JP2019504078A - （メタ）アクリル酸エステルの精製方法 - Google Patents

（メタ）アクリル酸エステルの精製方法 Download PDF

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Publication number
JP2019504078A
JP2019504078A JP2018538078A JP2018538078A JP2019504078A JP 2019504078 A JP2019504078 A JP 2019504078A JP 2018538078 A JP2018538078 A JP 2018538078A JP 2018538078 A JP2018538078 A JP 2018538078A JP 2019504078 A JP2019504078 A JP 2019504078A
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JP
Japan
Prior art keywords
meth
column
acrylic acid
ester
purified
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Pending
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JP2018538078A
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English (en)
Japanese (ja)
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JP2019504078A5 (https=
Inventor
トレチャク，セルジュ
エス，ナタリー
アギアル，ローズ
コノアール，ピエール−エマニュエル
オズ，クリストフ
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Arkema France SA
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Arkema France SA
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Application filed by Arkema France SA filed Critical Arkema France SA
Publication of JP2019504078A publication Critical patent/JP2019504078A/ja
Publication of JP2019504078A5 publication Critical patent/JP2019504078A5/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/62—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2018538078A 2016-01-21 2017-01-03 （メタ）アクリル酸エステルの精製方法 Pending JP2019504078A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1650469 2016-01-21
FR1650469A FR3047004B1 (fr) 2016-01-21 2016-01-21 Procede de purification d'esters (meth)acryliques
PCT/FR2017/050005 WO2017125657A1 (fr) 2016-01-21 2017-01-03 Procede de purification d'esters (meth)acryliques

Publications (2)

Publication Number Publication Date
JP2019504078A true JP2019504078A (ja) 2019-02-14
JP2019504078A5 JP2019504078A5 (https=) 2020-01-23

Family

ID=55542938

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018538078A Pending JP2019504078A (ja) 2016-01-21 2017-01-03 （メタ）アクリル酸エステルの精製方法

Country Status (9)

Country Link
US (1) US10508074B2 (https=)
EP (1) EP3405450A1 (https=)
JP (1) JP2019504078A (https=)
KR (1) KR102647454B1 (https=)
CN (1) CN108473412A (https=)
BR (1) BR112018013060B1 (https=)
FR (1) FR3047004B1 (https=)
TW (1) TW201738199A (https=)
WO (1) WO2017125657A1 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7337692B2 (ja) 2016-12-21 2023-09-04 ビーエーエスエフ ソシエタス・ヨーロピア 蒸留により対応する粗製アルキルアクリレートから純粋な２－エチルヘキシルアクリレートまたは純粋な２－プロピルヘプチルアクリレートを取得する方法
BR112019011294B1 (pt) 2016-12-21 2022-10-18 Basf Se Processo para isolar acrilato de butila puro de acrilato de butila bruto
EP3558922B1 (de) 2016-12-21 2020-10-14 Basf Se Verfahren zur destillativen gewinnung von rein-tert-butyl(meth)acrylat aus roh-tert-butyl(meth)acrylat
FR3083233B1 (fr) 2018-06-27 2020-05-29 Arkema France Procede de purification d'acrylates legers.
FR3091871B1 (fr) * 2019-01-22 2020-12-18 Arkema France Procede de purification d’esters (meth)acryliques a l’aide d’une colonne a partition
CN113574047A (zh) * 2019-04-16 2021-10-29 罗门哈斯公司 由丙烯酸和甲醇进行的酸催化的丙烯酸甲酯合成
EP3956285B1 (en) * 2019-04-16 2023-04-26 Rohm and Haas Company Acid catalyzed synthesis of methyl acrylate from acrylic acid and methanol
CN112552174B (zh) * 2020-12-23 2023-04-11 江门谦信化工发展有限公司 一种精馏乙酸酯的装置及方法
CN114011341B (zh) * 2021-11-15 2024-12-06 丹东明珠特种树脂有限公司 催化精馏塔和深脱除异丁烯之高纯度mtbe制备系统
WO2025131961A1 (en) * 2023-12-21 2025-06-26 Basf Se Device and process for manufacture of (meth)acrylates

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6299345A (ja) * 1985-10-24 1987-05-08 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの回収法
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
JP2002194022A (ja) * 2000-12-26 2002-07-10 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法、（メタ）アクリル酸エステルおよび（メタ）アクリル樹脂
JP2002205971A (ja) * 2001-01-10 2002-07-23 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法および（メタ）アクリル酸エステル
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
JP2014506235A (ja) * 2010-11-22 2014-03-13 ローム アンド ハース カンパニー アクリレートの製造方法
JP2014508736A (ja) * 2010-12-29 2014-04-10 エルジー・ケム・リミテッド 高純度の２−エチルヘキシル−アクリレート生産のための分離壁型蒸留塔及びこれを利用した製造方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101367720A (zh) * 2008-09-18 2009-02-18 中国石油大学(华东) 一种隔壁共沸精馏塔提纯丙烯酸的工艺方法及装置

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6299345A (ja) * 1985-10-24 1987-05-08 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの回収法
JP2001322968A (ja) * 2000-05-12 2001-11-20 Mitsubishi Rayon Co Ltd メタクリル酸エステルの精製方法
JP2002194022A (ja) * 2000-12-26 2002-07-10 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法、（メタ）アクリル酸エステルおよび（メタ）アクリル樹脂
JP2002205971A (ja) * 2001-01-10 2002-07-23 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの精製方法および（メタ）アクリル酸エステル
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
JP2007045803A (ja) * 2005-08-12 2007-02-22 Asahi Kasei Chemicals Corp 精製されたメタクリル酸メチルを得る方法
JP2014506235A (ja) * 2010-11-22 2014-03-13 ローム アンド ハース カンパニー アクリレートの製造方法
JP2014508736A (ja) * 2010-12-29 2014-04-10 エルジー・ケム・リミテッド 高純度の２−エチルヘキシル−アクリレート生産のための分離壁型蒸留塔及びこれを利用した製造方法

Also Published As

Publication number Publication date
TW201738199A (zh) 2017-11-01
US20190016665A1 (en) 2019-01-17
EP3405450A1 (fr) 2018-11-28
US10508074B2 (en) 2019-12-17
CN108473412A (zh) 2018-08-31
FR3047004B1 (fr) 2019-08-09
BR112018013060B1 (pt) 2022-02-15
FR3047004A1 (fr) 2017-07-28
KR20180108644A (ko) 2018-10-04
WO2017125657A1 (fr) 2017-07-27
BR112018013060A2 (pt) 2018-12-11
KR102647454B1 (ko) 2024-03-13

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