf / mm 2 grade. The materials of the manufactured high-strength cold-rolled steel sheet were investigated and shown in Table 2. Y. P, T. S, El, r values are characteristic values after temper rolling, YP-El is a value after aging treatment at 100 ° C. × 4 Hr, BH amount is measured under a prestrain amount of 2%,
It is a value when the heat treatment condition equivalent to coating baking is 170 ° C. × 20 min. In addition, the secondary workability is a drawing ratio of 2.52.
When the cup was squeezed with -40 ° C. and crushed at -40 ° C., the length of brittle fracture was evaluated.
The following items were evaluated as ◯ and more as ×.

【0024】[0024]

【表1】 [Table 1]

【0025】[0025]

【表2】 [Table 2]

【0026】鋼A,B,C,Dは、何れも本発明の成分
範囲内の鋼で、鋼AはBを添加しない請求項1の成分の
鋼、鋼B,C,Dは、本発明の請求項2のB添加量のそ
れぞれの下限値の3.3,3.1,4.4ppm以上の
6,6,9ppm添加した鋼、その内D鋼はPを0.1
10wt%添加し38kgf/mm2 級の高強度冷延鋼
板を製造する成分の鋼である。鋼Eは、C含有量を0.
0040wt%,Nb含有量を0.040wt%と本発
明の範囲より高い例で、従来法の特公昭60−1700
4号公報に準ずる鋼成分の例である。鋼Fは、Nb含有
量が0.003wt%と本発明鋼の範囲を下回った比較
例である。鋼Gは、C含有量を0.0040wt%,B
含有量を0.0045wt%とBを本発明の範囲より多
量に添加した例で、従来法の特開昭58−84928号
公報に準ずる鋼成分の例である。鋼Hは、C含有量が
0.0011wt%,Nb含有量が0.019wt%と
請求項の(1)式のNb含有量の上限値(7.75×w
t%C(0.0011)=0.0155%)を外れた鋼
成分の例である。鋼Iは、B含有量を0.0038wt
%とBを本発明の範囲より多量に添加した鋼成分の例で
ある。
All of the steels A, B, C and D are steels within the composition range of the present invention, and the steels A, B, C and D having the composition of claim 1 in which B is not added are steels of the present invention. 6. The steel containing 6,6,9 ppm of the lower limit of 3.3, 3.1, 4.4 ppm or more of the B addition amount of claim 2, wherein the D steel has a P of 0.1.
It is a component steel that is added with 10 wt% to produce a high strength cold rolled steel sheet of 38 kgf / mm 2 grade. Steel E has a C content of 0.
In an example in which the content of 0040 wt% and the content of Nb are 0.040 wt%, which is higher than the range of the present invention, the conventional method of Japanese Patent Publication No. 60-1700
It is an example of the steel composition according to the gazette of No. 4. Steel F is a comparative example in which the Nb content is 0.003 wt%, which is below the range of the steel of the present invention. Steel G has a C content of 0.0040 wt%, B
This is an example in which the content is 0.0045 wt% and B is added in a larger amount than the range of the present invention, and it is an example of a steel component according to the conventional method of JP-A-58-84928. Steel H has a C content of 0.0011 wt% and an Nb content of 0.019 wt%, and the upper limit value (7.75 × w) of the Nb content in the formula (1) of the claim.
It is an example of a steel composition that deviates from t% C (0.0011) = 0.0155%). Steel I has a B content of 0.0038 wt.
% Is an example of a steel component added with B in a larger amount than the range of the present invention.

【0027】試料1,2,3,5は、何れも本発明の実
施例で、試料4は連続焼鈍時の均熱後の冷却速度が1℃
/sと本発明の範囲を下回る比較例、試料7は成分が本
発明外の比較例、試料6,8の焼鈍条件は本発明の条件
であるが鋼成分が従来法の成分である比較例である。試
料1,2,3,5は、何れも時効後のYP−El,BH
量,r値の全てが優れた値になっており、本発明の方法
によって、耐デント性に優れたストレッチャストレイン
の発生しない深絞り用高強度冷延鋼板が製造できること
がわかる。また、得られた焼鈍板は何れも良好な形状が
得られており、本発明の冷却速度を10℃/s未満とす
る製造方法は良好な形状の鋼板を安定して得られると言
う点においても優れていることがわかる。
Samples 1, 2, 3, and 5 are all examples of the present invention, and Sample 4 has a cooling rate of 1 ° C. after soaking during continuous annealing.
/ S and a comparative example below the range of the present invention, sample 7 is a comparative example in which the components are outside the present invention, and the annealing conditions of samples 6 and 8 are those of the present invention, but the steel components are comparative examples Is. Samples 1, 2, 3 and 5 are all YP-El and BH after aging.
Since both the amount and the r value are excellent values, it can be seen that the method of the present invention can produce a high strength cold rolled steel sheet for deep drawing which is excellent in dent resistance and in which stretcher strain does not occur. Further, all of the obtained annealed plates have a good shape, and the manufacturing method of the present invention in which the cooling rate is less than 10 ° C./s is that a steel sheet having a good shape can be stably obtained. Also proves to be excellent.

【0028】また、請求項2の実施例である試料2,
3,5は耐二次加工性をも優れており、本発明のB(w
t%)を0.004×wt%P以上、0.0010wt
%以下で、且つ、B/N≦0.7(wt%比)の範囲と
することで優れた二次加工性をも付与することができる
ことがわかる。一方、比較例の鋼4は、連続焼鈍の冷却
条件が1℃/sと本発明の範囲を下回った条件のもの
で、BH量が0.5kgf/mm2 と低い値しか得られ
ておらず、本発明の実施例である試料3と比較すると、
連続焼鈍の冷却条件を2〜10℃/sとする本発明の製
造方法が優れているかがよくわかる。また、鋼6,7,
8,9,10は何れも比較例で、鋼6はC量が0.00
40wt%,及びNb量が0.040wt%と、鋼7は
Nb量が0.003wt%と、鋼8はB量が0.004
5wt%と、鋼9はNb量が請求項に記載の式の上限値
を超えて0.019wt%と、鋼10はB量が0.00
38wt%と、本発明の鋼成分範囲を外れた比較例で、
鋼6はBH量とr値が、鋼7,8,10はr値が、鋼9
はBH量が、劣悪な特性値となっている。
Further, the sample 2, which is the embodiment of claim 2,
Nos. 3 and 5 are also excellent in secondary workability, and B (w of the present invention
t%) is 0.004 x wt% P or more, 0.0010 wt
It can be seen that excellent secondary workability can also be imparted by setting the ratio to be B / N ≦ 0.7 (wt% ratio) in the range of 0.1% or less. On the other hand, the steel 4 of the comparative example has a cooling condition of continuous annealing of 1 ° C./s, which is below the range of the present invention, and the BH amount is as low as 0.5 kgf / mm 2. In comparison with Sample 3, which is an example of the present invention,
It can be clearly seen whether the manufacturing method of the present invention in which the cooling condition for continuous annealing is 2 to 10 ° C./s is excellent. In addition, steel 6,7,
8, 9 and 10 are all comparative examples, and steel 6 has a C content of 0.00
40 wt% and Nb content of 0.040 wt%, Steel 7 has Nb content of 0.003 wt%, and Steel 8 has B content of 0.004 wt%.
5 wt%, Steel 9 has an Nb amount of 0.019 wt% exceeding the upper limit of the formula described in the claims, and Steel 10 has a B amount of 0.00.
38 wt% and a comparative example out of the steel composition range of the present invention,
Steel 6 has BH content and r value, Steels 7, 8 and 10 have r value, Steel 9
Has an inferior characteristic value in the amount of BH.

【0029】以上の実施例の結果から明らかなように、
本発明の請求項1の製造方法によって、耐デント性に優
れたストレッチャストレインの発生しない深絞り用高強
度冷延鋼板が、請求項2の方法によって、耐二次加工性
に優れた特性をも付与することが出来、工業的価値が極
めて高いことがわかる。尚、本発明の製造方法は、電気
亜鉛メッキ等の各種の表面処理鋼板の原板の製造方法と
しても、また、溶融亜鉛メッキ鋼板の製造に於いても同
じ効果が得られる。
As is clear from the results of the above examples,
The high-strength cold-rolled steel sheet for deep drawing, which is excellent in dent resistance and does not generate stretcher strain, has the excellent secondary workability according to the method of claim 2 of the present invention. It can be given that the industrial value is extremely high. The production method of the present invention has the same effect as a production method of a raw plate of various surface-treated steel sheets such as electrogalvanized sheets and also in the production of hot-dip galvanized steel sheets.

【0030】[0030]

【発明の効果】以上、本発明について詳細に説明した
が、本発明の製造方法によって、耐デント性に優れたス
トレッチャストレインの発生しない深絞り用高強度冷延
鋼板を製造することができる優れた効果が発揮出来、そ
の工業的価値は大である。
As described above, the present invention has been described in detail. However, according to the manufacturing method of the present invention, it is possible to manufacture a high strength cold rolled steel sheet for deep drawing which is excellent in dent resistance and does not cause stretcher strain. It can be effective and its industrial value is great.

【図面の簡単な説明】[Brief description of drawings]

【図1】連続焼鈍の冷却速度と時効後のYP−El、B
H量との関係を示す図である。
FIG. 1 Cooling rate of continuous annealing and YP-El, B after aging
It is a figure which shows the relationship with H amount.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 芳賀 裕和 兵庫県姫路市広畑区富士町1番地 新日本 製鐵株式会社広畑製鐵所内 ─────────────────────────────────────────────────── ─── Continuation of front page (72) Inventor Hirokazu Haga 1 Fuji-machi, Hirohata-ku, Himeji-shi, Hyogo Shin Nippon Steel Corp. Hirohata Works

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 C:0.0010〜0.0030wt
%,Si≦0.50wt%,Mn:0.02〜0.80
wt%,P:0.035〜0.150wt%,S≦0.
030wt%,sol.Al:0.025〜0.100
wt%,N:0.0005〜0.0100wt%,N
b:0.007〜0.020wt%で、且つ、C量とN
b量の関係が下記式の範囲を満たし残部不可避的不純物
及び鉄よりなる鋳片を、Ar3 以上で仕上げ圧延を行い
巻き取り熱延鋼帯とし、冷間圧延を行い、連続焼鈍法で
750〜890℃に加熱し再結晶焼鈍を行い、その後、
冷却を行うに当たり、少なくとも730℃までの間を、
2℃/s以上10℃/s未満の冷却速度で冷却し、焼鈍
板を造り、その後、0.5〜3%の調質圧延を行うこと
を特徴とする耐デント性に優れたストレッチャストレイ
ンの発生しない深絞り用高強度冷延鋼板の製造方法。 Nb:7.75 ×wt% C−0.013 ≦Nb(wt%)≦7.75 ×
wt% C+0.007
1. C: 0.0010 to 0.0030 wt
%, Si ≦ 0.50 wt%, Mn: 0.02-0.80
wt%, P: 0.035 to 0.150 wt%, S ≦ 0.
030 wt%, sol. Al: 0.025 to 0.100
wt%, N: 0.0005 to 0.0100 wt%, N
b: 0.007 to 0.020 wt%, and C amount and N
A slab consisting of the balance unavoidable impurities and iron satisfying the range of the following formula is subjected to finish rolling with Ar 3 or more to make a hot rolled steel strip, cold rolling, and continuous annealing at 750 ~ 890 ℃ to heat recrystallization annealing, then,
For cooling, at least up to 730 ℃,
A stretcher strain with excellent dent resistance, which is characterized by cooling at a cooling rate of 2 ° C./s or more and less than 10 ° C./s to produce an annealed plate, and then temper rolling 0.5 to 3%. A method for producing a high-strength cold-rolled steel sheet for deep drawing that does not occur. Nb: 7.75 x wt% C-0.013 ≤ Nb (wt%) ≤ 7.75 x
wt% C + 0.007
【請求項2】 請求項1記載の方法に於いて、鋼の組成
を、更に、B(wt%)を0.004×wt%P以上、
0.0010wt%以下で、且つ、B/N≦0.7(w
t%比)の範囲とすることを特徴とする優れた二次加工
性をも付与する製造方法。
2. The method according to claim 1, wherein the composition of the steel further comprises B (wt%) of 0.004 × wt% P or more,
0.0010 wt% or less, and B / N ≦ 0.7 (w
(t% ratio). A manufacturing method that also imparts excellent secondary workability.
JP06243989A 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain Expired - Fee Related JP3110624B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP06243989A JP3110624B2 (en) 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP06243989A JP3110624B2 (en) 1994-10-07 1994-10-07 Method for producing high strength cold rolled steel sheet for deep drawing with excellent dent resistance and no stretcher strain

Publications (2)

Publication Number Publication Date
JPH08104926A true JPH08104926A (en) 1996-04-23
JP3110624B2 JP3110624B2 (en) 2000-11-20

Family

ID=17112062

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

Country Link
JP (1) JP3110624B2 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012036412A (en) * 2010-08-03 2012-02-23 Nippon Steel Corp Method for continuous-annealing steel sheet using continuous-annealing furnace
CN110408834A (en) * 2019-07-23 2019-11-05 舞阳钢铁有限责任公司 It improves steel ingot low Si of becoming a useful person and faces the method for hydrogen Cr-Mo steel flaw detection qualification rate
WO2020003986A1 (en) * 2018-06-27 2020-01-02 Jfeスチール株式会社 Methods for producing cold-rolled steel sheet, hot-dip galvanized steel sheet, and alloyed hot-dip galvanized steel sheet

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012036412A (en) * 2010-08-03 2012-02-23 Nippon Steel Corp Method for continuous-annealing steel sheet using continuous-annealing furnace
WO2020003986A1 (en) * 2018-06-27 2020-01-02 Jfeスチール株式会社 Methods for producing cold-rolled steel sheet, hot-dip galvanized steel sheet, and alloyed hot-dip galvanized steel sheet
JPWO2020003986A1 (en) * 2018-06-27 2020-07-02 Jfeスチール株式会社 Cold rolled steel sheet, hot dip galvanized steel sheet, and method for manufacturing alloyed hot dip galvanized steel sheet
CN110408834A (en) * 2019-07-23 2019-11-05 舞阳钢铁有限责任公司 It improves steel ingot low Si of becoming a useful person and faces the method for hydrogen Cr-Mo steel flaw detection qualification rate

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