JP2706310B2 - Aluminum alloy plate for automobile panel and method of manufacturing the same - Google Patents

Aluminum alloy plate for automobile panel and method of manufacturing the same

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Publication number
JP2706310B2
JP2706310B2 JP1104865A JP10486589A JP2706310B2 JP 2706310 B2 JP2706310 B2 JP 2706310B2 JP 1104865 A JP1104865 A JP 1104865A JP 10486589 A JP10486589 A JP 10486589A JP 2706310 B2 JP2706310 B2 JP 2706310B2
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JP
Japan
Prior art keywords
less
aluminum alloy
maximum value
alloy plate
anisotropy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP1104865A
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Japanese (ja)
Other versions
JPH02285045A (en
Inventor
幹 神林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
THE FURUKAW ELECTRIC CO., LTD.
Original Assignee
THE FURUKAW ELECTRIC CO., LTD.
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Priority to JP1104865A priority Critical patent/JP2706310B2/en
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  • Heat Treatment Of Steel (AREA)
  • Metal Rolling (AREA)

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は自動車のパネル用として使用する成形性にす
ぐれた自動車パネル用アルミニウム合金板とその製造方
法に関するものである。
Description: BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an aluminum alloy sheet for an automobile panel having excellent formability and used for an automobile panel, and a method for producing the same.

〔従来の技術と発明が解決しようとする課題〕[Problems to be solved by conventional technology and invention]

一般に自動車のパネルには鋼板が多く使用されている
が、近年燃料削減の観点から軽量化を図る目的でアルミ
ニウム合金が一部で使用されるようになった。
Generally, steel plates are often used for automobile panels, but in recent years, aluminum alloys have been partially used for the purpose of weight reduction from the viewpoint of fuel saving.

従来使用されているアルミニウム合金は成形性の向上
と、強度の向上を目的に組成を調整し、仕上げ焼鈍は箱
型の置換ガス雰囲気炉で徐々に昇温し、一定時間炉内に
保持する方式で造られている。
Conventionally used aluminum alloys are adjusted in composition for the purpose of improving formability and strength, and finish annealing is performed by gradually raising the temperature in a box-type replacement gas atmosphere furnace and holding it in the furnace for a certain time. It is made of.

しかしながら材料の強度及び伸び率に代表される延性
の方向性、即ち圧延方向とそれと直角方向あるいは45゜
の方向の強度及び伸び率に異方性を生じ、プレス成形す
る場合にしわや偏肉を発生し、あるいはスプリングパッ
クによる形状不良を起すため、その改善が望まれてい
る。
However, ductility represented by the strength and elongation of the material, that is, anisotropy occurs in the strength and elongation in the rolling direction and the direction perpendicular to it or in the direction of 45 °. Therefore, there is a need for an improvement in the shape of the spring due to the occurrence of the shape failure or the shape failure due to the spring pack.

〔課題を解決するための手段〕[Means for solving the problem]

本発明はこれに鑑み種々検討の結果、強度及び伸びの
異方性は従来の焼鈍方法では解消できないが、高温短時
間の処理により、圧延時に形成された集合組織が消出
し、異方性が緩和され、また熱処理時の昇温速度を大き
くすることにより、再結晶粒の粗大化が抑制され、また
素板の表面のミクロ的な形状も成形時の潤滑油保持に影
響し、いわゆる平均表面粗さRaに適正値が存在すること
を知見し、更に検討の結果、成形性のすぐれた自動車パ
ネル用アルミニウム合金板とその製造方法を開発したも
のである。
In view of this, as a result of various studies in view of this, although the anisotropy of strength and elongation cannot be eliminated by the conventional annealing method, the texture formed during rolling disappears due to the treatment at high temperature for a short time, and the anisotropy is reduced. By relaxing and increasing the rate of temperature rise during heat treatment, coarsening of recrystallized grains is suppressed, and the microscopic shape of the surface of the base plate also affects lubricating oil retention during molding, so-called average surface The inventors have found that there is an appropriate value for the roughness Ra, and as a result of further studies, have developed an aluminum alloy sheet for an automobile panel having excellent formability and a method for producing the same.

即ち本発明合金板の一つは、Mg2〜6wt%(以下wt%を
%と略機)、Mn0.05〜0.5%、Zn0.001〜0.3%を含み、
不純物中のFe含有量を0.2%以下に規制し、残部Alと不
可避的不純物からなるアルミニウム合金板であって、該
アルミニウム合金板の強度及び伸び率の圧延方向による
異方性のそれぞれ最大値と最小値の差が最大値の15%以
内で、平均表面粗さRaが0.1〜2.0μmであることを特徴
とするものである。
That is, one of the alloy sheets of the present invention contains Mg2 to 6 wt% (hereinafter, wt% is abbreviated as%), Mn0.05 to 0.5%, Zn0.001 to 0.3%,
An aluminum alloy plate comprising Fe and 0.2% or less in the impurities, the balance being Al and unavoidable impurities, and the maximum value of the anisotropy of the strength and elongation of the aluminum alloy plate depending on the rolling direction. The difference between the minimum values is within 15% of the maximum value, and the average surface roughness Ra is 0.1 to 2.0 μm.

また本発明合金板の他の一つは、Mg2〜6%、Mn0.05
〜0.5%、Zn0.001〜0.3%を含み、更にCu0.5%以下、Cr
0.3wt%以下、Ti0.3wt%以下、Zr0.3wt%以下、V0.3wt
%以下、B0.001wt%以下、Ni0.5wt%以下の範囲内で何
れか1種以上を含み、不純物のFe含有量を0.2%以下に
規制し、残部Alと不可避的不純物中からなるアルミニウ
ム合金板であって、該アルミニウム合金板の強度及び伸
び率の圧延方向による異方性のそれぞれ最大値と最小値
の差が最大値の15%以内で、平均表面粗さRaが0.1〜2.0
μmであることを特徴とするものである。
Another one of the alloy sheets of the present invention is Mg2-6%, Mn0.05.
0.5%, Zn 0.001-0.3%, Cu 0.5% or less, Cr
0.3wt% or less, Ti0.3wt% or less, Zr0.3wt% or less, V0.3wt
% Or less, B 0.001 wt% or less, Ni0.5 wt% or less, containing at least one type, restricting the Fe content of impurities to 0.2% or less, aluminum alloy consisting of the balance of Al and unavoidable impurities A difference between the maximum value and the minimum value of the anisotropy in the rolling direction of the strength and elongation percentage of the aluminum alloy plate is within 15% of the maximum value, and the average surface roughness Ra is 0.1 to 2.0.
μm.

更に本発明製造方法は、Mg2〜6%、Mn0.05〜0.5%、
Zn0.001〜0.3%を含み、又はこれにCu0.5%以下、Cr0.3
%以下、Ti0.3%以下、Zr0.3%以下、V0.3%以下、B0.0
01%以下、Ni0.5%以下の範囲内で何れか1種類以上を
含み、不純物中のFe含有量を0.2%以下に規制し、残部A
lと不可避的不純物からなる合金に、ソーキングと熱間
圧延を施した後、中間焼鈍と冷間圧延を行なうか、行な
うことなく、100℃/分以上の速度で昇温して400〜600
℃の温度で加熱処理することを特徴とするものである。
Further, the production method of the present invention, Mg2-6%, Mn0.05-0.5%,
Contains 0.001-0.3% of Zn, or Cu0.5% or less, Cr0.3
% Or less, Ti 0.3% or less, Zr 0.3% or less, V0.3% or less, B0.0
At least one type within the range of 01% or less and Ni 0.5% or less, the Fe content in impurities is regulated to 0.2% or less, and the balance A
After subjecting the alloy consisting of l and unavoidable impurities to soaking and hot rolling, intermediate annealing and cold rolling are performed, or the temperature is increased at a rate of 100 ° C / min or more without performing 400 to 600
The heat treatment is performed at a temperature of ° C.

〔作 用〕(Operation)

本発明合金板は上記組織からなり、Mgの添加は強度を
確保するためで、その含有量を2〜6%と限定したの
は、2%未満では効果がなく、6%を越えると耐応力腐
触割れ性を低下させるためである。Mnの添加はMgと同様
強度を確保すると共に、耐応力腐触割れ性を改善するた
めで、その含有量を0.05〜0.5%と限定したのは0.05%
未満では効果がなく、0.5%を越えるとAl−Mn−Fe系の
金属間化合物を形成して延性を低下させるためである。
Znの添加は延性を向上させるためで、その含有量を0.00
1〜0.3%と限定したのは、0.001%未満では効果がな
く、0.3%を越えると主要元素であるMgと結合して金属
間化合物を形成し、強度を低下させるためである。また
Cu≦0.5%、Cr≦0.3%、Ti≦0.3%、Zr≦0.3%、V≦0.
3%、B≦0.001%、Ni≦0.5%及びFe≦0.2%と規制した
のは、いずれも上限値を越えて含有されると延性を低下
させるからである。
The alloy sheet of the present invention has the above-mentioned structure, and the addition of Mg is for securing the strength. The content is limited to 2 to 6%. This is for reducing the corrosion cracking resistance. The addition of Mn is to ensure the same strength as Mg and to improve the stress corrosion cracking resistance. The content was limited to 0.05 to 0.5% by 0.05%.
If it is less than 0.5%, there is no effect, and if it exceeds 0.5%, an Al-Mn-Fe-based intermetallic compound is formed and ductility is reduced.
The addition of Zn is for improving ductility, and its content is 0.00
The reason for limiting the content to 1 to 0.3% is that if it is less than 0.001%, there is no effect, and if it exceeds 0.3%, it binds to Mg as a main element to form an intermetallic compound and lowers the strength. Also
Cu ≦ 0.5%, Cr ≦ 0.3%, Ti ≦ 0.3%, Zr ≦ 0.3%, V ≦ 0.
The reason for restricting the content to 3%, B ≦ 0.001%, Ni ≦ 0.5%, and Fe ≦ 0.2% is that if any of them exceeds the upper limit, the ductility is reduced.

本発明合金板は上記組成からなり、特に圧延方向の異
方性における強度の最大値と最小値の差が最大値の15%
以内と限定したのは、最大値と最小値の差が最大値の15
%を上回ると成形時に強度の高い方向に影響されてスプ
リングバックが生じ易くなるためである。また圧延方向
の異方性における伸び率の最大値と最小値の差が、最大
値の15%以内と限定したのは、最大値と最小値の差が最
大値の15%を上回ると、成形時にしわや偏肉の発生をと
もなうためである。更に平均表面粗さRaを0.1〜2.0μm
未満では潤滑油の保持効果が十分でなく、成形時の割
れ、焼付等の問題が発生し易く、2.0μmを越えると表
面の微視的凹部が切欠作用し、成形時に割れをともな
う。平均表面粗さRaのコントロールはロールの研磨方法
によるが、研磨としては砥石によってもよいし、レーザ
照射によりロール表面を局部的に溶融して円錐、円筒又
は角筒状の凹みを付ける方法でもよいし、更には化学的
研磨処理などでもよい。また素板表面を化学的にエッチ
ング処理しても差し支えない。
The alloy sheet of the present invention has the above composition, and particularly, the difference between the maximum value and the minimum value in the anisotropy in the rolling direction is 15% of the maximum value.
The difference between the maximum value and the minimum value is 15
%, Springback is likely to occur due to the direction of higher strength during molding. The difference between the maximum value and the minimum value of the elongation percentage in the anisotropy in the rolling direction is limited to within 15% of the maximum value, because the difference between the maximum value and the minimum value exceeds 15% of the maximum value. This is because wrinkles and uneven thickness sometimes occur. Further, the average surface roughness Ra is 0.1 to 2.0 μm
If it is less than 0.5 mm, the effect of retaining the lubricating oil is not sufficient, and problems such as cracking and seizure are likely to occur during molding. If it exceeds 2.0 μm, microscopic recesses on the surface are notched, causing cracking during molding. The control of the average surface roughness Ra depends on the method of polishing the roll, but the polishing may be performed by a grindstone, or a method of locally melting the roll surface by laser irradiation to form a conical, cylindrical or rectangular cylindrical dent. Alternatively, a chemical polishing treatment or the like may be used. Also, the surface of the base plate may be chemically etched.

次に本発明製造方法において、ソーキングと熱間圧延
を施した後、中間焼鈍と冷間圧延を行ない又は行なうこ
となく、100℃/分以上の速度で昇温して400〜600℃の
温度に加熱処理するのは、成形性を向上するためであ
り、昇温速度が100℃/分未満では昇温時に結晶粒の粗
大化をともなうことがあり、成形時の肌荒れ、割れ等の
不都合を生じ易いためである。また加熱温度が400℃未
満では溶体化処理効果が不充分で強度を確保することが
できず、加熱温度が600℃を越えると結晶粒粗大化やバ
ーニング現象を生じる恐れがあるばかりか、成形性の低
下につながる。保持時間は特に規定しないが、10分以内
とすることが望ましい。
Next, in the production method of the present invention, after performing soaking and hot rolling, without performing or performing intermediate annealing and cold rolling, the temperature is raised at a rate of 100 ° C / min or more to a temperature of 400 to 600 ° C. The heat treatment is performed to improve the formability. If the temperature rise rate is less than 100 ° C./min, the crystal grains may be coarsened at the time of temperature rise, causing inconvenience such as rough surface and cracks at the time of molding. This is because it is easy. If the heating temperature is lower than 400 ° C, the solution treatment effect is insufficient and the strength cannot be secured.If the heating temperature is higher than 600 ° C, not only the crystal grain coarsening and burning phenomenon may occur but also the moldability Leads to a decrease in The holding time is not particularly specified, but is preferably set within 10 minutes.

〔実施例〕〔Example〕

第1表に示す組成の厚さ500mmの鋳塊を520℃で4時間
ソーキングした後、熱間圧延を行なって厚さ5mmの板と
した。これを冷間圧延により厚さ1.0mmの板に仕上げ
た。この板について第2表に示す条件で加熱処理を施し
た後、耐力及び伸びの異方性と張り出し性を調べた。そ
の結果を第2表に併記した。
A 500 mm thick ingot having the composition shown in Table 1 was soaked at 520 ° C for 4 hours, and then hot rolled to obtain a 5 mm thick plate. This was finished into a 1.0 mm thick plate by cold rolling. After subjecting this plate to a heat treatment under the conditions shown in Table 2, the proof stress, elongation anisotropy and overhang property were examined. The results are shown in Table 2.

耐力及び伸びの異方性は上記板より圧延方向に対して
0゜,45゜,90゜の方向にJIS5号試験片を採取し、これに
ついて引張試験を行なって最大値を示した方向の値に対
する最大値と最小値の差の比率で示した。また張り出し
性は、上記板より90mm角の板を切り出し、所定の潤滑油
をスプレー塗装して張り出し試験を行なった。
The anisotropy of proof stress and elongation is the value in the direction where the maximum value was obtained by taking a JIS No. 5 test piece from the above plate in the direction of 0 °, 45 °, 90 ° with respect to the rolling direction and conducting a tensile test on this. And the ratio of the difference between the maximum value and the minimum value. For the overhang property, a 90 mm square plate was cut out from the above plate, and a predetermined lubricating oil was spray-coated to perform an overhang test.

第1表及び第2表から明らかなように本発明合金(A
〜H)を本発明方法(No.1〜8)により製造したもの
は、本発明の合金組成外の合金(I〜L)を用いた比較
方法(No.9〜12)と比較し、何れも成形性評価指標値で
ある張り出し性において優れていることが判る。
As is clear from Tables 1 and 2, the alloy of the present invention (A
To H) produced by the method of the present invention (Nos. 1 to 8) were compared with comparative methods (Nos. 9 to 12) using alloys (I to L) other than the alloy composition of the present invention. It can also be seen that this is also excellent in the overhang property, which is the value of the formability evaluation index.

これに対し、本発明の組成内の合金(No.A)であって
も、加熱処理条件の異なる比較方法(No.13〜15)では
異方性が増大するばかりか、張り出し性も劣り、また本
発明の組成内の合金(No.A)であっても表面粗度が外れ
る比較方法(No.16)では張り出し性が劣ることが判
る。
On the other hand, even in the case of the alloy (No. A) within the composition of the present invention, not only the anisotropy is increased but also the overhang property is inferior in the comparative method (Nos. 13 to 15) under different heat treatment conditions, Also, it can be seen that even in the case of the alloy (No. A) within the composition of the present invention, the overhanging property is inferior in the comparative method (No. 16) in which the surface roughness deviates.

〔発明の効果〕〔The invention's effect〕

このように本発明によれば、成形性に優れた自動車パ
ネル用アルミニウム合金を提供し得るもので、自動車の
軽量化を可能にする等工業上顕著な効果を奏するもので
ある。
As described above, according to the present invention, it is possible to provide an aluminum alloy for an automobile panel having excellent moldability, and has an industrially remarkable effect such as enabling a reduction in the weight of an automobile.

───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.6 識別記号 庁内整理番号 FI 技術表示箇所 C22F 1/00 686 8719−4K C22F 1/00 686A 691 8719−4K 691A 8719−4K 691B ──────────────────────────────────────────────────の Continuation of the front page (51) Int.Cl. 6 Identification code Agency reference number FI Technical display location C22F 1/00 686 8719-4K C22F 1/00 686A 691 8719-4K 691A 8719-4K 691B

Claims (3)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】Mg2〜6wt%、Mn0.05〜0.5wt%、Zn0.001〜
0.3wt%を含み、不純物中のFe含有量を0.2wt%以下に規
制し、残部Alと不可避的不純物からなるアルミニウム合
金板であって、該アルミニウム合金板の強度及び伸び率
の圧延方向による異方性のそれぞれ最大値と最小値の差
が最大値の15%以内で、平均表面粗さRaが0.1〜2.0μm
であることを特徴とする自動車パネル用アルミニウム合
金板。
(1) Mg2-6 wt%, Mn0.05-0.5 wt%, Zn0.001-
An aluminum alloy sheet containing 0.3 wt% and the Fe content in impurities is controlled to 0.2 wt% or less, and the balance of Al and unavoidable impurities is different depending on the rolling direction of the strength and elongation of the aluminum alloy sheet. The difference between the maximum value and the minimum value of the anisotropy is within 15% of the maximum value, and the average surface roughness Ra is 0.1 to 2.0 μm
An aluminum alloy plate for an automobile panel, characterized in that:
【請求項2】Mg2〜6wt%、Mn0.05〜0.5wt%、Zn0.001〜
0.3wt%を含み、更にCu0.5wt%以下、Cr0.3wt%以下、T
i0.3wt%以下、Zr0.3wt%以下、V0.3wt%以下、B0.001w
t%以下、Ni0.5wt%以下、及びFe0.2wt%以下に規制
し、残部Alと不可避的不純物からなるアルミニウム合金
板であって、該アルミニウム合金板の強度及び伸び率の
圧延方向による異方性のそれぞれ最大値と最小値の差が
最大値の15%以内で、平均表面粗さRaが0.1〜2.0μmで
あることを特徴とする自動車パネル用アルミニウム合金
板。
2. Mg 2-6 wt%, Mn 0.05-0.5 wt%, Zn 0.001-
0.3wt%, Cu0.5wt% or less, Cr0.3wt% or less, T
i0.3wt% or less, Zr0.3wt% or less, V0.3wt% or less, B0.001w
t% or less, Ni0.5wt% or less, Fe0.2wt% or less, aluminum alloy plate consisting of the balance of Al and unavoidable impurities, the anisotropy of the strength and elongation of the aluminum alloy plate depending on the rolling direction An aluminum alloy plate for an automobile panel, wherein the difference between the maximum value and the minimum value of each property is within 15% of the maximum value, and the average surface roughness Ra is 0.1 to 2.0 μm.
【請求項3】Mg2〜6wt%、Mn0.05〜0.5wt%、Zn0.001〜
0.3wt%を含み、又は更にCu0.5wt%以下、Cr0.3wt%以
下、Ti0.3wt%以下、Zr0.3wt%以下、V0.3wt%以下、B
0.001wt%以下、Ni0.5wt%以下、及びFe0.2wt%以下に
規制し、残部Alと不可避的不純物からなる合金に、ソー
キングと熱間圧延を施した後、中間焼鈍と冷間圧延を行
なうか、行なうことなく、100℃/分以上の速度で昇温
して400〜600℃の温度で加熱処理した後、表面粗面化処
理を施すことを特徴とする自動車パネル用アルミニウム
合金板の製造方法。
3. Mg2-6 wt%, Mn0.05-0.5 wt%, Zn0.001-
0.3wt% or more, Cu0.5wt% or less, Cr0.3wt% or less, Ti0.3wt% or less, Zr0.3wt% or less, V0.3wt% or less, B
After restricting to 0.001wt% or less, Ni0.5wt% or less, and Fe0.2wt% or less, perform soaking and hot rolling on an alloy containing the balance of Al and unavoidable impurities, and then perform intermediate annealing and cold rolling. Manufacturing an aluminum alloy sheet for an automotive panel, wherein the temperature is raised at a rate of 100 ° C./min or more, heat-treated at a temperature of 400 to 600 ° C., and then the surface is roughened. Method.
JP1104865A 1989-04-25 1989-04-25 Aluminum alloy plate for automobile panel and method of manufacturing the same Expired - Lifetime JP2706310B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1104865A JP2706310B2 (en) 1989-04-25 1989-04-25 Aluminum alloy plate for automobile panel and method of manufacturing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1104865A JP2706310B2 (en) 1989-04-25 1989-04-25 Aluminum alloy plate for automobile panel and method of manufacturing the same

Publications (2)

Publication Number Publication Date
JPH02285045A JPH02285045A (en) 1990-11-22
JP2706310B2 true JP2706310B2 (en) 1998-01-28

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100540703C (en) * 2002-03-22 2009-09-16 皮奇尼何纳吕公司 Be used for welded Al-Mg alloy product

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101880803B (en) * 2010-07-30 2012-10-17 浙江巨科铝业有限公司 Al-Mg aluminum alloy for automobile body panel and method for producing same

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6050864B2 (en) * 1982-03-31 1985-11-11 住友軽金属工業株式会社 Aluminum alloy material for forming with excellent bending workability and its manufacturing method
JPS61264150A (en) * 1985-05-15 1986-11-22 Kobe Steel Ltd Aluminum alloy sheet for can superior in bulge workability
JPS62146234A (en) * 1985-12-18 1987-06-30 Furukawa Alum Co Ltd Aluminum alloy stock and its production
JPS63286589A (en) * 1987-05-19 1988-11-24 Kobe Steel Ltd Hard al alloy sheet for packing having superior curlability and production thereof
JPS6468439A (en) * 1987-09-09 1989-03-14 Kobe Steel Ltd Aluminum alloy plate for can having excellent black stripe resistance
JPH0257656A (en) * 1988-08-23 1990-02-27 Kobe Steel Ltd Aluminum alloy for automobile panel having excellent zinc phosphate treatability and its manufacture

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100540703C (en) * 2002-03-22 2009-09-16 皮奇尼何纳吕公司 Be used for welded Al-Mg alloy product

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