JP2017515986A5 - - Google Patents
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- Publication number
- JP2017515986A5 JP2017515986A5 JP2016553534A JP2016553534A JP2017515986A5 JP 2017515986 A5 JP2017515986 A5 JP 2017515986A5 JP 2016553534 A JP2016553534 A JP 2016553534A JP 2016553534 A JP2016553534 A JP 2016553534A JP 2017515986 A5 JP2017515986 A5 JP 2017515986A5
- Authority
- JP
- Japan
- Prior art keywords
- polysilazane
- fiber
- vinyl
- temperature
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000835 fiber Substances 0.000 claims 18
- 229920001709 polysilazane Polymers 0.000 claims 17
- 238000000034 method Methods 0.000 claims 12
- 239000011347 resin Substances 0.000 claims 9
- 229920005989 resin Polymers 0.000 claims 9
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims 8
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 6
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 5
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 5
- 238000001723 curing Methods 0.000 claims 5
- 229920002554 vinyl polymer Polymers 0.000 claims 5
- 125000003342 alkenyl group Chemical group 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 4
- 238000009987 spinning Methods 0.000 claims 4
- 150000001367 organochlorosilanes Chemical class 0.000 claims 3
- 125000004400 (C1-C12) alkyl group Chemical group 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- 239000000654 additive Substances 0.000 claims 2
- 239000000460 chlorine Substances 0.000 claims 2
- 229910052801 chlorine Inorganic materials 0.000 claims 2
- 125000001309 chloro group Chemical group Cl* 0.000 claims 2
- KQHIGRPLCKIXNJ-UHFFFAOYSA-N chloro-methyl-silylsilane Chemical class C[SiH]([SiH3])Cl KQHIGRPLCKIXNJ-UHFFFAOYSA-N 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000003112 inhibitor Substances 0.000 claims 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims 2
- 150000002978 peroxides Chemical group 0.000 claims 2
- -1 vinyl benzyl Chemical group 0.000 claims 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 150000004978 peroxycarbonates Chemical class 0.000 claims 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims 1
- 229910010271 silicon carbide Inorganic materials 0.000 claims 1
- 125000005504 styryl group Chemical group 0.000 claims 1
- 230000007704 transition Effects 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/193,158 US9587331B2 (en) | 2014-02-28 | 2014-02-28 | Method for curing of green polysilazane-based silicon carbide precursor fibers |
| US14/193,158 | 2014-02-28 | ||
| PCT/US2015/016768 WO2015130564A1 (en) | 2014-02-28 | 2015-02-20 | Method for curing of green polysilazane-based silicon carbide precursor fibers |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017515986A JP2017515986A (ja) | 2017-06-15 |
| JP2017515986A5 true JP2017515986A5 (enExample) | 2018-03-22 |
| JP6626451B2 JP6626451B2 (ja) | 2019-12-25 |
Family
ID=52627572
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016553534A Active JP6626451B2 (ja) | 2014-02-28 | 2015-02-20 | 未焼結ポリシラザン系炭化ケイ素前駆体繊維の硬化方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US9587331B2 (enExample) |
| EP (1) | EP3110773B1 (enExample) |
| JP (1) | JP6626451B2 (enExample) |
| CN (1) | CN106061921B (enExample) |
| CA (1) | CA2940148C (enExample) |
| WO (1) | WO2015130564A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9593210B1 (en) * | 2015-06-03 | 2017-03-14 | General Electric Company | Methods of preparing polysilazane resin with low halogen content |
| KR102548405B1 (ko) * | 2017-04-20 | 2023-06-28 | (주)디엔에프 | 다이실릴아민 화합물을 포함하는 실리콘 함유 박막증착용 조성물 및 이를 이용하는 실리콘 함유 박막의 제조방법 |
| US20220340494A1 (en) * | 2019-09-13 | 2022-10-27 | Kansas State University Research Foundation | Polymer-derived ceramic fibers and methods of preparing the same |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3098830A (en) | 1961-04-14 | 1963-07-23 | Gen Electric | Polymeric silazanes |
| FR2581391B1 (fr) * | 1985-05-06 | 1987-06-05 | Rhone Poulenc Rech | Composition organo-polysilazane comportant des generateurs de radicaux libres et reticulable par apport d'energie |
| US4631260A (en) | 1985-06-24 | 1986-12-23 | Dow Corning Corporation | Process for preparing ceramic materials |
| US4997601A (en) | 1988-01-19 | 1991-03-05 | Hoechst Celanese Corp. | Process for dry spinning thermally sensitive organosilicon preceramic fibers with production of ceramic fibers therefrom |
| US4942011A (en) | 1988-05-03 | 1990-07-17 | E. I. Du Pont De Nemours And Company | Process for preparing silicon carbide fibers |
| US4929704A (en) | 1988-12-20 | 1990-05-29 | Hercules Incorporated | Isocyanate- and isothiocyanate-modified polysilazane ceramic precursors |
| US5223461A (en) | 1989-06-05 | 1993-06-29 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Ceramic silicon-boron-carhon fibers from organic silicon-boron-polymers |
| US5155181A (en) | 1989-11-27 | 1992-10-13 | Hercules Incorporated | (Thio)amide-modified silazane polymer composition containing a free radical generator |
| US5032649A (en) | 1989-11-27 | 1991-07-16 | Hercules Incorporated | Organic amide-modified polysilazane ceramic precursors |
| US5268336A (en) | 1990-06-18 | 1993-12-07 | Dow Corning Corporation | Preparation of substantially polycrystalline silicon carbide fibers from methylpolydisilylazanes |
| US5086126A (en) * | 1990-12-24 | 1992-02-04 | Dow Corning Corporation | Method for producing functional silazane polymers |
| US5171722A (en) | 1991-10-09 | 1992-12-15 | University Of Florida | SiC fibers having low oxygen content and methods of preparation |
| US5242870A (en) | 1991-10-09 | 1993-09-07 | University Of Florida | SIC fibers having low oxygen content and methods of preparation |
| US5792416A (en) * | 1996-05-17 | 1998-08-11 | University Of Florida | Preparation of boron-doped silicon carbide fibers |
| JP2001279535A (ja) * | 2000-01-25 | 2001-10-10 | Ube Ind Ltd | 結晶性炭化ケイ素系無機繊維及びその製造方法 |
| JP2007031186A (ja) * | 2005-07-25 | 2007-02-08 | Chugoku Electric Power Co Inc:The | 繊維結合体又はその製造方法 |
| US7700202B2 (en) * | 2006-02-16 | 2010-04-20 | Alliant Techsystems Inc. | Precursor formulation of a silicon carbide material |
| US20090001219A1 (en) * | 2006-12-07 | 2009-01-01 | Honeywell International, Inc. | Fiber polymer matrix composites having silicon-containing inorganic-organic matrices and methods of making the same |
| US8987402B2 (en) | 2010-02-26 | 2015-03-24 | General Electric Company | Stoichiometric silicon carbide fibers from thermo-chemically cured polysilazanes |
| US9045347B2 (en) | 2010-02-26 | 2015-06-02 | General Electric Company | Stiochiometric silicon carbide fibers from thermo-chemically cured polysilazanes |
| US9359479B2 (en) | 2013-05-30 | 2016-06-07 | General Electric Company | Methods of using boron-containing additives as silicon carbide crosslinking agents |
-
2014
- 2014-02-28 US US14/193,158 patent/US9587331B2/en active Active
-
2015
- 2015-02-20 CN CN201580010709.2A patent/CN106061921B/zh active Active
- 2015-02-20 CA CA2940148A patent/CA2940148C/en active Active
- 2015-02-20 WO PCT/US2015/016768 patent/WO2015130564A1/en not_active Ceased
- 2015-02-20 EP EP15708076.3A patent/EP3110773B1/en active Active
- 2015-02-20 JP JP2016553534A patent/JP6626451B2/ja active Active
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