JP2017517497A5 - - Google Patents
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- Publication number
- JP2017517497A5 JP2017517497A5 JP2016563986A JP2016563986A JP2017517497A5 JP 2017517497 A5 JP2017517497 A5 JP 2017517497A5 JP 2016563986 A JP2016563986 A JP 2016563986A JP 2016563986 A JP2016563986 A JP 2016563986A JP 2017517497 A5 JP2017517497 A5 JP 2017517497A5
- Authority
- JP
- Japan
- Prior art keywords
- cyclotetrasiloxane
- formula
- heptamethyl
- group
- cyclosiloxane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 125000005842 heteroatom Chemical group 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 17
- 229910052760 oxygen Inorganic materials 0.000 claims description 15
- 229910052717 sulfur Inorganic materials 0.000 claims description 15
- 239000003054 catalyst Substances 0.000 claims description 13
- 229910052736 halogen Inorganic materials 0.000 claims description 13
- 150000002367 halogens Chemical class 0.000 claims description 12
- 238000006459 hydrosilylation reaction Methods 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 125000006652 (C3-C12) cycloalkyl group Chemical group 0.000 claims description 8
- 125000003342 alkenyl group Chemical group 0.000 claims description 8
- 125000002877 alkyl aryl group Chemical group 0.000 claims description 8
- 125000000304 alkynyl group Chemical group 0.000 claims description 8
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 8
- 125000003118 aryl group Chemical group 0.000 claims description 8
- 125000000392 cycloalkenyl group Chemical group 0.000 claims description 8
- 125000004404 heteroalkyl group Chemical group 0.000 claims description 8
- 125000001072 heteroaryl group Chemical group 0.000 claims description 8
- 125000000623 heterocyclic group Chemical group 0.000 claims description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims description 7
- 239000001257 hydrogen Substances 0.000 claims description 7
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 4
- 125000000524 functional group Chemical group 0.000 claims description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 4
- 238000006243 chemical reaction Methods 0.000 claims 4
- -1 1-phenylvinyl Chemical group 0.000 claims 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- 229910052697 platinum Inorganic materials 0.000 claims 3
- CFNAPNIXPUMJSP-UHFFFAOYSA-N 2,2,4,4,6,6,8-heptamethyl-8-(2-phenylethenyl)-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound O1[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si]1(C)C=CC1=CC=CC=C1 CFNAPNIXPUMJSP-UHFFFAOYSA-N 0.000 claims 2
- HCDVTAHLGOSFQN-UHFFFAOYSA-N 2-(1-phenylethenyl)-4-(2-phenylethenyl)-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound C1(=CC=CC=C1)C(=C)[SiH]1O[SiH](O[SiH2]O[SiH2]O1)C=CC1=CC=CC=C1 HCDVTAHLGOSFQN-UHFFFAOYSA-N 0.000 claims 2
- FNGGZWAATUWAJZ-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C(=C)C1=CC=CC=C1)C)(C(=C)C1=CC=CC=C1)C)(C(=C)C1=CC=CC=C1)C)C(=C)C1=CC=CC=C1 Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C(=C)C1=CC=CC=C1)C)(C(=C)C1=CC=CC=C1)C)(C(=C)C1=CC=CC=C1)C)C(=C)C1=CC=CC=C1 FNGGZWAATUWAJZ-UHFFFAOYSA-N 0.000 claims 2
- ORLLOXPUFWBUKD-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C(=C)C1=CC=C(C=C1)C(F)(F)F)C)C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C(=C)C1=CC=C(C=C1)C(F)(F)F)C)C ORLLOXPUFWBUKD-UHFFFAOYSA-N 0.000 claims 2
- FMYLXJJLWCRHJE-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C(=C)C1=CC=CC=C1)C)C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C(=C)C1=CC=CC=C1)C)C FMYLXJJLWCRHJE-UHFFFAOYSA-N 0.000 claims 2
- JAUMDILTRARNGD-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(C(C)(O)C)=C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(C(C)(O)C)=C JAUMDILTRARNGD-UHFFFAOYSA-N 0.000 claims 2
- NFEVXBSIQGLDPV-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(CCC(=O)O)=C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(CCC(=O)O)=C NFEVXBSIQGLDPV-UHFFFAOYSA-N 0.000 claims 2
- GQWWFOMZTWQSBO-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(CCCO)=C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C(CCCO)=C GQWWFOMZTWQSBO-UHFFFAOYSA-N 0.000 claims 2
- MBWGUPIKYNCPKK-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CC(C)(O)C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CC(C)(O)C MBWGUPIKYNCPKK-UHFFFAOYSA-N 0.000 claims 2
- KSWNLVJFDMCSOK-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CCCC(=O)O Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CCCC(=O)O KSWNLVJFDMCSOK-UHFFFAOYSA-N 0.000 claims 2
- IVISUCMNFVIESR-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CCCCO Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C)C)C=CCCCO IVISUCMNFVIESR-UHFFFAOYSA-N 0.000 claims 2
- JTLNXJOXFKTXCW-UHFFFAOYSA-N C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C=CC1=CC=C(C=C1)C(F)(F)F)C)C Chemical compound C[Si]1(O[Si](O[Si](O[Si](O1)(C)C)(C)C)(C=CC1=CC=C(C=C1)C(F)(F)F)C)C JTLNXJOXFKTXCW-UHFFFAOYSA-N 0.000 claims 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims 2
- RCNRJBWHLARWRP-UHFFFAOYSA-N ethenyl-[ethenyl(dimethyl)silyl]oxy-dimethylsilane;platinum Chemical compound [Pt].C=C[Si](C)(C)O[Si](C)(C)C=C RCNRJBWHLARWRP-UHFFFAOYSA-N 0.000 claims 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- 239000010948 rhodium Substances 0.000 claims 2
- 239000000377 silicon dioxide Substances 0.000 claims 2
- 239000007983 Tris buffer Substances 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 239000012300 argon atmosphere Substances 0.000 claims 1
- 239000012298 atmosphere Substances 0.000 claims 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims 1
- 239000000969 carrier Substances 0.000 claims 1
- 239000003610 charcoal Substances 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims 1
- 229910052741 iridium Inorganic materials 0.000 claims 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 claims 1
- 230000007935 neutral effect Effects 0.000 claims 1
- 239000013110 organic ligand Substances 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 150000003003 phosphines Chemical class 0.000 claims 1
- 229910000073 phosphorus hydride Inorganic materials 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 229910052703 rhodium Inorganic materials 0.000 claims 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 1
Images
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14165544.9A EP2937353A1 (en) | 2014-04-23 | 2014-04-23 | Method for the preparation of functionalized cyclosiloxanes |
| EP14165544.9 | 2014-04-23 | ||
| PCT/EP2015/058638 WO2015162145A1 (en) | 2014-04-23 | 2015-04-22 | Method for the preparation of functionalized cyclosiloxanes |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017517497A JP2017517497A (ja) | 2017-06-29 |
| JP2017517497A5 true JP2017517497A5 (enExample) | 2018-06-07 |
| JP6608844B2 JP6608844B2 (ja) | 2019-11-20 |
Family
ID=50513133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016563986A Expired - Fee Related JP6608844B2 (ja) | 2014-04-23 | 2015-04-22 | 官能化シクロシロキサンの調製のための方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10059728B2 (enExample) |
| EP (1) | EP2937353A1 (enExample) |
| JP (1) | JP6608844B2 (enExample) |
| KR (1) | KR20160148605A (enExample) |
| CN (1) | CN106414464A (enExample) |
| TW (1) | TWI672312B (enExample) |
| WO (1) | WO2015162145A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112225852B (zh) * | 2020-09-28 | 2021-10-08 | 浙江大学 | 一种聚硅氧烷功能化乙烯-降冰片烯共聚物及其制备方法 |
| CN116789967A (zh) * | 2023-06-29 | 2023-09-22 | 中国科学院化学研究所 | 一种分子量可控的乙基硅氧烷聚合物的制备方法及其应用 |
| CN117003789A (zh) * | 2023-07-03 | 2023-11-07 | 衢州科峰新材料有限公司 | 一种甲基乙基环硅氧烷的制备方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2762829A (en) | 1952-01-02 | 1956-09-11 | Stanolind Oil & Gas Co | Process for converting olefins to oxygenated organic compounds |
| US2793222A (en) | 1954-05-11 | 1957-05-21 | Gen Electric | 1, 2-bis-heptamethylcyclotetrasiloxanylethane and polymeric derivatives thereof |
| US2785147A (en) | 1954-05-11 | 1957-03-12 | Gen Electric | Process for making octamethylcyclotetrasiloxane gels |
| US5352753A (en) * | 1991-04-25 | 1994-10-04 | Allergan, Inc. | Ultraviolet light absorbing compounds, silicone compositions and methods for making same |
| JPH0517486A (ja) * | 1991-07-04 | 1993-01-26 | Shin Etsu Chem Co Ltd | 有機ケイ素化合物及びその製造方法 |
| US7138108B2 (en) * | 2002-06-13 | 2006-11-21 | L'oreal | Photoprotective UV-screening compositions comprising (phenylsulfonyl) acrylonitrile-substituted silanes/siloxanes |
| JP4217870B2 (ja) * | 2002-07-15 | 2009-02-04 | 日本電気株式会社 | 有機シロキサン共重合体膜、その製造方法、成長装置、ならびに該共重合体膜を用いた半導体装置 |
| JP4296006B2 (ja) | 2003-02-27 | 2009-07-15 | 独立行政法人科学技術振興機構 | ビニルシランの製造方法 |
| US8501893B2 (en) | 2008-01-25 | 2013-08-06 | National Science And Technology Development Agency | Synthetic method for preparing dual curable silicone compositions |
| JP2011144272A (ja) * | 2010-01-15 | 2011-07-28 | Nippon Shokubai Co Ltd | ジルコニアナノ粒子を含むシリコーン樹脂組成物 |
-
2014
- 2014-04-23 EP EP14165544.9A patent/EP2937353A1/en not_active Withdrawn
-
2015
- 2015-04-10 TW TW104111543A patent/TWI672312B/zh not_active IP Right Cessation
- 2015-04-22 WO PCT/EP2015/058638 patent/WO2015162145A1/en not_active Ceased
- 2015-04-22 CN CN201580020913.2A patent/CN106414464A/zh active Pending
- 2015-04-22 KR KR1020167032298A patent/KR20160148605A/ko not_active Withdrawn
- 2015-04-22 JP JP2016563986A patent/JP6608844B2/ja not_active Expired - Fee Related
-
2016
- 2016-10-17 US US15/294,920 patent/US10059728B2/en not_active Expired - Fee Related
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