JP2018043972A5 - - Google Patents
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- Publication number
- JP2018043972A5 JP2018043972A5 JP2017118805A JP2017118805A JP2018043972A5 JP 2018043972 A5 JP2018043972 A5 JP 2018043972A5 JP 2017118805 A JP2017118805 A JP 2017118805A JP 2017118805 A JP2017118805 A JP 2017118805A JP 2018043972 A5 JP2018043972 A5 JP 2018043972A5
- Authority
- JP
- Japan
- Prior art keywords
- acid
- dicarboxylic acid
- production method
- carbon atoms
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims 22
- 238000004519 manufacturing process Methods 0.000 claims 19
- 125000004432 carbon atom Chemical group C* 0.000 claims 13
- 229920000642 polymer Polymers 0.000 claims 13
- -1 polyoxyethylene chain Polymers 0.000 claims 13
- 239000013078 crystal Substances 0.000 claims 12
- 150000003839 salts Chemical class 0.000 claims 12
- 239000007864 aqueous solution Substances 0.000 claims 8
- 238000001556 precipitation Methods 0.000 claims 8
- 239000002736 nonionic surfactant Substances 0.000 claims 7
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims 6
- 229920001577 copolymer Polymers 0.000 claims 6
- 238000001816 cooling Methods 0.000 claims 4
- 238000000034 method Methods 0.000 claims 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims 4
- 239000002253 acid Substances 0.000 claims 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims 3
- 239000000194 fatty acid Substances 0.000 claims 3
- 229930195729 fatty acid Natural products 0.000 claims 3
- 239000001530 fumaric acid Substances 0.000 claims 3
- 230000001376 precipitating effect Effects 0.000 claims 3
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 2
- 239000002563 ionic surfactant Substances 0.000 claims 2
- 229920003145 methacrylic acid copolymer Polymers 0.000 claims 2
- 229940117841 methacrylic acid copolymer Drugs 0.000 claims 2
- 238000010979 pH adjustment Methods 0.000 claims 2
- 239000002994 raw material Substances 0.000 claims 2
- 239000001384 succinic acid Substances 0.000 claims 2
- 238000003786 synthesis reaction Methods 0.000 claims 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 2
- JWNWCEAWZGLYTE-UHFFFAOYSA-N 2-(trimethylazaniumyl)butanoate Chemical compound CCC(C([O-])=O)[N+](C)(C)C JWNWCEAWZGLYTE-UHFFFAOYSA-N 0.000 claims 1
- MUZDXNQOSGWMJJ-UHFFFAOYSA-N 2-methylprop-2-enoic acid;prop-2-enoic acid Chemical compound OC(=O)C=C.CC(=C)C(O)=O MUZDXNQOSGWMJJ-UHFFFAOYSA-N 0.000 claims 1
- 229920002126 Acrylic acid copolymer Polymers 0.000 claims 1
- RUIYSHWWARQKKK-UHFFFAOYSA-N C(C(=C)C)(=O)OCCN.C(C(=C)C)(=O)O Chemical compound C(C(=C)C)(=O)OCCN.C(C(=C)C)(=O)O RUIYSHWWARQKKK-UHFFFAOYSA-N 0.000 claims 1
- MYBGXHYNILTXRW-UHFFFAOYSA-N C(C(=C)C)(=O)OCCP(=O)=C(O)C[N+](C)(C)C.C(C(=C)C)(=O)[O-] Chemical group C(C(=C)C)(=O)OCCP(=O)=C(O)C[N+](C)(C)C.C(C(=C)C)(=O)[O-] MYBGXHYNILTXRW-UHFFFAOYSA-N 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims 1
- LGPCLLQCHLRRDE-UHFFFAOYSA-N OC(=O)C=C.CNCCOC(=O)C(C)=C Chemical compound OC(=O)C=C.CNCCOC(=O)C(C)=C LGPCLLQCHLRRDE-UHFFFAOYSA-N 0.000 claims 1
- 229920001214 Polysorbate 60 Polymers 0.000 claims 1
- 239000004372 Polyvinyl alcohol Substances 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 claims 1
- 150000005215 alkyl ethers Chemical class 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 229920006317 cationic polymer Polymers 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 238000000151 deposition Methods 0.000 claims 1
- 150000001991 dicarboxylic acids Chemical class 0.000 claims 1
- 229930182478 glucoside Natural products 0.000 claims 1
- 229920013821 hydroxy alkyl cellulose Polymers 0.000 claims 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims 1
- 239000011976 maleic acid Substances 0.000 claims 1
- 239000000178 monomer Substances 0.000 claims 1
- 230000002093 peripheral effect Effects 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 229920002451 polyvinyl alcohol Polymers 0.000 claims 1
- 239000000600 sorbitol Substances 0.000 claims 1
- 229920003179 starch-based polymer Polymers 0.000 claims 1
- 239000004628 starch-based polymer Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 229920002554 vinyl polymer Polymers 0.000 claims 1
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2017/023515 WO2018047443A1 (ja) | 2016-09-09 | 2017-06-27 | ジカルボン酸結晶及びその製造方法 |
| KR1020197004568A KR102341902B1 (ko) | 2016-09-09 | 2017-06-27 | 디카르복실산 결정 및 그 제조 방법 |
| TW106121388A TWI739856B (zh) | 2016-09-09 | 2017-06-27 | 二羧酸結晶及其製造方法 |
| CN201780051200.1A CN109689609B (zh) | 2016-09-09 | 2017-06-27 | 二羧酸结晶及其制造方法 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2016176416 | 2016-09-09 | ||
| JP2016176416 | 2016-09-09 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018043972A JP2018043972A (ja) | 2018-03-22 |
| JP2018043972A5 true JP2018043972A5 (https=) | 2020-05-21 |
| JP6944746B2 JP6944746B2 (ja) | 2021-10-06 |
Family
ID=61693577
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017118805A Active JP6944746B2 (ja) | 2016-09-09 | 2017-06-16 | ジカルボン酸結晶及びその製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP6944746B2 (https=) |
| CN (1) | CN109689609B (https=) |
| TW (1) | TWI739856B (https=) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10844408B2 (en) | 2015-12-24 | 2020-11-24 | Kao Corporation | Method for manufacturing fumaric acid |
| JP7236285B2 (ja) * | 2019-02-13 | 2023-03-09 | 花王株式会社 | テトラアセチルエチレンジアミン結晶の製造方法 |
| CN117304019A (zh) * | 2022-06-22 | 2023-12-29 | 万华化学(四川)有限公司 | 一种晶体粒径均匀的丁二酸的制备方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS415729B1 (https=) * | 1964-10-24 | 1966-03-29 | ||
| US5034105A (en) * | 1989-07-27 | 1991-07-23 | Michigan Biotechnology Institute | Carboxylic acid purification and crystallization process |
| DE19705329A1 (de) * | 1997-02-12 | 1998-08-13 | Basf Ag | Dicarbonsäurekristallisate |
| JP4170079B2 (ja) * | 2002-11-26 | 2008-10-22 | 花王株式会社 | 粉末洗浄剤組成物 |
| JP2004238321A (ja) * | 2003-02-05 | 2004-08-26 | Kao Corp | 口腔用組成物 |
| JP4842119B2 (ja) * | 2006-12-28 | 2011-12-21 | 花王株式会社 | 粉末洗剤の製造方法 |
| EP2246319A1 (en) * | 2009-04-28 | 2010-11-03 | DSM IP Assets B.V. | Fumaric acid crystallization process |
| JP2012180306A (ja) * | 2011-03-01 | 2012-09-20 | Mitsubishi Chemicals Corp | 脂肪族ジカルボン酸結晶および脂肪族ジカルボン酸の製造方法 |
| FR3028864B1 (fr) * | 2014-11-26 | 2018-05-18 | Roquette Freres | Procede de recuperation de cristaux d'acide succinique avec mise en œuvre de tensioactifs au cours de la cristallisation, cristaux obtenus et leurs utilisations |
| JP7053220B2 (ja) * | 2017-06-15 | 2022-04-12 | 花王株式会社 | ジカルボン酸結晶の製造方法 |
-
2017
- 2017-06-16 JP JP2017118805A patent/JP6944746B2/ja active Active
- 2017-06-27 TW TW106121388A patent/TWI739856B/zh active
- 2017-06-27 CN CN201780051200.1A patent/CN109689609B/zh active Active
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